A method is presented for producing hollow microspheres of metal oxides (HMOMS) and/or hollow metal silicates microspheres (HMSMS) in a transforming solution. The transforming solution contains an atom M, or an M-ion, or a radical containing M. M in the transforming solution has the thermodynamic ability to replace silicon atoms in hollow silica microspheres (HSMS) and/or hollow glass microspheres (HGMS). The maximum temperature for transformation is set by the chemical physical properties of the transforming solution, and the viscosity of the silica in the walls of the HSMS and/or the glass in the walls of the HGMS. Viscosity, of enough magnitude, helps retain the desired shape of the hollow sphere as it is transformed to HMOMS and/or HMSMS. Non-spherical shapes can be produced by increasing the transformation temperature whereby the viscosity of the walls of the HSMS and/or the HGMS is reduced. Transformation can take place at a single temperature or at several temperatures, each temperature for a separate hold time.
A method is presented for producing hollow microspheres of metal oxides (HMOMS) and/or hollow metal silicates microspheres (HMSMS) in a transforming solution. The transforming solution contains an atom M, or an M-ion, or a radical containing M. M in the transforming solution has the thermodynamic ability to replace silicon atoms in hollow silica microspheres (HSMS) and/or hollow glass microspheres (HGMS). The maximum temperature for transformation is set by the chemical physical properties of the transforming solution, and the viscosity of the silica in the walls of the HSMS and/or the glass in the walls of the HGMS. Viscosity, of enough magnitude, helps retain the desired shape of the hollow sphere as it is transformed to HMOMS and/or HMSMS. Non-spherical shapes can be produced by increasing the transformation temperature whereby the viscosity of the walls of the HSMS and/or the HGMS is reduced. Transformation can take place at a single temperature or at several temperatures, each temperature for a separate hold time.
Methods are presented for:
1. production of micro composite castings and continuous production of sheets of micro composites, both consisting of hollow spheres in a matrix,
2. harvesting of HMOMS and HMSMS, and
3. specialty castings for anisotropic properties using 3-dimensional printing
Increasing Tortuosity To Decrease Heat Transfer In Hollow Structures By Shaping The Hollow Structures, A Process That Entails Distribution Of Forces During Transformation Of Seeds
Methods are presented for altering the thermal conductivity of a material consisting of sealed and hollow structures by altering their shape to impact heat transfer through increasing tortuosity and altering molecular behavior of gas within the hollow structures. Procedures are presented whereby desired shape of the hollow structures can be formed as seeds and are transformed into the sealed and hollow structures that constitute VacuBoards and HollowBoards. Techniques are presented to prevent the impact of gravitational forces that can collapse hollow structures during their formation and cooling.
C03B 19/08 - Other methods of shaping glass by foaming
3.
INCREASING TORTUOSITY TO DECREASE HEAT TRANSFER IN HOLLOW STRUCTURES BY SHAPING THE HOLLOW STRUCTURES, A PROCESS THAT ENTAILS DISTRIBUTION OF FORCES DURING TRANSFORMATION OF SEEDS
Methods are presented for altering the thermal conductivity of a material consisting of sealed and hollow structures by altering their shape to impact heat transfer through increasing tortuosity and altering molecular behavior of gas within the hollow structures. Procedures are presented whereby desired shape of the hollow structures can be formed as seeds and are transformed into the sealed and hollow structures that constitute VacuBoards and HollowBoards. Techniques are presented to prevent the impact of gravitational forces that can collapse hollow structures during their formation and cooling.
A novel plasma generation and containment system includes a first electrode, a second electrode, a power source, and an electromagnet. The first electrode and the second electrode are electrically coupled via a wire to form an open circuit. The voltage is asserted on the open circuit to form a spark between the first electrode and the second electrode to form a closed circuit. Then, a current is asserted on the closed circuit to form a plasma between the first electrode and the second electrode. The electromagnet provides a magnetic field to contain and compress the plasma.
An example method for producing a seed capable of transforming into a hollow structure includes providing a core, forming a coating around the core to create a coated core, forming an exterior layer surrounding the coated core, forming a layer of release agent surrounding the exterior layer, and heating the core, the coating and the exterior layer. Heating the core, the coating, and the exterior layer to a particular temperature transforms the exterior layer to a fixed shell and produces a seed with the coated core surrounded by the fixed shell. The particular temperature is sufficient to fuse or sinter the exterior layer, but too low to fuse the coating, and too low to cause the core to generate a gas.
An example method for producing a seed capable of transforming into a hollow structure includes providing a core, forming a coating around the core to create a coated core, forming an exterior layer surrounding the coated core, forming a layer of release agent surrounding the exterior layer, and heating the core, the coating and the exterior layer. Heating the core, the coating, and the exterior layer to a particular temperature transforms the exterior layer to a fixed shell and produces a seed with the coated core surrounded by the fixed shell. The particular temperature is sufficient to fuse or sinter the exterior layer, but too low to fuse the coating, and too low to cause the core to generate a gas.
A process for producing solar grade silicon from silica sand employs a plurality of plasma furnaces to perform a sequence of chemical reactions together with other process steps to produce solar grade silicon. The plasma furnace generates a stable dirty air, donutshaped plasma into which particulate matter can be introduced. The plasma in the first two stages is formed by gases from the chemical reactions and in the third from inert gasses. Cyclone separators are used to extract particulates from the plasma in an inert gas that prevents reverse reactions as the particular cools.
C01B 33/025 - Preparation by reduction of silica or silica-containing material with carbon or a solid carbonaceous material, i.e. carbo-thermal process
C01B 33/18 - Preparation of finely divided silica neither in sol nor in gel formAfter-treatment thereof
Methods for producing a hollow spheres, optionally with a vacuum inside, are disclosed. An example method includes providing a seed with a core and a coating. The seed is heated to a temperature sufficient to transform the coating into a continuous shell having an interior and an exterior. The shell isolates the core from the exterior of the shell. The temperature is also sufficient to cause a reaction with the materials of the core, and the reaction converts the core to a gas within said shell. Controlling the rate of heating and the pressure surrounding the shell allows the shell to expand responsive to gas pressure within the shell. Cooling the shell causes the gases within the shell to revert to a solid form, thereby creating a vacuum within the shell. Products incorporating the hollow spheres are also disclosed.
Methods and apparatus are disclosed for producing seeds that are transformed into hollow spheres. A seed includes a core and a coating. Upon heating, the coating becomes viscous and expands responsive to an internal gas pressure created by the core. Example applications for the seeds and/or cores are disclosed, including bricks and other construction materials having the hollow spheres incorporated therein.
Methods and apparatus are disclosed for producing seeds that are transformed into hollow spheres. A seed includes a core and a coating. Upon heating, the coating becomes viscous and expands responsive to an internal gas pressure created by the core. Example applications for the seeds and/or cores are disclosed, including bricks and other construction materials having the hollow spheres incorporated therein.
Methods and apparatus are disclosed for producing seeds that are transformed into hollow spheres. A seed includes a core and a coating. Upon heating, the coating becomes viscous and expands responsive to an internal gas pressure created by the core. Example applications for the seeds and/or cores are disclosed, including bricks and other construction materials having the hollow spheres incorporated therein.
Methods for producing a hollow spheres, optionally with a vacuum inside, are disclosed. An example method includes providing a seed with a core and a coating. The seed is heated to a temperature sufficient to transform the coating into a continuous shell having an interior and an exterior. The shell isolates the core from the exterior of the shell. The temperature is also sufficient to cause a reaction with the materials of the core, and the reaction converts the core to a gas within said shell. Controlling the rate of heating and the pressure surrounding the shell allows the shell to expand responsive to gas pressure within the shell. Cooling the shell causes the gases within the shell to revert to a solid form, thereby creating a vacuum within the shell. Products incorporating the hollow spheres are also disclosed.
Methods for producing a hollow spheres, optionally with a vacuum inside, are disclosed. An example method includes providing a seed with a core and a coating. The seed is heated to a temperature sufficient to transform the coating into a continuous shell having an interior and an exterior. The shell isolates the core from the exterior of the shell. The temperature is also sufficient to cause a reaction with the materials of the core, and the reaction converts the core to a gas within said shell. Controlling the rate of heating and the pressure surrounding the shell allows the shell to expand responsive to gas pressure within the shell. Cooling the shell causes the gases within the shell to revert to a solid form, thereby creating a vacuum within the shell. Products incorporating the hollow spheres are also disclosed.
A novel plasma generation and containment system includes a first electrode, a second electrode, a power source, and an electromagnet. The first electrode and the second electrode are electrically coupled via a wire to form an open circuit. The voltage is asserted on the open circuit to form a spark between the first electrode and the second electrode to form a closed circuit. Then, a current is asserted on the closed circuit to form a plasma between the first electrode and the second electrode. The electromagnet provides a magnetic field to contain and compress the plasma.
A method is presented for producing hollow microspheres of metal oxides (HMOMS) and/or hollow metal silicates microspheres (HMSMS) in a transforming solution. The transforming solution contains an atom M, or an M-ion, or a radical containing M. M in the transforming solution has the thermodynamic ability to replace silicon atoms in hollow silica microspheres (HSMS) and/or hollow glass microspheres (HGMS). The maximum temperature for transformation is set by the chemical physical properties of the transforming solution, and the viscosity of the silica in the walls of the HSMS and/or the glass in the walls of the HGMS. Viscosity, of enough magnitude, helps retain the desired shape of the hollow sphere as it is transformed to HMOMS and/or HMSMS. Non-spherical shapes can be produced by increasing the transformation temperature whereby the viscosity of the walls of the HSMS and/or the HGMS is reduced. Transformation can take place at a single temperature or at several temperatures, each temperature for a separate hold time.
3. specialty castings for anisotropic properties using 3-dimensional printing.
A method is presented for producing hollow microspheres of metal oxides (HMOMS) and/or hollow metal silicates microspheres (HMSMS) in a transforming solution. The transforming solution contains an atom M, or an M-ion, or a radical containing M. M in the transforming solution has the thermodynamic ability to replace silicon atoms in hollow silica microspheres (HSMS) and/or hollow glass microspheres (HGMS). The maximum temperature for transformation is set by the chemical physical properties of the transforming solution, and the viscosity of the silica in the walls of the HSMS and/or the glass in the walls of the HGMS. Viscosity, of enough magnitude, helps retain the desired shape of the hollow sphere as it is transformed to HMOMS and/or HMSMS. Non- spherical shapes can be produced by increasing the transformation temperature whereby the viscosity of the walls of the HSMS and/or the HGMS is reduced. Transformation can take place at a single temperature or at several temperatures, each temperature for a separate hold time. Methods are presented for: 1. production of micro composite castings and continuous production of sheets of micro composites, both consisting of hollow spheres in a matrix, 2. harvesting of HMOMS and HMSMS, and 3. specialty castings for anisotropic properties using 3 -dimensional printing.
A method is presented for producing hollow microspheres of metal oxides (HMOMS) and/or hollow metal silicates microspheres (HMSMS) in a transforming solution. The transforming solution contains an atom M, or an M-ion, or a radical containing M. M in the transforming solution has the thermodynamic ability to replace silicon atoms in hollow silica microspheres (HSMS) and/or hollow glass microspheres (HGMS). The maximum temperature for transformation is set by the chemical physical properties of the transforming solution, and the viscosity of the silica in the walls of the HSMS and/or the glass in the walls of the HGMS. Viscosity, of enough magnitude, helps retain the desired shape of the hollow sphere as it is transformed to HMOMS and/or HMSMS. Non- spherical shapes can be produced by increasing the transformation temperature whereby the viscosity of the walls of the HSMS and/or the HGMS is reduced. Transformation can take place at a single temperature or at several temperatures, each temperature for a separate hold time. Methods are presented for: 1. production of micro composite castings and continuous production of sheets of micro composites, both consisting of hollow spheres in a matrix, 2. harvesting of HMOMS and HMSMS, and 3. specialty castings for anisotropic properties using 3 -dimensional printing.
A process for producing solar grade silicon from an impurity containing silica employs a plurality of plasma furnaces to perform a sequence of chemical reactions together with other process steps to produce solar grade silicon. The plasma furnace generates a stable dirty air, donut-shaped plasma into which particulate matter can be introduced. The plasma in the first two stages is formed by gases from the chemical reactions and in the third from inert gasses. Cyclone separators are used to extract particulates from the plasma in an inert gas that prevents reverse reactions as the particular cools.
C01B 33/025 - Preparation by reduction of silica or silica-containing material with carbon or a solid carbonaceous material, i.e. carbo-thermal process
C01B 33/18 - Preparation of finely divided silica neither in sol nor in gel formAfter-treatment thereof
19.
REFINING PROCESS FOR PRODUCING SOLAR SILICON, SILICON CARBIDE, HIGH-PURITY GRAPHITE AND HOLLOW SILICA MICROSPHERES
A process for producing solar grade silicon from an impurity containing silica employs a plurality of plasma furnaces to perform a sequence of chemical reactions together with other process steps to produce solar grade silicon. The plasma furnace generates a stable dirty air, donut-shaped plasma into which particulate matter can be introduced. The plasma in the first two stages is formed by gases from the chemical reactions and in the third from inert gasses. Cyclone separators are used to extract particulates from the plasma in an inert gas that prevents reverse reactions as the particular cools.
C01B 33/025 - Preparation by reduction of silica or silica-containing material with carbon or a solid carbonaceous material, i.e. carbo-thermal process
A novel plasma generation and containment system includes a first electrode, a second electrode, a power source, and an electromagnet. The first electrode and the second electrode are electrically coupled via a wire to form an open circuit. The voltage is asserted on the open circuit to form a spark between the first electrode and the second electrode to form a closed circuit. Then, a current is asserted on the closed circuit to form a plasma between the first electrode and the second electrode. The electromagnet provides a magnetic field to contain and compress the plasma.
A novel plasma generation and containment system includes a first electrode, a second electrode, a power source, and an electromagnet. The first electrode and the second electrode are electrically coupled via a wire to form an open circuit. The voltage is asserted on the open circuit to form a spark between the first electrode and the second electrode to form a closed circuit. Then, a current is asserted on the closed circuit to form a plasma between the first electrode and the second electrode. The electromagnet provides a magnetic field to contain and compress the plasma.
patents
