SLT Technologies, Inc.

United States of America

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C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes 60
C30B 29/40 - AIIIBV compounds 50
H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof 22
H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds 21
H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof 19
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1.

IMPROVED ALUMINUM-CONTAINING NITRIDE CERAMIC MATRIX COMPOSITE, METHOD OF MAKING, AND METHOD OF USE

      
Application Number US2024017969
Publication Number 2024/215403
Status In Force
Filing Date 2024-03-01
Publication Date 2024-10-17
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Italiano, David N.

Abstract

Embodiments of disclosure may provide a method for forming an aluminum- containing nitride ceramic matrix composite, comprising heating a green body, an aluminum-containing composition, ammonia and a mineralizer composition in a sealable container to a temperature between about 400 degrees Celsius and about 800 degrees Celsius and a pressure between about 10 MPa and about 1000 MPa, to form an aluminum-containing nitride ceramic matrix composite characterized by a phosphor-to-aluminum nitride (AIN) ratio, by volume, between about 1 % and about 99%, by a porosity between about 1 % and about 50%, and by a thermal conductivity between about 1 watt per meter-Kelvin and about 320 watts per meter-Kelvin. The green body comprises a phosphor powder comprising at least one phosphor composition, wherein the phosphor powder particles are characterized by a D50 diameter between about 100 nanometers and about 500 micrometers, and the green body has a porosity between about 10% and about 80%. The aluminum-containing composition has a purity, on a metals basis, between about 90% and about 99.9999%. The fraction of free volume within the sealable container contains between about 10% and about 95% of liquid ammonia prior to heating the green body, the aluminum- containing composition, ammonia and the mineralizer composition in the sealable container.

2.

HIGH QUALITY GROUP-III METAL NITRIDE CRYSTALS AND METHODS OF MAKING

      
Application Number US2024023419
Publication Number 2024/211817
Status In Force
Filing Date 2024-04-05
Publication Date 2024-10-10
Owner
  • SLT TECHNOLOGIES, INC. (USA)
  • KYOCERA CORPORATION (Japan)
Inventor
  • D'Evelyn, Mark P.
  • Tsukada, Yusuke
  • Kamikawa, Takeshi

Abstract

Embodiments of the disclosure include a free-standing crystal, comprising a group III metal and nitrogen. The free-standing crystal can include a wurtzite crystal structure, a first surface having a maximum dimension greater than 80 millimeters in a first direction, an average concentration of stacking faults below 103cm-1, and an average concentration of threading dislocations between 1 cm-2and 106cm-2, wherein the average concentration of threading dislocations on the first surface varies periodically by at least a factor of two in the first direction, a period of the variation in the first direction being between 5 micrometers and 20 millimeters. Each of five points are distributed evenly within a central 80% of an area of the first surface, the free-standing crystal is characterized by a x-ray rocking curve in the first direction having a full-width-at-half-maximum FWHM± value that is greater than the FWHM± value of an x-ray rocking curve measured in a second direction orthogonal to the first direction by a difference corresponding to a difference in crystallographic orientation between about 0.01 degrees and about 0.4 degrees.

IPC Classes  ?

  • C30B 29/40 - AIIIBV compounds
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 23/04 - Pattern deposit, e.g. by using masks
  • C30B 25/04 - Pattern deposit, e.g. by using masks
  • C30B 33/06 - Joining of crystals

3.

IMPROVED PROCESS FOR RETROGRADE SOLVOTHERMAL CRYSTAL GROWTH AND SINGLE CRYSTAL GROWN THEREBY

      
Application Number US2024012253
Publication Number 2024/155944
Status In Force
Filing Date 2024-01-19
Publication Date 2024-07-25
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Cardwell, Drew, W.
  • Ehrentraut, Dirk
  • D'Evelyn, Mark, P.
  • Pakalapati, Rajeev Tirumala

Abstract

Embodiments of the disclosure include a free-standing crystal, comprising a group III metal and nitrogen. The free-standing crystal may comprise: a wurtzite crystal structure; a growth direction, the growth direction being selected from one of [0 0 0 ±1 ], {1 0 -1 0}, {1 0 -1 ±1 }, or {1 0 -1 ±2}. A first surface having a dislocation density between 1 cm-2and 107cm 2, the dislocations having an orientation within 30 degrees of the growth direction, and an average impurity concentration of H greater than 1017cm-3. The free-standing crystal having at least four sets of bands, wherein each set of bands includes a first sub-band and a second sub-band, the first sub-band having a concentration of at least one impurity selected from H, O, Li, Na, K, F, Cl, Br, and I; and each of the at least four sets of bands have portions that are substantially parallel.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds

4.

PROCESS FOR RETROGRADE SOLVOTHERMAL CRYSTAL GROWTH AND SINGLE CRYSTAL GROWN THEREBY

      
Application Number 18418141
Status Pending
Filing Date 2024-01-19
First Publication Date 2024-07-25
Owner SLT Technologies, Inc. (USA)
Inventor
  • Cardwell, Drew W.
  • Ehrentraut, Dirk
  • D'Evelyn, Mark P.
  • Pakalapati, Rajeev Tirumala

Abstract

Embodiments of the disclosure include a free-standing crystal, comprising a group III metal and nitrogen. The free-standing crystal may comprise: a wurtzite crystal structure; a growth direction, the growth direction being selected from one of [0 0 0 ±1], {1 0 −1 0}, {1 0 −1 ±1}, or {1 0 −1 ±2}. A first surface having a dislocation density between 1 cm−2 and 107 cm−2, the dislocations having an orientation within 30 degrees of the growth direction, and an average impurity concentration of H greater than 1017 cm−3. The free-standing crystal having at least four sets of bands, wherein each set of bands includes a first sub-band and a second sub-band, the first sub-band having a concentration of at least one impurity selected from H, O, Li, Na, K, F, Cl, Br, and I; and each of the at least four sets of bands have portions that are substantially parallel.

IPC Classes  ?

  • C30B 29/40 - AIIIBV compounds
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

5.

ULTRAPURE MINERALIZER AND IMPROVED METHODS FOR NITRIDE CRYSTAL GROWTH

      
Application Number 18434568
Status Pending
Filing Date 2024-02-06
First Publication Date 2024-07-18
Owner SLT Technologies, Inc. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Von Dollen, Paul M.
  • Gay, Lisa M.
  • Pocius, Douglas W.
  • Cook, Jonathan D.

Abstract

A method for growth of group Ill metal nitride crystals includes providing one or more transfer vessels, a source vessel containing a condensable mineralizer composition, and a receiving vessel, chilling a metallic surface within the one or more transfer vessels, transferring a quantity of the condensable mineralizer composition to the one or more transfer vessels via a vapor phase and causing condensation of the condensable mineralizer composition within the one or more transfer vessels, measuring the quantity of the condensable mineralizer composition within the at least one transfer vessel, transferring at least a portion of the condensable mineralizer composition to the receiving vessel, and forming at least a portion of a group Ill metal nitride boule by an ammonothermal crystal growth process.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds

6.

OXYGEN-DOPED GROUP III METAL NITRIDE AND METHOD OF MANUFACTURE

      
Application Number 18440646
Status Pending
Filing Date 2024-02-13
First Publication Date 2024-06-06
Owner SLT Technologies, Inc. (USA)
Inventor
  • Jiang, Wenkan
  • Ehrentraut, Dirk
  • D'Evelyn, Mark P.

Abstract

A gallium-containing nitride crystals comprising: a top surface having a crystallographic orientation within 5 degrees of a plane selected from a (0001) +c-plane and a (000-1) −c-plane; a substantially wurtzite structure; n-type electronic properties; an impurity concentration of hydrogen >5×1017 cm−3; an impurity concentration of oxygen between 2×1017 cm−3 and 1×1020 cm−3; an [H]/[O] ratio of at least 0.3; an impurity concentration of at least one of Li, Na, K, Rb, Cs, Ca, F, and Cl >1×1016 cm−3; a compensation ratio between 1.0 and 4.0; an absorbance per unit thickness of at least 0.01 cm−1 at wavenumbers of 3175 cm−1, 3164 cm−1, and 3150 cm−1; and wherein, at wavenumbers between 3200 cm−1 and 3400 cm−1 and between 3075 cm−1 and 3125 cm−1, said gallium-containing nitride crystal is essentially free of infrared absorption peaks having an absorbance per unit thickness >10% of the absorbance per unit thickness at 3175 cm−1.

IPC Classes  ?

  • C30B 29/40 - AIIIBV compounds
  • C01B 21/06 - Binary compounds of nitrogen with metals, with silicon, or with boron
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 29/30 - Semiconductor bodies having polished or roughened surface

7.

STRUCTURES FOR COMMUNICATION, MONITORING AND CONTROL OF CORROSIVE PROCESS ENVIRONMENTS AT HIGH PRESSURE AND HIGH TEMPERATURE

      
Application Number 18501951
Status Pending
Filing Date 2023-11-03
First Publication Date 2024-05-16
Owner SLT Technologies, Inc. (USA)
Inventor Von Dollen, Paul M.

Abstract

Embodiments of disclosure include an apparatus for high-temperature crystal growth. The apparatus can include a pressure vessel having a capsule that has an interior surface that defines an internal capsule volume, a fill tube that comprises an outer surface and an inner surface, wherein an interior fill tube volume defined by the inner surface is in fluid communication with the internal capsule volume of the capsule, a sleeve axially surrounding the outer surface of the fill tube, wherein the sleeve is configured to support the outer surface of the fill tube, along the length of the fill tube, during a high-temperature crystal growth process, and a manifold comprising an interior manifold volume that is in fluid communication with the interior fill tube volume of the fill tube.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • B01D 53/22 - Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases or aerosols by diffusion
  • B01D 71/02 - Inorganic material

8.

APPARATUS FOR RETROGRADE SOLVOTHERMAL CRYSTAL GROWTH, METHOD OF MAKING, AND METHOD OF USE

      
Application Number 18505971
Status Pending
Filing Date 2023-11-09
First Publication Date 2024-05-16
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Von Dollen, Paul M.
  • D'Evelyn, Mark P.

Abstract

According to the present disclosure, techniques related to processing of materials for growth of crystals are provided. More particularly, the present disclosure provides apparatus and methods for heating of seed crystals suitable for use in conjunction with a high-pressure vessel for crystal growth of a material having a retrograde solubility in a supercritical fluid, including crystal growth of a group III metal nitride crystal by an ammonobasic or ammonoacidic technique, but there can be others. In other embodiments, the present disclosure provides methods suitable for synthesis of crystalline nitride materials, but it would be recognized that other crystals and materials can also be processed. Such crystals and materials include, but are not limited to, GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic devices, lasers, light emitting diodes, solar cells, photoelectrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, among other devices.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

9.

METAL-BASED THERMAL INSULATION STRUCTURES

      
Application Number 18506790
Status Pending
Filing Date 2023-11-10
First Publication Date 2024-05-16
Owner SLT Technologies, Inc. (USA)
Inventor Von Dollen, Paul M.

Abstract

Embodiments of the disclosure include a thermal insulation structure, comprising a plurality of stacked layers that include a first layer and a second layer. The first layer includes a first surface, a second surface, disposed opposite of the first surface, and a plurality of perforations extending between the first surface and the second surface, wherein the plurality of perforations comprise a first pattern of two or more perforations that form a patterned in a first direction that is parallel to the first surface. The second layer includes a third surface, wherein the third surface is in contact with the second surface of the first layer, a fourth surface, disposed opposite of the third surface, and a plurality of perforations extending between the third surface and the fourth surface, wherein the plurality of perforations comprise a second pattern of two or more perforations that form a pattern in the first direction that is parallel to the third surface.

IPC Classes  ?

  • F16L 59/02 - Shape or form of insulating materials, with or without coverings integral with the insulating materials
  • B32B 3/26 - Layered products essentially comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar form; Layered products essentially having particular features of form characterised by a layer with cavities or internal voids
  • B32B 15/01 - Layered products essentially comprising metal all layers being exclusively metallic
  • B32B 15/02 - Layered products essentially comprising metal in a form other than a sheet, e.g. wire, particles
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

10.

DIRECT HEATING AND TEMPERATURE CONTROL SYSTEM FOR CRYSTAL GROWTH

      
Application Number 18388479
Status Pending
Filing Date 2023-11-09
First Publication Date 2024-05-16
Owner
  • SLT TECHNOLOGIES, INC. (USA)
  • KYOCERA CORPORATION (Japan)
Inventor
  • Von Dollen, Paul M.
  • Miyamoto, Koji

Abstract

Embodiments of the disclosure include a temperature control assembly for performing a crystal growth process. The temperature control assembly will include one or more temperature distribution units (TDUs) coupled to an end cap of a capsule. Each of the one or more TDUs comprise: an interior component comprising a major surface; a heating element disposed over the major surface of the interior component; a via tube comprising a central opening that is configured to accommodate lead wires, wherein the lead wires are configured to electrically connect the heating element to a power supply which is disposed on a side of the end cap that is opposite to the side on which the via tube is disposed; and a sheath layer covering the interior component, the heating element, and the via tube, wherein the sheath layer is hermetically sealed to the end cap and is configured to isolate the interior component, the heating element, and the via tube from an external environment in which the one or more TDUs are disposed during processing.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

11.

METAL-BASED THERMAL INSULATION STRUCTURES

      
Application Number US2023079423
Publication Number 2024/103031
Status In Force
Filing Date 2023-11-10
Publication Date 2024-05-16
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor Von Dollen, Paul, M.

Abstract

Embodiments of the disclosure include a thermal insulation structure, comprising a plurality of stacked layers that include a first layer and a second layer. The first layer includes a first surface, a second surface, disposed opposite of the first surface, and a plurality of perforations extending between the first surface and the second surface, wherein the plurality of perforations comprise a first pattern of two or more perforations that form a patterned in a first direction that is parallel to the first surface. The second layer includes a third surface, wherein the third surface is in contact with the second surface of the first layer, a fourth surface, disposed opposite of the third surface, and a plurality of perforations extending between the third surface and the fourth surface, wherein the plurality of perforations comprise a second pattern of two or more perforations that form a pattern in the first direction that is parallel to the third surface.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 35/00 - Apparatus not otherwise provided for, specially adapted for the growth, production or after-treatment of single crystals or of a homogeneous polycrystalline material with defined structure

12.

DIRECT HEATING AND TEMPERATURE CONTROL SYSTEM FOR CRYSTAL GROWTH

      
Application Number US2023079391
Publication Number 2024/103009
Status In Force
Filing Date 2023-11-10
Publication Date 2024-05-16
Owner
  • SLT TECHNOLOGIES, INC. (USA)
  • KYOCERA CORPORATION (Japan)
Inventor
  • Von Dollen, Paul M.
  • Miyamoto, Koji

Abstract

Embodiments of the disclosure include a temperature control assembly for performing a crystal growth process. The temperature control assembly will include one or more temperature distribution units (TDUs) coupled to an end cap of a capsule. Each of the one or more TDUs comprise: an interior component comprising a major surface; a heating element disposed over the major surface of the interior component; a via tube comprising a central opening that is configured to accommodate lead wires, wherein the lead wires are configured to electrically connect the heating element to a power supply which is disposed on a side of the end cap that is opposite to the side on which the via tube is disposed; and a sheath layer covering the interior component, the heating element, and the via tube, wherein the sheath layer is hermetically sealed to the end cap and is configured to isolate the interior component, the heating element, and the via tube from an external environment in which the one or more TDUs are disposed during processing.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

13.

APPARATUS FOR RETROGRADE SOLVOTHERMAL CRYSTAL GROWTH, METHOD OF MAKING, AND METHOD OF USE

      
Application Number 18505963
Status Pending
Filing Date 2023-11-09
First Publication Date 2024-05-16
Owner SLT Technologies, Inc. (USA)
Inventor
  • Von Dollen, Paul M.
  • Cardwell, Drew W.
  • D'Evelyn, Mark P.
  • Pakalapati, Rajeev Tirumala

Abstract

According to the present disclosure, techniques related to processing of materials for growth of crystals are provided. More particularly, the present disclosure provides apparatus and methods for heating of seed crystals suitable for use in conjunction with a high-pressure vessel for crystal growth of a material having a retrograde solubility in a supercritical fluid, including crystal growth of a group III metal nitride crystal by an ammonobasic or ammonoacidic technique, but there can be others. In other embodiments, the present disclosure provides methods suitable for synthesis of crystalline nitride materials, but it would be recognized that other crystals and materials can also be processed. Such crystals and materials include, but are not limited to, GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic devices, lasers, light emitting diodes, solar cells, photoelectrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, among other devices.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

14.

STRUCTURES FOR COMMUNICATION, MONITORING AND CONTROL OF CORROSIVE PROCESS ENVIRONMENTS AT HIGH PRESSURE AND HIGH TEMPERATURE

      
Application Number US2023078816
Publication Number 2024/102653
Status In Force
Filing Date 2023-11-06
Publication Date 2024-05-16
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor Von Dollen, Paul M.

Abstract

Embodiments of disclosure include an apparatus for high-temperature crystal growth. The apparatus can include a pressure vessel having a capsule that has an interior surface that defines an internal capsule volume, a fill tube that comprises an outer surface and an inner surface, wherein an interior fill tube volume defined by the inner surface is in fluid communication with the internal capsule volume of the capsule, a sleeve axially surrounding the outer surface of the fill tube, wherein the sleeve is configured to support the outer surface of the fill tube, along the length of the fill tube, during a high-temperature crystal growth process, and a manifold comprising an interior manifold volume that is in fluid communication with the interior fill tube volume of the fill tube.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds

15.

APPARATUS FOR RETROGRADE SOLVOTHERMAL CRYSTAL GROWTH, METHOD OF MAKING, AND METHOD OF USE

      
Application Number US2023079417
Publication Number 2024/103027
Status In Force
Filing Date 2023-11-10
Publication Date 2024-05-16
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Cardwell, Drew W.
  • Von Dollen, Paul M.
  • D'Evelyn, Mark P.
  • Pakalapati, Rajeev Tirumala

Abstract

According to the present disclosure, techniques related to processing of materials for growth of crystals are provided. More particularly, the present disclosure provides apparatus and methods for heating of seed crystals suitable for use in conjunction with a high-pressure vessel for crystal growth of a material having a retrograde solubility in a supercritical fluid, including crystal growth of a group III metal nitride crystal by an ammonobasic or ammonoacidic technique, but there can be others. In other embodiments, the present disclosure provides methods suitable for synthesis of crystalline nitride materials, but it would be recognized that other crystals and materials can also be processed. Such crystals and materials include, but are not limited to, GaN, AIN, InN, InGaN, AIGaN, and AllnGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic devices, lasers, light emitting diodes, solar cells, photoelectrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, among other devices.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds

16.

OXYGEN-DOPED GROUP III METAL NITRIDE AND METHOD OF MANUFACTURE

      
Application Number 18542594
Status Pending
Filing Date 2023-12-16
First Publication Date 2024-04-25
Owner SLT Technologies, Inc. (USA)
Inventor
  • Jiang, Wenkan
  • Ehrentraut, Dirk
  • D'Evelyn, Mark P.

Abstract

A gallium-containing nitride crystals are disclosed, comprising: a top surface having a crystallographic orientation within about 5 degrees of a plane selected from a (0001) +c-plane and a (000-1) −c-plane; a substantially wurtzite structure; n-type electronic properties; an impurity concentration of hydrogen greater than about 5×1017 cm−3; an impurity concentration of oxygen between about 2×1017 cm−3 and about 1×1020 cm−3; an [H]/[O] ratio of at least 0.3; an impurity concentration of at least one of Li, Na, K, Rb, Cs, Ca, F, and Cl greater than about 1×1016 cm−3; a compensation ratio between about 1.0 and about 4.0; an absorbance per unit thickness of at least 0.01 cm−1 at wavenumbers of approximately 3175 cm−1, 3164 cm−1, and 3150 cm−1; and wherein, at wavenumbers between about 3200 cm−1 and about 3400 cm−1 and between about 3075 cm−1 and about 3125 cm−1, said gallium-containing nitride crystal is essentially free of infrared absorption peaks having an absorbance per unit thickness greater than 10% of the absorbance per unit thickness at 3175 cm.

IPC Classes  ?

  • C30B 29/40 - AIIIBV compounds
  • C01B 21/06 - Binary compounds of nitrogen with metals, with silicon, or with boron
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 29/30 - Semiconductor bodies having polished or roughened surface

17.

IMPROVED INTERNALLY-HEATED HIGH-PRESSURE APPARATUS FOR SOLVOTHERMAL CRYSTAL GROWTH

      
Application Number US2023070631
Publication Number 2024/020509
Status In Force
Filing Date 2023-07-20
Publication Date 2024-01-25
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Von Dollen, Paul M.

Abstract

Embodiments of the disclosure can include an apparatus for solvothermal crystal growth. The apparatus can include a cylindrical shaped enclosure, a cylindrical heater, a first end closure member, a load-bearing annular insulating member, and a first end plug. The cylindrical heater includes a first end, a second end and a cylindrical wall that extends between the first end and the second end, wherein an interior surface of the cylindrical wall defines a capsule region. The first end closure member is disposed proximate to the first end of the cylindrical heater, the first end closure member being configured to provide axial support for a capsule disposed within the capsule region. The load-bearing annular insulating member is disposed between an inner surface of the cylindrical shaped enclosure and an outer surface of the cylindrical wall of the cylindrical heater. The first end plug is disposed between the first end of the cylindrical heater and the first end closure. The load-bearing annular insulating member or the first end plug comprises a packed-bed ceramic composition, the packed-bed ceramic composition being characterized by a density that is between about 30% and about 98% of a theoretical density of a 100%-dense ceramic having the same composition.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

18.

INTERNALLY-HEATED HIGH-PRESSURE APPARATUS FOR SOLVOTHERMAL CRYSTAL GROWTH

      
Application Number 18355676
Status Pending
Filing Date 2023-07-20
First Publication Date 2024-01-25
Owner SLT Technologies, Inc. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Von Dollen, Paul M.

Abstract

Embodiments of the disclosure can include an apparatus for solvothermal crystal growth. The apparatus can include a cylindrical shaped enclosure, a cylindrical heater, a first end closure member, a load-bearing annular insulating member, and a first end plug. The cylindrical heater includes a first end, a second end and a cylindrical wall that extends between the first end and the second end, wherein an interior surface of the cylindrical wall defines a capsule region. The first end closure member is disposed proximate to the first end of the cylindrical heater, the first end closure member being configured to provide axial support for a capsule disposed within the capsule region. The load-bearing annular insulating member is disposed between an inner surface of the cylindrical shaped enclosure and an outer surface of the cylindrical wall of the cylindrical heater. The first end plug is disposed between the first end of the cylindrical heater and the first end closure. The load-bearing annular insulating member or the first end plug comprises a packed-bed ceramic composition, the packed-bed ceramic composition being characterized by a density that is between about 30% and about 98% of a theoretical density of a 100%-dense ceramic having the same composition.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 35/00 - Apparatus not otherwise provided for, specially adapted for the growth, production or after-treatment of single crystals or of a homogeneous polycrystalline material with defined structure

19.

COMPOUND INTERNALLY-HEATED HIGH-PRESSURE APPARATUS FOR SOLVOTHERMAL CRYSTAL GROWTH

      
Application Number 18356127
Status Pending
Filing Date 2023-07-20
First Publication Date 2024-01-25
Owner SLT Technologies, Inc. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Von Dollen, Paul M.

Abstract

Embodiments of the disclosure include a crystal growth apparatus, comprising a cylindrical-shaped enclosure, a primary liner disposed within the cylindrical-shaped enclosure, wherein the primary liner comprises a cylindrical wall that extends between a first end and a second end, and an interior surface of the primary liner defines an interior region, at least one load-bearing annular insulating member disposed between the cylindrical-shaped enclosure and the primary liner, a plurality of heating elements disposed between the primary liner and the at least one load-bearing annular insulating member, at least one end closure member disposed proximate to a first end of the cylindrical-shaped enclosure, and a primary liner lid disposed proximate to the first end of the cylindrical wall of the primary liner. The at least one load-bearing annular insulating member comprising at least one of a packed-bed ceramic composition, the packed-bed ceramic composition having a density that is between about 30% and about 98% of a theoretical density of a 100%-dense ceramic having the same composition, or a perforated metal member, comprising a perforated metal foil or a plurality of perforated metal plates, wherein the perforations have a percent open area between about 25% and about 90%, and the perforations have a diameter between about 1 millimeter and about 25 millimeters.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

20.

COMPOUND INTERNALLY-HEATED HIGH-PRESSURE APPARATUS FOR SOLVOTHERMAL CRYSTAL GROWTH

      
Application Number US2023070635
Publication Number 2024/020513
Status In Force
Filing Date 2023-07-20
Publication Date 2024-01-25
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Von Dollen, Paul M.

Abstract

Embodiments of the disclosure include a crystal growth apparatus, comprising a cylindrical-shaped enclosure, a primary liner disposed within the cylindrical-shaped enclosure, wherein the primary liner comprises a cylindrical wall that extends between a first end and a second end, and an interior surface of the primary liner defines an interior region, at least one load-bearing annular insulating member disposed between the cylindrical-shaped enclosure and the primary liner, a plurality of heating elements disposed between the primary liner and the at least one load-bearing annular insulating member, at least one end closure member disposed proximate to a first end of the cylindrical-shaped enclosure, and a primary liner lid disposed proximate to the first end of the cylindrical wall of the primary liner. The at least one load-bearing annular insulating member comprising at least one of a packed-bed ceramic composition, the packed-bed ceramic composition having a density that is between about 30% and about 98% of a theoretical density of a 100%-dense ceramic having the same composition, or a perforated metal member, comprising a perforated metal foil or a plurality of perforated metal plates, wherein the perforations have a percent open area between about 25% and about 90%, and the perforations have a diameter between about 1 millimeter and about 25 millimeters.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

21.

PHOTODIODE WITH HIGH POWER CONVERSION EFFICIENCY AND POSITIVE TEMPERATURE COEFFICIENT

      
Application Number US2023069206
Publication Number 2024/006787
Status In Force
Filing Date 2023-06-27
Publication Date 2024-01-04
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Sayed, Islam
  • Oh, Sang Ho
  • Young, Nathan
  • Cardwell, Drew, W.
  • D'Evelyn, Mark, P.

Abstract

According to the present disclosure, techniques related to manufacturing and applications of power photodiode structures and devices based on group-III metal nitride and gallium-based substrates are provided. More specifically, embodiments of the disclosure include techniques for fabricating photodiode devices comprising one or more of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, structures and devices. Such structures or devices can be used for a variety of applications including optoelectronic devices, photodiodes, power-over-fiber receivers, and others.

IPC Classes  ?

  • H01L 31/105 - Devices sensitive to infrared, visible or ultraviolet radiation characterised by only one potential barrier or surface barrier the potential barrier being of the PIN type
  • H01L 31/0352 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their shape or by the shapes, relative sizes or disposition of the semiconductor regions
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds

22.

PHOTODIODE WITH HIGH POWER CONVERSION EFFICIENCY AND POSITIVE TEMPERATURE COEFFICIENT

      
Application Number 18342617
Status Pending
Filing Date 2023-06-27
First Publication Date 2023-12-28
Owner SLT Technologies, Inc. (USA)
Inventor
  • Sayed, Islam
  • Oh, Sang Ho
  • Young, Nathan
  • Cardwell, Drew W.
  • D'Evelyn, Mark P.

Abstract

According to the present disclosure, techniques related to manufacturing and applications of power photodiode structures and devices based on group-III metal nitride and gallium-based substrates are provided. More specifically, embodiments of the disclosure include techniques for fabricating photodiode devices comprising one or more of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, structures and devices. Such structures or devices can be used for a variety of applications including optoelectronic devices, photodiodes, power-over-fiber receivers, and others.

IPC Classes  ?

  • H01L 31/0352 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their shape or by the shapes, relative sizes or disposition of the semiconductor regions
  • H01L 31/0224 - Electrodes
  • H01L 31/0232 - Optical elements or arrangements associated with the device
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 31/0236 - Special surface textures
  • H01L 31/109 - Devices sensitive to infrared, visible or ultraviolet radiation characterised by only one potential barrier or surface barrier the potential barrier being of the PN heterojunction type
  • H01L 31/18 - Processes or apparatus specially adapted for the manufacture or treatment of these devices or of parts thereof

23.

LARGE AREA GROUP III NITRIDE CRYSTALS AND SUBSTRATES, METHODS OF MAKING, AND METHODS OF USE

      
Application Number 18338280
Status Pending
Filing Date 2023-06-20
First Publication Date 2023-10-26
Owner SLT Technologies, Inc. (USA)
Inventor
  • Ehrentraut, Dirk
  • D'Evelyn, Mark P.
  • Cardwell, Drew W.

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-III metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for growing large area substrates using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

  • C30B 29/60 - Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape characterised by shape
  • C30B 29/40 - AIIIBV compounds
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

24.

ALUMINUM-CONTAINING NITRIDE CERAMIC MATRIX COMPOSITE, METHOD OF MAKING, AND METHOD OF USE

      
Application Number US2022077922
Publication Number 2023/200492
Status In Force
Filing Date 2022-10-11
Publication Date 2023-10-19
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark, P.
  • Italiano, David, N.

Abstract

Embodiments of disclosure may provide a method for forming an aluminum-containing nitride ceramic matrix composite, comprising heating a green body, an aluminum-containing composition, ammonia and a mineralizer composition in a sealable container to a temperature between about 400 degrees Celsius and about 800 degrees Celsius and a pressure between about 10 MPa and about 1000 MPa, to form an aluminum-containing nitride ceramic matrix composite characterized by a phosphor-to-aluminum nitride (AIN) ratio, by volume, between about 1 % and about 99%, by a porosity between about 1% and about 50%, and by a thermal conductivity between about 1 watt per meter-Kelvin and about 320 watts per meter-Kelvin. The green body comprises a phosphor powder comprising at least one phosphor composition, wherein the phosphor powder particles are characterized by a D50 diameter between about 100 nanometers and about 500 micrometers, and the green body has a porosity between about 10% and about 80%. The aluminum-containing composition has a purity, on a metals basis, between about 90% and about 99.9999%. The fraction of free volume within the sealable container contains between about 10% and about 95% of liquid ammonia prior to heating the green body, the aluminum-containing composition, ammonia and the mineralizer composition in the sealable container.

IPC Classes  ?

  • C04B 35/581 - Shaped ceramic products characterised by their composition; Ceramic compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxides based on borides, nitrides or silicides based on aluminium nitride
  • C04B 38/00 - Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
  • C09K 11/77 - Luminescent, e.g. electroluminescent, chemiluminescent, materials containing inorganic luminescent materials containing rare earth metals

25.

GROUP III NITRIDE SUBSTRATE, METHOD OF MAKING, AND METHOD OF USE

      
Application Number 18331719
Status Pending
Filing Date 2023-06-08
First Publication Date 2023-10-05
Owner SLT Technologies, Inc. (USA)
Inventor
  • Jiang, Wenkan
  • D'Evelyn, Mark P.
  • Kamber, Derrick S.
  • Ehrentraut, Dirk
  • Cook, Jonathan D.
  • Wenger, James

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-III metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for growing large area substrates using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 33/10 - Etching in solutions or melts
  • C30B 7/00 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
  • C30B 29/40 - AIIIBV compounds

26.

Reusable nitride wafer, method of making, and use thereof

      
Application Number 17013487
Grant Number RE049677
Status In Force
Filing Date 2020-09-04
First Publication Date 2023-10-03
Grant Date 2023-10-03
Owner SLT Technologies, Inc (USA)
Inventor
  • D'Evelyn, Mark P.
  • Krames, Michael Ragan

Abstract

Techniques for processing materials for manufacture of gallium-containing nitride substrates are disclosed. More specifically, techniques for fabricating and reusing large area substrates using a combination of processing techniques are disclosed. The methods can be applied to fabricating substrates of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others. Such substrates can be used for a variety of applications including optoelectronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photo detectors, integrated circuits, transistors, and others.

IPC Classes  ?

  • C30B 25/18 - Epitaxial-layer growth characterised by the substrate
  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • C30B 23/02 - Epitaxial-layer growth
  • C30B 29/40 - AIIIBV compounds
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • H01L 21/78 - Manufacture or treatment of devices consisting of a plurality of solid state components or integrated circuits formed in, or on, a common substrate with subsequent division of the substrate into plural individual devices
  • H01L 29/04 - Semiconductor bodies characterised by their crystalline structure, e.g. polycrystalline, cubic or particular orientation of crystalline planes
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 29/36 - Semiconductor bodies characterised by the concentration or distribution of impurities
  • H01L 31/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 31/18 - Processes or apparatus specially adapted for the manufacture or treatment of these devices or of parts thereof
  • H01L 33/32 - Materials of the light emitting region containing only elements of group III and group V of the periodic system containing nitrogen
  • H01S 5/30 - Structure or shape of the active region; Materials used for the active region

27.

GROUP III NITRIDE SUBSTRATE AND METHOD OF MAKING

      
Application Number 18122989
Status Pending
Filing Date 2023-03-17
First Publication Date 2023-09-21
Owner SLT Technologies, Inc. (USA)
Inventor
  • Fukutomi, Keiji
  • Jiang, Wenkan
  • Tamaki, Motoi
  • D'Evelyn, Mark P.

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-III metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for growing large area substrates using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

  • C30B 29/40 - AIIIBV compounds
  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

28.

GROUP III NITRIDE SUBSTRATE AND METHOD OF MAKING

      
Application Number US2023064651
Publication Number 2023/178322
Status In Force
Filing Date 2023-03-17
Publication Date 2023-09-21
Owner
  • SLT TECHNOLOGIES, INC. (USA)
  • KYOCERA CORPORATION (Japan)
Inventor
  • Fukutomi, Keiji
  • Jiang, Wenkan
  • Tamaki, Motoi
  • D'Evelyn, Mark P.

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-III metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for growing large area substrates using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • C30B 29/40 - AIIIBV compounds

29.

GROUP III NITRIDE SUBSTRATE WITH OXYGEN GRADIENT, METHOD OF MAKING, AND METHOD OF USE

      
Application Number US2022080713
Publication Number 2023/102456
Status In Force
Filing Date 2022-11-30
Publication Date 2023-06-08
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Fukutomi, Keiji
  • Cardwell, Drew W.
  • Italiano, David N.
  • Domoto, Chiaki

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-III metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for substrates with a controlled oxygen gradient using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof

30.

GROUP III NITRIDE SUBSTRATE WITH OXYGEN GRADIENT, METHOD OF MAKING, AND METHOD OF USE

      
Application Number 18072680
Status Pending
Filing Date 2022-11-30
First Publication Date 2023-06-01
Owner SLT Technologies, Inc. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Fukutomi, Keiji
  • Cardwell, Drew W.
  • Italiano, David N.

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-III metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for substrates with a controlled oxygen gradient using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof

31.

GROUP III NITRIDE SUBSTRATE WITH OXYGEN GRADIENT, METHOD OF MAKING, AND METHOD OF USE

      
Application Number 18072684
Status Pending
Filing Date 2022-11-30
First Publication Date 2023-06-01
Owner SLT Technologies, Inc. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Fukutomi, Keiji
  • Cardwell, Drew W.
  • Italiano, David N.
  • Domoto, Chiaki

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-III metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for substrates with a controlled oxygen gradient using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

32.

IMPROVED HEATER FOR RETROGRADE SOLVOTHERMAL CRYSTAL GROWTH, METHOD OF MAKING, AND METHOD OF USE

      
Application Number US2022077867
Publication Number 2023/064737
Status In Force
Filing Date 2022-10-10
Publication Date 2023-04-20
Owner
  • SLT TECHNOLOGIES, INC. (USA)
  • KYOCERA CORPORATION (Japan)
Inventor
  • D'Evelyn, Mark P.
  • Von Dollen, Paul M.
  • Pakalapati, Rajeev Timala
  • Fukutomi, Keiji
  • Monzen, Maimi
  • Miyamoto, Koji
  • Tamaki, Motoi

Abstract

Embodiments of the disclosure an apparatus for solvothermal crystal growth, comprising: a pressure vessel having a cylindrical shape and a vertical orientation; a cylindrical heater having an upper zone and a lower zone that can be independently controlled; at least one end heater; and an inward-facing surface of a baffle placed within 100 millimeters of a bottom end or top end surface of the growth chamber. The end heater is configured to enable: a variation in the temperature distribution along a first surface to be less than about 10 °C, and a variation in the temperature distribution along a second surface to be less than about 20 °C, during a crystal growth process. The first surface has a cylindrical shape and is positioned within the pressure vessel, and the second surface comprises an inner diameter of the growth chamber, and the temperature distribution along the second surface is created within an axial distance of at least 100 millimeters of an end of the growth chamber proximate to the first surface.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds

33.

Aluminum-containing nitride ceramic matrix composite, method of making, and method of use

      
Application Number 17963910
Grant Number 12168632
Status In Force
Filing Date 2022-10-11
First Publication Date 2023-04-13
Grant Date 2024-12-17
Owner SLT Technologies, Inc. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Italiano, David N.

Abstract

Embodiments of disclosure may provide a method for forming an aluminum-containing nitride ceramic matrix composite, comprising heating a green body, an aluminum-containing composition, ammonia and a mineralizer composition in a sealable container to a temperature between about 400 degrees Celsius and about 800 degrees Celsius and a pressure between about 10 MPa and about 1000 MPa, to form an aluminum-containing nitride ceramic matrix composite characterized by a phosphor-to-aluminum nitride (AlN) ratio, by volume, between about 1% and about 99%, by a porosity between about 1% and about 50%, and by a thermal conductivity between about 1 watt per meter-Kelvin and about 320 watts per meter-Kelvin. The green body comprises a phosphor powder comprising at least one phosphor composition, wherein the phosphor powder particles are characterized by a D50 diameter between about 100 nanometers and about 500 micrometers, and the green body has a porosity between about 10% and about 80%. The aluminum-containing composition has a purity, on a metals basis, between about 90% and about 99.9999%. The fraction of free volume within the sealable container contains between about 10% and about 95% of liquid ammonia prior to heating the green body, the aluminum-containing composition, ammonia and the mineralizer composition in the sealable container.

IPC Classes  ?

  • C04B 35/581 - Shaped ceramic products characterised by their composition; Ceramic compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxides based on borides, nitrides or silicides based on aluminium nitride
  • C04B 35/626 - Preparing or treating the powders individually or as batches
  • C04B 35/645 - Pressure sintering
  • C04B 35/65 - Reaction sintering of free metal- or free silicon-containing compositions
  • C09K 11/02 - Use of particular materials as binders, particle coatings or suspension media therefor
  • C09K 11/77 - Luminescent, e.g. electroluminescent, chemiluminescent, materials containing inorganic luminescent materials containing rare earth metals
  • B28B 1/30 - Producing shaped articles from the material by applying the material on to a core, or other moulding surface to form a layer thereon
  • B28B 3/02 - Producing shaped articles from the material by using presses; Presses specially adapted therefor wherein a ram exerts pressure on the material in a moulding space; Ram heads of special form

34.

HEATER FOR RETROGRADE SOLVOTHERMAL CRYSTAL GROWTH, METHOD OF MAKING, AND METHOD OF USE

      
Application Number 17963004
Status Pending
Filing Date 2022-10-10
First Publication Date 2023-04-13
Owner
  • SLT Technologies, Inc. (USA)
  • Kyocera Corporation (Japan)
Inventor
  • D'Evelyn, Mark P.
  • Von Dollen, Paul M.
  • Pakalapati, Rajeev Tirumala
  • Fukutomi, Keiji
  • Monzen, Maimi
  • Miyamoto, Koji
  • Tamaki, Motoi

Abstract

Embodiments of the disclosure an apparatus for solvothermal crystal growth, comprising: a pressure vessel having a cylindrical shape and a vertical orientation; a cylindrical heater having an upper zone and a lower zone that can be independently controlled; at least one end heater; and an inward-facing surface of a baffle placed within 100 millimeters of a bottom end or top end surface of the growth chamber. The end heater is configured to enable: a variation in the temperature distribution along a first surface to be less than about 10° C., and a variation in the temperature distribution along a second surface to be less than about 20° C., during a crystal growth process. The first surface has a cylindrical shape and is positioned within the pressure vessel, and the second surface comprises an inner diameter of the growth chamber, and the temperature distribution along the second surface is created within an axial distance of at least 100 millimeters of an end of the growth chamber proximate to the first surface.

IPC Classes  ?

  • C30B 35/00 - Apparatus not otherwise provided for, specially adapted for the growth, production or after-treatment of single crystals or of a homogeneous polycrystalline material with defined structure
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

35.

Power photodiode structures and devices

      
Application Number 18059293
Grant Number 12040417
Status In Force
Filing Date 2022-11-28
First Publication Date 2023-04-06
Grant Date 2024-07-16
Owner SLT Technologies, Inc. (USA)
Inventor
  • Cardwell, Drew W.
  • D'Evelyn, Mark P.

Abstract

According to the present disclosure, techniques related to manufacturing and applications of power photodiode structures and devices based on group-III metal nitride and gallium-based substrates are provided. More specifically, embodiments of the disclosure include techniques for fabricating photodiode devices comprising one or more of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, structures and devices. Such structures or devices can be used for a variety of applications including optoelectronic devices, photodiodes, power-over-fiber receivers, and others.

IPC Classes  ?

  • H01L 31/0232 - Optical elements or arrangements associated with the device
  • G02B 6/42 - Coupling light guides with opto-electronic elements
  • H01L 31/0216 - Coatings
  • H01L 31/0224 - Electrodes
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 31/0352 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their shape or by the shapes, relative sizes or disposition of the semiconductor regions
  • H01L 31/036 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their crystalline structure or particular orientation of the crystalline planes
  • H01L 31/109 - Devices sensitive to infrared, visible or ultraviolet radiation characterised by only one potential barrier or surface barrier the potential barrier being of the PN heterojunction type
  • H01L 31/18 - Processes or apparatus specially adapted for the manufacture or treatment of these devices or of parts thereof

36.

Methods for coupling of optical fibers to a power photodiode

      
Application Number 18059307
Grant Number 12027635
Status In Force
Filing Date 2022-11-28
First Publication Date 2023-04-06
Grant Date 2024-07-02
Owner SLT Technologies, Inc. (USA)
Inventor
  • Cardwell, Drew W.
  • D'Evelyn, Mark P.

Abstract

According to the present disclosure, techniques related to manufacturing and applications of power photodiode structures and devices based on group-III metal nitride and gallium-based substrates are provided. More specifically, embodiments of the disclosure include techniques for fabricating photodiode devices comprising one or more of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, structures and devices. Such structures or devices can be used for a variety of applications including optoelectronic devices, photodiodes, power-over-fiber receivers, and others.

IPC Classes  ?

  • H01L 31/0232 - Optical elements or arrangements associated with the device
  • G01J 1/04 - Optical or mechanical part
  • G01J 1/44 - Electric circuits
  • H01L 31/109 - Devices sensitive to infrared, visible or ultraviolet radiation characterised by only one potential barrier or surface barrier the potential barrier being of the PN heterojunction type

37.

POWER PHOTODIODE STRUCTURES, METHODS OF MAKING, AND METHODS OF USE

      
Application Number 17893048
Status Pending
Filing Date 2022-08-22
First Publication Date 2022-12-22
Owner SLT Technologies, Inc. (USA)
Inventor
  • Cardwell, Drew W.
  • D'Evelyn, Mark P.

Abstract

According to the present disclosure, techniques related to manufacturing and applications of power photodiode structures and devices based on group-III metal nitride and gallium-based substrates are provided. More specifically, embodiments of the disclosure include techniques for fabricating photodiode devices comprising one or more of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, structures and devices. Such structures or devices can be used for a variety of applications including optoelectronic devices, photodiodes, power-over-fiber receivers, and others.

IPC Classes  ?

  • H01L 31/109 - Devices sensitive to infrared, visible or ultraviolet radiation characterised by only one potential barrier or surface barrier the potential barrier being of the PN heterojunction type
  • H01L 31/0232 - Optical elements or arrangements associated with the device
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 31/0352 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their shape or by the shapes, relative sizes or disposition of the semiconductor regions
  • H01L 31/18 - Processes or apparatus specially adapted for the manufacture or treatment of these devices or of parts thereof

38.

Ultrapure mineralizer and improved methods for nitride crystal growth

      
Application Number 17514656
Grant Number 12024795
Status In Force
Filing Date 2021-10-29
First Publication Date 2022-05-05
Grant Date 2024-07-02
Owner SLT Technologies, Inc. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Von Dollen, Paul M.
  • Gay, Lisa M.
  • Pocius, Douglas W.
  • Cook, Jonathan D.

Abstract

A method for growth of group III metal nitride crystals includes providing a manifold comprising including one or more transfer vessels, a source vessel containing a condensable mineralizer composition, and a receiving vessel, chilling a metallic surface within the one or more transfer vessels, the metallic surface comprising a composition that does not form a reaction product when exposed to the condensable mineralizer composition, transferring a quantity of the condensable mineralizer composition to the one or more transfer vessels via a vapor phase and causing condensation of the condensable mineralizer composition within the one or more transfer vessels, measuring the quantity of the condensable mineralizer composition within the at least one transfer vessel, transferring at least a portion of the condensable mineralizer composition to the receiving vessel, and forming at least a portion of a group III metal nitride boule by an ammonothermal crystal growth process that comprises exposing a seed crystal to a temperature of at least about 400 degrees Celsius, and exposing the seed crystal to a mineralizer that is formed from the condensable mineralizer composition transferred from the receiving vessel.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds

39.

POWER PHOTODIODE, METHODS FOR COUPLING OF OPTICAL FIBERS TO A POWER PHOTODIODE, AND POWER-OVER-FIBER SYSTEM BACKGROUND

      
Application Number US2021013760
Publication Number 2021/167724
Status In Force
Filing Date 2021-01-15
Publication Date 2021-08-26
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Cardwell, Drew W.
  • D'Evelyn, Mark P.

Abstract

According to the present disclosure, techniques related to manufacturing and applications of power photodiode structures and devices based on group-Ill metal nitride and gallium-based substrates are provided. More specifically, embodiments of the disclosure include techniques for fabricating photodiode devices comprising one or more of GaN, AIN, InN, InGaN, AIGaN, and AllnGaN, structures and devices. Such structures or devices can be used for a variety of applications including optoelectronic devices, photodiodes, power-over-fiber receivers, and others.

IPC Classes  ?

  • H01L 31/0232 - Optical elements or arrangements associated with the device
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 31/036 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their crystalline structure or particular orientation of the crystalline planes
  • H01L 31/054 - Optical elements directly associated or integrated with the PV cell, e.g. light-reflecting means or light-concentrating means
  • H01L 31/0693 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof adapted as photovoltaic [PV] conversion devices characterised by at least one potential-jump barrier or surface barrier the potential barriers being only of the PN homojunction type, e.g. bulk silicon PN homojunction solar cells or thin film polycrystalline silicon PN homojunction solar cells the devices including, apart from doping material or other impurities, only AIIIBV compounds, e.g. GaAs or InP solar cells
  • H01L 31/105 - Devices sensitive to infrared, visible or ultraviolet radiation characterised by only one potential barrier or surface barrier the potential barrier being of the PIN type
  • G02B 6/10 - Light guides; Structural details of arrangements comprising light guides and other optical elements, e.g. couplings of the optical waveguide type

40.

IMPROVED GROUP III NITRIDE SUBSTRATE, METHOD OF MAKING, AND METHOD OF USE

      
Application Number US2020034405
Publication Number 2021/162727
Status In Force
Filing Date 2020-05-22
Publication Date 2021-08-19
Owner SLT TECHNOLOGIES, INC (USA)
Inventor
  • Jiang, Wenkan
  • D'Evelyn, Mark, P.
  • Kamber, Derrick, S.
  • Ehrentraut, Dirk
  • Cook, Jonathan, D.
  • Wenger, James

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-ill metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for growing large area substrates using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AIN, InN, InGaN, AIGaN, and AllnGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof

41.

LARGE AREA GROUP III NITRIDE CRYSTALS AND SUBSTRATES, METHODS OF MAKING, AND METHODS OF USE

      
Application Number US2021017514
Publication Number 2021/163230
Status In Force
Filing Date 2021-02-10
Publication Date 2021-08-19
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Cardwell, Drew
  • D'Evelyn, Mark P.

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-ill metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for growing large area substrates using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • C30B 29/38 - Nitrides
  • C30B 29/40 - AIIIBV compounds
  • H01L 29/04 - Semiconductor bodies characterised by their crystalline structure, e.g. polycrystalline, cubic or particular orientation of crystalline planes
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds

42.

Large area group III nitride crystals and substrates, methods of making, and methods of use

      
Application Number 17173169
Grant Number 11721549
Status In Force
Filing Date 2021-02-10
First Publication Date 2021-08-12
Grant Date 2023-08-08
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Jiang, Wenkan
  • Cardwell, Drew W.
  • Ehrentraut, Dirk

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-III metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for growing large area substrates using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 29/36 - Semiconductor bodies characterised by the concentration or distribution of impurities
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof

43.

Group III nitride substrate, method of making, and method of use

      
Application Number 16882219
Grant Number 11705322
Status In Force
Filing Date 2020-05-22
First Publication Date 2021-08-12
Grant Date 2023-07-18
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Jiang, Wenkan
  • D'Evelyn, Mark P.
  • Kamber, Derrick S.
  • Ehrentraut, Dirk
  • Cook, Jonathan D.
  • Wenger, James

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-III metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for growing large area substrates using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 7/00 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
  • C30B 29/40 - AIIIBV compounds
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • C30B 33/10 - Etching in solutions or melts
  • H01L 29/778 - Field-effect transistors with two-dimensional charge carrier gas channel, e.g. HEMT
  • H01L 33/32 - Materials of the light emitting region containing only elements of group III and group V of the periodic system containing nitrogen

44.

Large area group III nitride crystals and substrates, methods of making, and methods of use

      
Application Number 17173170
Grant Number 12091771
Status In Force
Filing Date 2021-02-10
First Publication Date 2021-08-12
Grant Date 2024-09-17
Owner SLT Technologies, Inc. (USA)
Inventor
  • Cardwell, Drew W.
  • D'Evelyn, Mark P.

Abstract

Embodiments of the present disclosure include techniques related to techniques for processing materials for manufacture of group-III metal nitride and gallium based substrates. More specifically, embodiments of the disclosure include techniques for growing large area substrates using a combination of processing techniques. Merely by way of example, the disclosure can be applied to growing crystals of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others for manufacture of bulk or patterned substrates. Such bulk or patterned substrates can be used for a variety of applications including optoelectronic and electronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photodetectors, integrated circuits, and transistors, and others.

IPC Classes  ?

  • C30B 29/40 - AIIIBV compounds
  • C01B 21/06 - Binary compounds of nitrogen with metals, with silicon, or with boron
  • C30B 25/04 - Pattern deposit, e.g. by using masks
  • C30B 25/18 - Epitaxial-layer growth characterised by the substrate

45.

High quality group-III metal nitride seed crystal and method of making

      
Application Number 17133002
Grant Number 11661670
Status In Force
Filing Date 2020-12-23
First Publication Date 2021-07-22
Grant Date 2023-05-30
Owner SLT Technologies, Inc (USA)
Inventor
  • D'Evelyn, Mark P.
  • Cardwell, Drew W.
  • Cook, Jonathan D.

Abstract

High quality ammonothermal group III metal nitride crystals having a pattern of locally-approximately-linear arrays of threading dislocations, methods of manufacturing high quality ammonothermal group III metal nitride crystals, and methods of using such crystals are disclosed. The crystals are useful for seed bulk crystal growth and as substrates for light emitting diodes, laser diodes, transistors, photodetectors, solar cells, and for photoelectrochemical water splitting for hydrogen generation devices.

IPC Classes  ?

  • C30B 28/04 - Production of homogeneous polycrystalline material with defined structure from liquids
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds

46.

HIGH-QUALITY GROUP-III METAL NITRIDE SEED CRYSTAL AND METHOD OF MAKING

      
Application Number US2020066900
Publication Number 2021/146042
Status In Force
Filing Date 2020-12-23
Publication Date 2021-07-22
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Cardwell, Drew W.
  • Cook, Jonathan D.

Abstract

High quality ammonothermal group III metal nitride crystals having a pattern of locally-approximately-linear arrays of threading dislocations, methods of manufacturing high quality ammonothermal group III metal nitride crystals, and methods of using such crystals are disclosed. The crystals are useful for seed bulk crystal growth and as substrates for light emitting diodes, laser diodes, transistors, photodetectors, solar cells, and for photoelectrochemical water splitting for hydrogen generation devices.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds
  • C30B 33/00 - After-treatment of single crystals or homogeneous polycrystalline material with defined structure
  • C30B 33/06 - Joining of crystals
  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • C30B 25/04 - Pattern deposit, e.g. by using masks

47.

Power photodiode structures and devices

      
Application Number 17151109
Grant Number 11569398
Status In Force
Filing Date 2021-01-15
First Publication Date 2021-06-03
Grant Date 2023-01-31
Owner SLT Technologies, Inc (USA)
Inventor
  • Cardwell, Drew W.
  • D'Evelyn, Mark P.

Abstract

According to the present disclosure, techniques related to manufacturing and applications of power photodiode structures and devices based on group-III metal nitride and gallium-based substrates are provided. More specifically, embodiments of the disclosure include techniques for fabricating photodiode devices comprising one or more of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, structures and devices. Such structures or devices can be used for a variety of applications including optoelectronic devices, photodiodes, power-over-fiber receivers, and others.

IPC Classes  ?

  • H01L 31/0232 - Optical elements or arrangements associated with the device
  • H01L 31/0216 - Coatings
  • H01L 31/0224 - Electrodes
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds
  • G02B 6/42 - Coupling light guides with opto-electronic elements
  • H01L 31/036 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their crystalline structure or particular orientation of the crystalline planes
  • H01L 31/109 - Devices sensitive to infrared, visible or ultraviolet radiation characterised by only one potential barrier or surface barrier the potential barrier being of the PN heterojunction type
  • H01L 31/18 - Processes or apparatus specially adapted for the manufacture or treatment of these devices or of parts thereof
  • H01L 31/0352 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their shape or by the shapes, relative sizes or disposition of the semiconductor regions

48.

Methods for coupling of optical fibers to a power photodiode

      
Application Number 17151110
Grant Number 11575055
Status In Force
Filing Date 2021-01-15
First Publication Date 2021-06-03
Grant Date 2023-02-07
Owner SLT Technologies, Inc (USA)
Inventor
  • Cardwell, Drew W.
  • D'Evelyn, Mark P.

Abstract

According to the present disclosure, techniques related to manufacturing and applications of power photodiode structures and devices based on group-III metal nitride and gallium-based substrates are provided. More specifically, embodiments of the disclosure include techniques for fabricating photodiode devices comprising one or more of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, structures and devices. Such structures or devices can be used for a variety of applications including optoelectronic devices, photodiodes, power-over-fiber receivers, and others.

IPC Classes  ?

  • H01L 31/0232 - Optical elements or arrangements associated with the device
  • H01L 31/109 - Devices sensitive to infrared, visible or ultraviolet radiation characterised by only one potential barrier or surface barrier the potential barrier being of the PN heterojunction type
  • G01J 1/44 - Electric circuits
  • G01J 1/04 - Optical or mechanical part

49.

Power photodiode structures, methods of making, and methods of use

      
Application Number 16930250
Grant Number 11444216
Status In Force
Filing Date 2020-07-15
First Publication Date 2021-01-21
Grant Date 2022-09-13
Owner SLT Technologies, Inc. (USA)
Inventor
  • Cardwell, Drew W.
  • D'Evelyn, Mark P.

Abstract

According to the present disclosure, techniques related to manufacturing and applications of power photodiode structures and devices based on group-III metal nitride and gallium-based substrates are provided. More specifically, embodiments of the disclosure include techniques for fabricating photodiode devices comprising one or more of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, structures and devices. Such structures or devices can be used for a variety of applications including optoelectronic devices, photodiodes, power-over-fiber receivers, and others.

IPC Classes  ?

  • H01L 31/036 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their crystalline structure or particular orientation of the crystalline planes
  • H01L 31/0224 - Electrodes
  • H01L 31/0232 - Optical elements or arrangements associated with the device
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 31/105 - Devices sensitive to infrared, visible or ultraviolet radiation characterised by only one potential barrier or surface barrier the potential barrier being of the PIN type
  • H01L 31/18 - Processes or apparatus specially adapted for the manufacture or treatment of these devices or of parts thereof

50.

POWER PHOTODIODE STRUCTURES, METHODS OF MAKING, AND METHODS OF USE

      
Application Number US2020042205
Publication Number 2021/011705
Status In Force
Filing Date 2020-07-15
Publication Date 2021-01-21
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Cardwell, Drew, W.
  • D'Evelyn, Mark, P.

Abstract

According to the present disclosure, techniques related to manufacturing and applications of power photodiode structures and devices based on group-ill metal nitride and gallium-based substrates are provided. More specifically, embodiments of the disclosure include techniques for fabricating photodiode devices comprising one or more of GaN, AIN, InN, InGaN, AIGaN, and AllnGaN, structures and devices. Such structures or devices can be used for a variety of applications including optoelectronic devices, photodiodes, power-over-fiber receivers, and others.

IPC Classes  ?

  • H01L 31/0232 - Optical elements or arrangements associated with the device
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 31/036 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their crystalline structure or particular orientation of the crystalline planes
  • H01L 31/054 - Optical elements directly associated or integrated with the PV cell, e.g. light-reflecting means or light-concentrating means
  • H01L 31/0693 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof adapted as photovoltaic [PV] conversion devices characterised by at least one potential-jump barrier or surface barrier the potential barriers being only of the PN homojunction type, e.g. bulk silicon PN homojunction solar cells or thin film polycrystalline silicon PN homojunction solar cells the devices including, apart from doping material or other impurities, only AIIIBV compounds, e.g. GaAs or InP solar cells
  • H01L 31/105 - Devices sensitive to infrared, visible or ultraviolet radiation characterised by only one potential barrier or surface barrier the potential barrier being of the PIN type

51.

Method and system for preparing polycrystalline group III metal nitride

      
Application Number 16814813
Grant Number 11047041
Status In Force
Filing Date 2020-03-10
First Publication Date 2020-09-10
Grant Date 2021-06-29
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Pocius, Douglas W.
  • Kamber, Derrick S.
  • D'Evelyn, Mark P.
  • Cook, Jonathan D.

Abstract

A process of preparing polycrystalline group III nitride chunks comprising the steps of (a) placing a group III metal inside a source chamber; (b) flowing a halogen-containing gas over the group III metal to form a group III metal halide; (c) contacting the group III metal halide with a nitrogen-containing gas in a deposition chamber containing a foil, the foil comprising at least one of Mo, W, Ta, Pd, Pt, Ir, or Re; (d) forming a polycrystalline group III nitride layer on the foil within the deposition chamber; (e) removing the polycrystalline group III nitride layer from the foil; and (f) comminuting the polycrystalline group III nitride layer to form the polycrystalline group III nitride chunks, wherein the removing and the comminuting are performed in any order or simultaneously.

IPC Classes  ?

  • C23C 16/30 - Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
  • C23C 16/44 - Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition (CVD) processes characterised by the method of coating
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds
  • C23C 16/01 - Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition (CVD) processes on temporary substrates, e.g. on substrates subsequently removed by etching
  • C01B 21/06 - Binary compounds of nitrogen with metals, with silicon, or with boron
  • C23C 16/448 - Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition (CVD) processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials

52.

Oxygen-doped group III metal nitride and method of manufacture

      
Application Number 16868528
Grant Number 11898269
Status In Force
Filing Date 2020-05-06
First Publication Date 2020-08-20
Grant Date 2024-02-13
Owner SLT Technologies, Inc. (USA)
Inventor
  • Jiang, Wenkan
  • Ehrentraut, Dirk
  • D'Evelyn, Mark P.

Abstract

−1, said gallium-containing nitride crystal is essentially free of infrared absorption peaks having an absorbance per unit thickness greater than 10% of the absorbance per unit thickness at 3175 cm.

IPC Classes  ?

  • C30B 29/40 - AIIIBV compounds
  • C01B 21/06 - Binary compounds of nitrogen with metals, with silicon, or with boron
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 29/30 - Semiconductor bodies having polished or roughened surface
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

53.

Method of forming a high quality group-III metal nitride boule or wafer using a patterned substrate

      
Application Number 16736274
Grant Number 11466384
Status In Force
Filing Date 2020-01-07
First Publication Date 2020-07-16
Grant Date 2022-10-11
Owner SLT Technologies, Inc. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Kamber, Derrick S.

Abstract

2, gallium nitride, or aluminum nitride (AlN), forming a pattern on the substrate, the pattern comprising growth centers having a minimum dimension between 1 micrometer and 100 micrometers, and being characterized by at least one pitch dimension between 20 micrometers and 5 millimeters, growing a group III metal nitride from the pattern of growth centers vertically and laterally, and removing the laterally-grown group III metal nitride layer from the substrate. A laterally-grown group III metal nitride layer coalesces, leaving an air gap between the laterally-grown group III metal nitride layer and the substrate or a mask thereupon.

IPC Classes  ?

  • C30B 25/04 - Pattern deposit, e.g. by using masks
  • C30B 29/40 - AIIIBV compounds
  • C30B 25/16 - Controlling or regulating
  • C30B 25/20 - Epitaxial-layer growth characterised by the substrate the substrate being of the same materials as the epitaxial layer

54.

Method for growth of a merged crystal by bonding at least a first and second crystal to an adhesion layer to form a tiled substrate and growing a crystalline composition over said tiled substrate

      
Application Number 16550947
Grant Number 11453956
Status In Force
Filing Date 2019-08-26
First Publication Date 2020-03-19
Grant Date 2022-09-27
Owner SLT Technologies, Inc. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Speck, James S.
  • Kamber, Derrick S.
  • Pocius, Douglas W.

Abstract

Techniques for processing materials in supercritical fluids including processing in a capsule disposed within a high-pressure apparatus enclosure are disclosed. The disclosed techniques are useful for growing crystals of GaN, AlN, InN, and their alloys, including InGaN, AlGaN, and AlInGaN for the manufacture of bulk or patterned substrates, which in turn can be used to make optoelectronic devices, lasers, light emitting diodes, solar cells, photoelectrochemical water splitting and hydrogen generation devices, photodetectors, integrated circuits, and transistors.

IPC Classes  ?

  • C30B 33/06 - Joining of crystals
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • C30B 25/02 - Epitaxial-layer growth
  • C30B 25/18 - Epitaxial-layer growth characterised by the substrate
  • C30B 29/40 - AIIIBV compounds
  • C30B 19/06 - Reaction chambers; Boats for supporting the melt; Substrate holders
  • C30B 19/12 - Liquid-phase epitaxial-layer growth characterised by the substrate

55.

White light devices using non-polar or semipolar gallium containing materials and phosphors

      
Application Number 14882893
Grant Number RE047711
Status In Force
Filing Date 2015-10-14
First Publication Date 2019-11-05
Grant Date 2019-11-05
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Raring, James W.
  • Hall, Eric M.
  • D'Evelyn, Mark P.

Abstract

A packaged optical device includes a substrate having a surface region with light emitting diode devices fabricated on a semipolar or nonpolar GaN substrate. The LEDs emit polarized light and are characterized by an overlapped electron wave function and a hole wave function. Phosphors within the package are excited by the polarized light and, in response, emit electromagnetic radiation of a second wavelength.

IPC Classes  ?

  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • H01L 33/50 - Wavelength conversion elements
  • H01L 33/32 - Materials of the light emitting region containing only elements of group III and group V of the periodic system containing nitrogen
  • H01L 33/54 - Encapsulations having a particular shape
  • H01L 33/58 - Optical field-shaping elements
  • H01L 33/16 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies with a particular crystal structure or orientation, e.g. polycrystalline, amorphous or porous

56.

Method and system for preparing polycrystalline group III metal nitride

      
Application Number 16023137
Grant Number 10619239
Status In Force
Filing Date 2018-06-29
First Publication Date 2019-05-30
Grant Date 2020-04-14
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Pocius, Douglas W.
  • Kamber, Derrick S.
  • D'Evelyn, Mark P.
  • Cook, Jonathan D.

Abstract

A process of preparing polycrystalline group III nitride chunks comprising the steps of (a) placing a group III metal inside a source chamber; (b) flowing a halogen-containing gas over the group III metal to form a group III metal halide; (c) contacting the group III metal halide with a nitrogen-containing gas in a deposition chamber containing a foil, the foil comprising at least one of Mo, W, Ta, Pd, Pt, Ir, or Re; (d) forming a polycrystalline group III nitride layer on the foil within the deposition chamber; (e) removing the polycrystalline group III nitride layer from the foil; and (f) comminuting the polycrystalline group III nitride layer to form the polycrystalline group III nitride chunks, wherein the removing and the comminuting are performed in any order or simultaneously.

IPC Classes  ?

  • C23C 16/448 - Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition (CVD) processes characterised by the method of coating characterised by the method used for generating reactive gas streams, e.g. by evaporation or sublimation of precursor materials
  • C23C 16/30 - Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
  • C23C 16/44 - Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition (CVD) processes characterised by the method of coating
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds
  • C23C 16/01 - Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition (CVD) processes on temporary substrates, e.g. on substrates subsequently removed by etching
  • C01B 21/06 - Binary compounds of nitrogen with metals, with silicon, or with boron

57.

Polarized white light devices using non-polar or semipolar gallium containing materials and transparent phosphors

      
Application Number 14979027
Grant Number RE047241
Status In Force
Filing Date 2015-12-22
First Publication Date 2019-02-12
Grant Date 2019-02-12
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Sharma, Rajat
  • Hall, Eric M.
  • Feezell, Daniel F.

Abstract

A light emitting device includes a substrate having a surface region and a light emitting diode overlying the surface region. The light emitting diode is fabricated on a semipolar or nonpolar GaN containing substrate and emits electromagnetic radiation of a first wavelength. The diode includes a quantum well region characterized by an electron wave function and a hole wave function. The electron wave function and the hole wave function are substantially overlapped within a predetermined spatial region of the quantum well region. The device has a transparent phosphor overlying the light emitting diode. The phosphor is excited by the substantially polarized emission to emit electromagnetic radiation of a second wavelength.

IPC Classes  ?

  • H01L 27/15 - Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components with at least one potential-jump barrier or surface barrier, specially adapted for light emission
  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • H01L 33/50 - Wavelength conversion elements
  • H01L 33/44 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the coatings, e.g. passivation layer or anti-reflective coating
  • H01L 33/32 - Materials of the light emitting region containing only elements of group III and group V of the periodic system containing nitrogen
  • H01L 33/40 - Materials therefor
  • H01L 33/38 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the electrodes with a particular shape
  • H01L 33/16 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies with a particular crystal structure or orientation, e.g. polycrystalline, amorphous or porous

58.

Process for large-scale ammonothermal manufacturing of semipolar gallium nitride boules

      
Application Number 16019528
Grant Number 10604865
Status In Force
Filing Date 2018-06-26
First Publication Date 2019-01-03
Grant Date 2020-03-31
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Ehrentraut, Dirk
  • Kamber, Derrick S.
  • Downey, Bradley C.

Abstract

Methods for large-scale manufacturing of semipolar gallium nitride boules are disclosed. The disclosed methods comprise suspending large-area single crystal seed plates in a rack, placing the rack in a large diameter autoclave or internally-heated high pressure apparatus along with ammonia and a mineralizer, and growing crystals ammonothermally. A bi-faceted growth morphology may be maintained to facilitate fabrication of large area semipolar wafers without growing thick boules.

IPC Classes  ?

  • C30B 19/02 - Liquid-phase epitaxial-layer growth using molten solvents, e.g. flux
  • C30B 29/40 - AIIIBV compounds
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 23/04 - Pattern deposit, e.g. by using masks
  • C30B 25/04 - Pattern deposit, e.g. by using masks

59.

Polycrystalline group III metal nitride with getter and method of making

      
Application Number 15469196
Grant Number RE047114
Status In Force
Filing Date 2017-03-24
First Publication Date 2018-11-06
Grant Date 2018-11-06
Owner SLT Technologies, Inc. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Kamber, Derrick S.

Abstract

A gettered polycrystalline group III metal nitride is formed by heating a group III metal with an added getter in a nitrogen-containing gas. Most of the residual oxygen in the gettered polycrystalline nitride is chemically bound by the getter. The gettered polycrystalline group III metal nitride is useful as a raw material for ammonothermal growth of bulk group III nitride crystals.

IPC Classes  ?

  • C04B 35/00 - Shaped ceramic products characterised by their composition; Ceramic compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
  • C01B 21/06 - Binary compounds of nitrogen with metals, with silicon, or with boron
  • C30B 9/00 - Single-crystal growth from melt solutions using molten solvents
  • C30B 28/06 - Production of homogeneous polycrystalline material with defined structure from liquids by normal freezing or freezing under temperature gradient
  • C30B 29/40 - AIIIBV compounds
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

60.

Apparatus for high pressure reaction

      
Application Number 15474806
Grant Number 10174438
Status In Force
Filing Date 2017-03-30
First Publication Date 2018-10-04
Grant Date 2019-01-08
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Pakalapati, Rajeev Tirumala
  • D'Evelyn, Mark P.

Abstract

An apparatus for processing material at elevated pressure, the apparatus comprising: (a) two or more radial restraint structures defining an interior region configured to receive a processing chamber, the radial restraint structures being configured to resist an outward radial force from the interior region; (b) upper and lower crown members being disposed axially on either end of the interior region and configured to resist an outward axial force from the interior region; (c) a first axial restraint structure coupling the upper crown member and the lower crown member to provide axial restraint of the upper crown member and the lower crown; and (d) a second axial restraint structure compressing the two or more radial restraint structures to provide an axial restraint of the two or more radial restraint structures.

IPC Classes  ?

  • C30B 7/14 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions the crystallising materials being formed by chemical reactions in the solution
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds

61.

Capsule for high pressure, high temperature processing of materials and methods of use

      
Application Number 13657551
Grant Number 10029955
Status In Force
Filing Date 2012-10-22
First Publication Date 2018-07-24
Grant Date 2018-07-24
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Rajeev, Pakalapati Tirumala
  • Pocius, Douglas Wayne
  • Kamber, Derrick S.
  • Coulter, Michael

Abstract

An improved capsule and method of use for processing materials or growing crystals in supercritical fluids is disclosed. The capsule is scalable up to very large volumes and provides for cost-effective processing. In conjunction with suitable high pressure apparatus, the capsule is capable of processing materials at pressures and temperatures of up to approximately 8 GPa and 1500° C., respectively.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 19/08 - Heating of the reaction chamber or the substrate
  • C07B 33/00 - Oxidation in general
  • C30B 35/00 - Apparatus not otherwise provided for, specially adapted for the growth, production or after-treatment of single crystals or of a homogeneous polycrystalline material with defined structure
  • C30B 29/38 - Nitrides
  • B01J 21/06 - Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof

62.

Oxygen-doped group III metal nitride and method of manufacture

      
Application Number 15865391
Grant Number 10648102
Status In Force
Filing Date 2018-01-09
First Publication Date 2018-07-12
Grant Date 2020-05-12
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Jiang, Wenkan
  • Ehrentraut, Dirk
  • D'Evelyn, Mark P.

Abstract

−1.

IPC Classes  ?

  • C30B 29/40 - AIIIBV compounds
  • C01B 21/06 - Binary compounds of nitrogen with metals, with silicon, or with boron
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 29/30 - Semiconductor bodies having polished or roughened surface
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

63.

Reusable nitride wafer, method of making, and use thereof

      
Application Number 15596728
Grant Number 10087550
Status In Force
Filing Date 2017-05-16
First Publication Date 2017-08-31
Grant Date 2018-10-02
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Krames, Michael Ragan

Abstract

Techniques for processing materials for manufacture of gallium-containing nitride substrates are disclosed. More specifically, techniques for fabricating and reusing large area substrates using a combination of processing techniques are disclosed. The methods can be applied to fabricating substrates of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others. Such substrates can be used for a variety of applications including optoelectronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photo detectors, integrated circuits, transistors, and others.

IPC Classes  ?

  • B32B 3/02 - Layered products essentially comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar form; Layered products essentially having particular features of form characterised by features of form at particular places, e.g. in edge regions
  • C30B 25/18 - Epitaxial-layer growth characterised by the substrate
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 29/04 - Semiconductor bodies characterised by their crystalline structure, e.g. polycrystalline, cubic or particular orientation of crystalline planes
  • H01L 29/36 - Semiconductor bodies characterised by the concentration or distribution of impurities
  • H01L 21/78 - Manufacture or treatment of devices consisting of a plurality of solid state components or integrated circuits formed in, or on, a common substrate with subsequent division of the substrate into plural individual devices
  • H01L 31/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • H01L 33/32 - Materials of the light emitting region containing only elements of group III and group V of the periodic system containing nitrogen
  • C30B 23/02 - Epitaxial-layer growth
  • C30B 29/40 - AIIIBV compounds
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 31/18 - Processes or apparatus specially adapted for the manufacture or treatment of these devices or of parts thereof
  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • H01S 5/30 - Structure or shape of the active region; Materials used for the active region

64.

Apparatus for large volume ammonothermal manufacture of gallium nitride crystals and methods of use

      
Application Number 13656615
Grant Number 09724666
Status In Force
Filing Date 2012-10-19
First Publication Date 2017-08-08
Grant Date 2017-08-08
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Rajeev, Pakalapati Tirumala
  • Pocius, Douglas W.
  • D'Evelyn, Mark P.

Abstract

An apparatus to contain the reaction vessel in which gallium nitride crystals (henceforth referred to as bulk crystals) can be grown using the ammonothermal method at high pressure and temperature is disclosed. The apparatus provides adequate containment in all directions, which, for a typical cylindrical vessel, can be classified as radial and axial. Furthermore, depending on the specifics of the design parameters, the apparatus is capable of operating at a temperature up to 1,200 degrees Celsius, a pressure up to 2,000 MPa, and for whatever length of time is necessary to grow satisfactory bulk crystals. The radial constraint in the current disclosure is provided by using several stacked composite rings. The design of the apparatus is scalable to contain reaction volumes larger than 100 cubic centimeters.

IPC Classes  ?

  • B01J 19/06 - Solidifying liquids
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 35/00 - Apparatus not otherwise provided for, specially adapted for the growth, production or after-treatment of single crystals or of a homogeneous polycrystalline material with defined structure

65.

Method for growth of a merged crystal by bonding at least a first and second crystal to an adhesion layer to form a tiled substrate and growing a crystalline composition over said tiled substrate

      
Application Number 15426770
Grant Number 10400352
Status In Force
Filing Date 2017-02-07
First Publication Date 2017-05-25
Grant Date 2019-09-03
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Speck, James S.
  • Kamber, Derrick S.
  • Pocius, Douglas W.

Abstract

Techniques for processing materials in supercritical fluids including processing in a capsule disposed within a high-pressure apparatus enclosure are disclosed. The disclosed techniques are useful for growing crystals of GaN, AlN, InN, and their alloys, including InGaN, AlGaN, and AlInGaN for the manufacture of bulk or patterned substrates, which in turn can be used to make optoelectronic devices, lasers, light emitting diodes, solar cells, photoelectrochemical water splitting and hydrogen generation devices, photodetectors, integrated circuits, and transistors.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • C30B 25/02 - Epitaxial-layer growth
  • C30B 25/18 - Epitaxial-layer growth characterised by the substrate
  • C30B 29/40 - AIIIBV compounds
  • C30B 33/06 - Joining of crystals
  • C30B 19/06 - Reaction chambers; Boats for supporting the melt; Substrate holders
  • C30B 19/12 - Liquid-phase epitaxial-layer growth characterised by the substrate

66.

Large area seed crystal for ammonothermal crystal growth and method of making

      
Application Number 14249708
Grant Number 09650723
Status In Force
Filing Date 2014-04-10
First Publication Date 2017-05-16
Grant Date 2017-05-16
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Jiang, Wenkan
  • Kamber, Derrick S.
  • Pakalapati, Rajeev T.
  • Krames, Michael R.

Abstract

Large area seed crystals for ammonothermal GaN growth are fabricated by deposition or layer transfer of a GaN layer on a CTE-matched handle substrate. The sides and back of the handle substrate are protected from the ammonothermal growth environment by a coating comprising an adhesion layer, a diffusion barrier layer, and an inert layer. A patterned mask, also comprising an adhesion layer, a diffusion barrier layer, and an inert layer, may be provided over the GaN layer to allow for reduction of the dislocation density by lateral epitaxial growth.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 9/00 - Single-crystal growth from melt solutions using molten solvents
  • C30B 29/40 - AIIIBV compounds
  • C30B 25/02 - Epitaxial-layer growth
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof

67.

Surface morphology of non-polar gallium nitride containing substrates

      
Application Number 14302250
Grant Number 09831386
Status In Force
Filing Date 2014-06-11
First Publication Date 2017-03-30
Grant Date 2017-11-28
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Raring, James W.
  • Elsass, Christiane

Abstract

Optical devices such as LEDs and lasers are discloses. The devices include a non-polar gallium nitride substrate member having an off-axis non-polar oriented crystalline surface plane. The off-axis non-polar oriented crystalline surface plane can be up to about −0.6 degrees in a c-plane direction and up to about −20 degrees in a c-plane direction in certain embodiments. In certain embodiments, a gallium nitride containing epitaxial layer is formed overlying the off-axis non-polar oriented crystalline surface plane. In certain embodiments, devices include a surface region overlying the gallium nitride epitaxial layer that is substantially free of hillocks.

IPC Classes  ?

  • H01L 33/32 - Materials of the light emitting region containing only elements of group III and group V of the periodic system containing nitrogen
  • H01L 33/18 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies with a particular crystal structure or orientation, e.g. polycrystalline, amorphous or porous within the light emitting region
  • H01L 33/06 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies with a quantum effect structure or superlattice, e.g. tunnel junction within the light emitting region, e.g. quantum confinement structure or tunnel barrier
  • H01L 33/24 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies with a particular shape, e.g. curved or truncated substrate of the light emitting region, e.g. non-planar junction
  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • H01S 5/32 - Structure or shape of the active region; Materials used for the active region comprising PN junctions, e.g. hetero- or double- hetero-structures
  • H01S 5/323 - Structure or shape of the active region; Materials used for the active region comprising PN junctions, e.g. hetero- or double- hetero-structures in AIIIBV compounds, e.g. AlGaAs-laser
  • H01S 5/343 - Structure or shape of the active region; Materials used for the active region comprising quantum well or superlattice structures, e.g. single quantum well [SQW] lasers, multiple quantum well [MQW] lasers or graded index separate confinement heterostructure [GRINSCH] lasers in AIIIBV compounds, e.g. AlGaAs-laser

68.

Pressure release mechanism for capsule and method of use with supercritical fluids

      
Application Number 15269538
Grant Number 10293318
Status In Force
Filing Date 2016-09-19
First Publication Date 2017-03-23
Grant Date 2019-05-21
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark Philip
  • Pakalapati, Rajeev Tirumala

Abstract

A pressure release mechanism for use with a capsule for processing materials or growing crystals in supercritical fluids is disclosed. The capsule with the pressure release mechanism is scalable up to very large volumes and is cost effective according to a preferred embodiment. In conjunction with suitable high pressure apparatus, the capsule with pressure release mechanism is capable of processing materials at pressures and temperatures of 20-2000 MPa and 25-1500° C., respectively. Of course, there can be other variations, modifications, and alternatives.

IPC Classes  ?

  • B01J 13/00 - Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
  • B01J 3/00 - Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
  • B01J 3/04 - Pressure vessels, e.g. autoclaves
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 35/00 - Apparatus not otherwise provided for, specially adapted for the growth, production or after-treatment of single crystals or of a homogeneous polycrystalline material with defined structure
  • B08B 7/00 - Cleaning by methods not provided for in a single other subclass or a single group in this subclass

69.

Large area, low-defect gallium-containing nitride crystals, method of making, and method of use

      
Application Number 15226552
Grant Number 10301745
Status In Force
Filing Date 2016-08-02
First Publication Date 2017-02-02
Grant Date 2019-05-28
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Ehrentraut, Dirk
  • Jiang, Wenkan
  • Downey, Bradley C.

Abstract

An ultralow defect gallium-containing nitride crystal and methods of making ultralow defect gallium-containing nitride crystals are disclosed. The crystals are useful as substrates for light emitting diodes, laser diodes, transistors, photodetectors, solar cells, and photoelectrochemical water splitting for hydrogen generators.

IPC Classes  ?

  • C30B 33/00 - After-treatment of single crystals or homogeneous polycrystalline material with defined structure
  • C30B 33/06 - Joining of crystals
  • C30B 29/40 - AIIIBV compounds
  • C30B 25/18 - Epitaxial-layer growth characterised by the substrate
  • C30B 25/02 - Epitaxial-layer growth
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 25/20 - Epitaxial-layer growth characterised by the substrate the substrate being of the same materials as the epitaxial layer
  • H01L 29/04 - Semiconductor bodies characterised by their crystalline structure, e.g. polycrystalline, cubic or particular orientation of crystalline planes
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 33/32 - Materials of the light emitting region containing only elements of group III and group V of the periodic system containing nitrogen
  • H01S 5/32 - Structure or shape of the active region; Materials used for the active region comprising PN junctions, e.g. hetero- or double- hetero-structures
  • H01S 5/323 - Structure or shape of the active region; Materials used for the active region comprising PN junctions, e.g. hetero- or double- hetero-structures in AIIIBV compounds, e.g. AlGaAs-laser

70.

Transparent group III metal nitride and method of manufacture

      
Application Number 14485516
Grant Number 09543392
Status In Force
Filing Date 2014-09-12
First Publication Date 2017-01-10
Grant Date 2017-01-10
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Jiang, Wenkan
  • Ehrentraut, Dirk
  • D'Evelyn, Mark P.

Abstract

Large-area, low-cost single crystal transparent gallium-containing nitride crystals useful as substrates for fabricating GaN devices for electronic and/or optoelectronic applications are disclosed. The gallium-containing nitride crystals are formed by controlling impurity concentrations during ammonothermal growth and processing to control the relative concentrations of point defect species.

IPC Classes  ?

  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • C30B 29/40 - AIIIBV compounds
  • H01L 29/04 - Semiconductor bodies characterised by their crystalline structure, e.g. polycrystalline, cubic or particular orientation of crystalline planes
  • H01L 29/36 - Semiconductor bodies characterised by the concentration or distribution of impurities
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

71.

Method and system for preparing polycrystalline group III metal nitride

      
Application Number 15011266
Grant Number 10094017
Status In Force
Filing Date 2016-01-29
First Publication Date 2016-08-04
Grant Date 2018-10-09
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Pocius, Douglas W.
  • Kamber, Derrick S.
  • D'Evelyn, Mark P.
  • Cook, Jonathan D.

Abstract

A process of preparing polycrystalline group III nitride chunks comprising the steps of (a) placing a group III metal inside a source chamber; (b) flowing a halogen-containing gas over the group III metal to form a group III metal halide; (c) contacting the group III metal halide with a nitrogen-containing gas in a deposition chamber containing a foil, the foil comprising at least one of Mo, W, Ta, Pd, Pt, Ir, or Re; (d) forming a polycrystalline group III nitride layer on the foil within the deposition chamber; (e) removing the polycrystalline group III nitride layer from the foil; and (f) comminuting the polycrystalline group III nitride layer to form the polycrystalline group III nitride chunks, wherein the removing and the comminuting are performed in any order or simultaneously.

IPC Classes  ?

  • C23C 16/30 - Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
  • C23C 16/44 - Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition (CVD) processes characterised by the method of coating
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds
  • C23C 16/01 - Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition (CVD) processes on temporary substrates, e.g. on substrates subsequently removed by etching
  • C01B 21/06 - Binary compounds of nitrogen with metals, with silicon, or with boron

72.

Ultrapure mineralizers and methods for nitride crystal growth

      
Application Number 14033107
Grant Number 09299555
Status In Force
Filing Date 2013-09-20
First Publication Date 2016-03-29
Grant Date 2016-03-29
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Alexander, Alex
  • Nink, Jr., John W.
  • D'Evelyn, Mark P.

Abstract

An ultrapure mineralizer is formed by vaporization, condensation, and delivery of a condensable mineralizer composition. The mineralizer has an oxygen content below 100 parts per million. The ultrapure mineralizer is useful as a raw material for ammonothermal growth of bulk group III metal nitride crystals.

IPC Classes  ?

  • C30B 9/12 - Salt solvents, e.g. flux growth
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 9/04 - Single-crystal growth from melt solutions using molten solvents by cooling of the solution
  • C30B 9/08 - Single-crystal growth from melt solutions using molten solvents by cooling of the solution using other solvents
  • C30B 29/38 - Nitrides

73.

Method for quantification of extended defects in gallium-containing nitride crystals

      
Application Number 14013753
Grant Number 09275912
Status In Force
Filing Date 2013-08-29
First Publication Date 2016-03-01
Grant Date 2016-03-01
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Jiang, Wenkan
  • Ehrentraut, Dirk
  • Downey, Bradley C.
  • D'Evelyn, Mark P.

Abstract

4; removing the gallium-containing nitride crystal, wafer, or device from the etchant solution; and quantifying the concentration of at least one of etch pits or etch grooves.

IPC Classes  ?

  • H01L 29/04 - Semiconductor bodies characterised by their crystalline structure, e.g. polycrystalline, cubic or particular orientation of crystalline planes
  • H01L 31/036 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their crystalline structure or particular orientation of the crystalline planes
  • H01L 33/16 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies with a particular crystal structure or orientation, e.g. polycrystalline, amorphous or porous
  • H01L 21/66 - Testing or measuring during manufacture or treatment

74.

Method for synthesis of high quality large area bulk gallium based crystals

      
Application Number 14930170
Grant Number 10100425
Status In Force
Filing Date 2015-11-02
First Publication Date 2016-02-25
Grant Date 2018-10-16
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Speck, James S.

Abstract

A large area nitride crystal, comprising gallium and nitrogen, with a non-polar or semi-polar large-area face, is disclosed, along with a method of manufacture. The crystal is useful as a substrate for a light emitting diode, a laser diode, a transistor, a photodetector, a solar cell, or for photoelectrochemical water splitting for hydrogen generation.

IPC Classes  ?

  • C30B 1/10 - Single-crystal growth directly from the solid state by solid state reactions or multi-phase diffusion
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 25/02 - Epitaxial-layer growth
  • C30B 29/40 - AIIIBV compounds
  • C30B 7/00 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • H01L 29/04 - Semiconductor bodies characterised by their crystalline structure, e.g. polycrystalline, cubic or particular orientation of crystalline planes
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 29/34 - Semiconductor bodies having polished or roughened surface the imperfections being on the surface
  • H01L 29/36 - Semiconductor bodies characterised by the concentration or distribution of impurities

75.

Reusable nitride wafer, method of making, and use thereof

      
Application Number 14805278
Grant Number 09653554
Status In Force
Filing Date 2015-07-21
First Publication Date 2016-01-21
Grant Date 2017-05-16
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Krames, Michael Ragan

Abstract

Techniques for processing materials for manufacture of gallium-containing nitride substrates are disclosed. More specifically, techniques for fabricating and reusing large area substrates using a combination of processing techniques are disclosed. The methods can be applied to fabricating substrates of GaN, AlN, InN, InGaN, AlGaN, and AlInGaN, and others. Such substrates can be used for a variety of applications including optoelectronic devices, lasers, light emitting diodes, solar cells, photo electrochemical water splitting and hydrogen generation, photo detectors, integrated circuits, transistors, and others.

IPC Classes  ?

  • B32B 3/02 - Layered products essentially comprising a layer with external or internal discontinuities or unevennesses, or a layer of non-planar form; Layered products essentially having particular features of form characterised by features of form at particular places, e.g. in edge regions
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 29/04 - Semiconductor bodies characterised by their crystalline structure, e.g. polycrystalline, cubic or particular orientation of crystalline planes
  • H01L 29/36 - Semiconductor bodies characterised by the concentration or distribution of impurities
  • H01L 21/78 - Manufacture or treatment of devices consisting of a plurality of solid state components or integrated circuits formed in, or on, a common substrate with subsequent division of the substrate into plural individual devices
  • H01L 31/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • H01L 33/32 - Materials of the light emitting region containing only elements of group III and group V of the periodic system containing nitrogen

76.

High pressure apparatus and method for nitride crystal growth

      
Application Number 13556105
Grant Number 09157167
Status In Force
Filing Date 2012-07-23
First Publication Date 2015-10-13
Grant Date 2015-10-13
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Pakalapati, Rajeev T.
  • D'Evelyn, Mark P.

Abstract

A high pressure apparatus and related methods for processing supercritical fluids are disclosed. In certain embodiments, the present apparatus includes a capsule, a heater, at least one ceramic ring or multiple rings, optionally, with one or more scribe marks and/or cracks present. In certain embodiments, the apparatus has a metal sleeve containing each ceramic ring. The apparatus also has a high strength enclosure, end flanges with associated insulation, and a power control system. In certain embodiments, a high pressure apparatus is constructed such that the diametric annular gap between the outer diameter of the heater and the ceramic ring is selected to provide radial load-bearing contact above a particular temperature and pressure. In certain embodiments, the apparatus is capable of accessing pressures of 0.2 GPa to 2 GPa and temperatures of 400° C. to 1200° C.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

77.

Process for large-scale ammonothermal manufacturing of gallium nitride boules

      
Application Number 14599335
Grant Number 10036099
Status In Force
Filing Date 2015-01-16
First Publication Date 2015-05-14
Grant Date 2018-07-31
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Ehrentraut, Dirk
  • Kamber, Derrick S.
  • Downey, Bradley C.

Abstract

Large-scale manufacturing of gallium nitride boules using m-plane or wedge-shaped seed crystals can be accomplished using ammonothermal growth methods. Large-area single crystal seed plates are suspended in a rack, placed in a large diameter autoclave or internally-heated high pressure apparatus along with ammonia and a mineralizer, and crystals are grown ammonothermally. The orientation of the m-plane or wedge-shaped seed crystals are chosen to provide efficient utilization of the seed plates and of the volume inside the autoclave or high pressure apparatus.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • B01J 3/00 - Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
  • B01J 3/04 - Pressure vessels, e.g. autoclaves
  • B01J 3/06 - Processes using ultra-high pressure, e.g. for the formation of diamonds; Apparatus therefor, e.g. moulds or dies
  • B30B 11/00 - Presses specially adapted for forming shaped articles from material in particulate or plastic state, e.g. briquetting presses or tabletting presses

78.

Apparatus for processing materials at high temperatures and pressures

      
Application Number 13812757
Grant Number 10145021
Status In Force
Filing Date 2011-07-28
First Publication Date 2015-05-07
Grant Date 2018-12-04
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Afimiwala, Kirsh
  • Zeng, Larry

Abstract

An apparatus for processing materials at high temperatures comprises a high strength enclosure; a plurality of high strength radial segments disposed adjacent to and radially inward from the high strength enclosure; a liner disposed adjacent to and radially inward from the radical segments; a chamber defined interior to the liner; a heating device disposed within the chamber; and a capsule disposed within the chamber, the capsule configured to hold a supercritical fluid. The apparatus may be used for growing crystals, e.g., GaN, under high temperature and pressure conditions.

IPC Classes  ?

  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds
  • C30B 7/14 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions the crystallising materials being formed by chemical reactions in the solution
  • C30B 35/00 - Apparatus not otherwise provided for, specially adapted for the growth, production or after-treatment of single crystals or of a homogeneous polycrystalline material with defined structure

79.

Gallium—nitride-on-handle substrate materials and devices and method of manufacture

      
Application Number 14301520
Grant Number 08946865
Status In Force
Filing Date 2014-06-11
First Publication Date 2014-11-27
Grant Date 2015-02-03
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Chakraborty, Arpan
  • Houck, William D.

Abstract

A gallium and nitrogen containing substrate structure includes a handle substrate member having a first surface and a second surface and a transferred thickness of gallium and nitrogen material. The structure has a gallium and nitrogen containing active region grown overlying the transferred thickness and a recessed region formed within a portion of the handle substrate member. The substrate structure has a conductive material formed within the recessed region configured to transfer thermal energy from at least the transferred thickness of gallium and nitrogen material.

IPC Classes  ?

  • H01L 29/06 - Semiconductor bodies characterised by the shapes, relative sizes, or dispositions of the semiconductor regions
  • H01L 31/0304 - Inorganic materials including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 31/0352 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their shape or by the shapes, relative sizes or disposition of the semiconductor regions
  • H01L 31/036 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by their crystalline structure or particular orientation of the crystalline planes
  • H01L 33/32 - Materials of the light emitting region containing only elements of group III and group V of the periodic system containing nitrogen
  • H01L 33/22 - Roughened surfaces, e.g. at the interface between epitaxial layers
  • H01L 33/50 - Wavelength conversion elements

80.

White light devices using non-polar or semipolar gallium containing materials and phosphors

      
Application Number 14035693
Grant Number 08956894
Status In Force
Filing Date 2013-09-24
First Publication Date 2014-07-31
Grant Date 2015-02-17
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Raring, James W.
  • Hall, Eric M.
  • D'Evelyn, Mark P.

Abstract

A packaged optical device includes a substrate having a surface region with light emitting diode devices fabricated on a semipolar or nonpolar GaN substrate. The light emitting diodes emit polarized light and are characterized by an overlapped electron wave function and a hole wave function. Phosphors within the package are excited by the polarized light and, in response, emit electromagnetic radiation of a second wavelength.

IPC Classes  ?

  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • H01L 33/50 - Wavelength conversion elements
  • H01L 33/32 - Materials of the light emitting region containing only elements of group III and group V of the periodic system containing nitrogen
  • H01L 33/16 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies with a particular crystal structure or orientation, e.g. polycrystalline, amorphous or porous
  • H01L 33/54 - Encapsulations having a particular shape
  • H01L 33/58 - Optical field-shaping elements

81.

High quality group-III metal nitride crystals, methods of making, and methods of use

      
Application Number 14089281
Grant Number 09589792
Status In Force
Filing Date 2013-11-25
First Publication Date 2014-05-29
Grant Date 2017-03-07
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Jiang, Wenkan
  • D'Evelyn, Mark P.
  • Kamber, Derrick S.
  • Ehrentraut, Dirk
  • Krames, Michael

Abstract

High quality ammonothermal group III metal nitride crystals having a pattern of locally-approximately-linear arrays of threading dislocations, methods of manufacturing high quality ammonothermal group III metal nitride crystals, and methods of using such crystals are disclosed. The crystals are useful for seed bulk crystal growth and as substrates for light emitting diodes, laser diodes, transistors, photodetectors, solar cells, and for photoelectrochemical water splitting for hydrogen generation devices.

IPC Classes  ?

  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes
  • C30B 29/40 - AIIIBV compounds

82.

Large area, low-defect gallium-containing nitride crystals, method of making, and method of use

      
Application Number 13600191
Grant Number 09404197
Status In Force
Filing Date 2012-08-30
First Publication Date 2014-03-06
Grant Date 2016-08-02
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Ehrentraut, Dirk
  • Jiang, Wenkan
  • Downey, Bradley C.

Abstract

An ultralow defect gallium-containing nitride crystal and methods of making ultralow defect gallium-containing nitride crystals are disclosed. The crystals are useful as substrates for light emitting diodes, laser diodes, transistors, photodetectors, solar cells, and photoelectrochemical water splitting for hydrogen generators.

IPC Classes  ?

83.

Process for large-scale ammonothermal manufacturing of semipolar gallium nitride boules

      
Application Number 13908836
Grant Number 10145026
Status In Force
Filing Date 2013-06-03
First Publication Date 2013-12-05
Grant Date 2018-12-04
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Ehrentraut, Dirk
  • Kamber, Derrick S.
  • Downey, Bradley C.

Abstract

Methods for large-scale manufacturing of semipolar gallium nitride boules are disclosed. The disclosed methods comprise suspending large-area single crystal seed plates in a rack, placing the rack in a large diameter autoclave or internally-heated high pressure apparatus along with ammonia and a mineralizer, and growing crystals ammonothermally. A bi-faceted growth morphology may be maintained to facilitate fabrication of large area semipolar wafers without growing thick boules.

IPC Classes  ?

  • C30B 29/40 - AIIIBV compounds
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

84.

Method and surface morphology of non-polar gallium nitride containing substrates

      
Application Number 13548635
Grant Number 08575728
Status In Force
Filing Date 2012-07-13
First Publication Date 2013-11-05
Grant Date 2013-11-05
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Raring, James W.
  • Poblenz, Christiane

Abstract

An optical device, e.g., LED, laser. The device includes a non-polar gallium nitride substrate member having a slightly off-axis non-polar oriented crystalline surface plane. In a specific embodiment, the slightly off-axis non-polar oriented crystalline surface plane is up to about −0.6 degrees in a c-plane direction, but can be others. In a specific embodiment, the present invention provides a gallium nitride containing epitaxial layer formed overlying the slightly off-axis non-polar oriented crystalline surface plane. In a specific embodiment, the device includes a surface region overlying the gallium nitride epitaxial layer that is substantially free of hillocks.

IPC Classes  ?

  • H01L 29/04 - Semiconductor bodies characterised by their crystalline structure, e.g. polycrystalline, cubic or particular orientation of crystalline planes

85.

Polarized white light devices using non-polar or semipolar gallium containing materials and transparent phosphors

      
Application Number 13623788
Grant Number 08618560
Status In Force
Filing Date 2012-09-20
First Publication Date 2013-10-17
Grant Date 2013-12-31
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Sharma, Rajat
  • Hall, Eric M.
  • Feezell, Daniel F.

Abstract

A light emitting device includes a substrate having a surface region and a light emitting diode overlying the surface region. The light emitting diode is fabricated on a semipolar or nonpolar GaN containing substrate and emits electromagnetic radiation of a first wavelength. The diode includes a quantum well region characterized by an electron wave function and a hole wave function. The electron wave function and the hole wave function are substantially overlapped within a predetermined spatial region of the quantum well region. The device has a transparent phosphor overlying the light emitting diode. The phosphor is excited by the substantially polarized emission to emit electromagnetic radiation of a second wavelength.

IPC Classes  ?

  • H01L 27/15 - Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components with at least one potential-jump barrier or surface barrier, specially adapted for light emission
  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof

86.

Polycrystalline group III metal nitride with getter and method of making

      
Application Number 13894220
Grant Number 08987156
Status In Force
Filing Date 2013-05-14
First Publication Date 2013-09-26
Grant Date 2015-03-24
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Kamber, Derrick S.

Abstract

A gettered polycrystalline group III metal nitride is formed by heating a group III metal with an added getter in a nitrogen-containing gas. Most of the residual oxygen in the gettered polycrystalline nitride is chemically bound by the getter. The gettered polycrystalline group III metal nitride is useful as a raw material for ammonothermal growth of bulk group III nitride crystals.

IPC Classes  ?

  • C04B 35/00 - Shaped ceramic products characterised by their composition; Ceramic compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
  • C01B 21/06 - Binary compounds of nitrogen with metals, with silicon, or with boron
  • C30B 9/00 - Single-crystal growth from melt solutions using molten solvents
  • C30B 28/06 - Production of homogeneous polycrystalline material with defined structure from liquids by normal freezing or freezing under temperature gradient
  • C30B 29/40 - AIIIBV compounds
  • C30B 7/10 - Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions by application of pressure, e.g. hydrothermal processes

87.

Method and surface morphology of non-polar gallium nitride containing substrates

      
Application Number 13548770
Grant Number 08524578
Status In Force
Filing Date 2012-07-13
First Publication Date 2013-09-03
Grant Date 2013-09-03
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Raring, James W.
  • Poblenz, Christiane

Abstract

An optical device, e.g., LED, laser. The device includes a non-polar gallium nitride substrate member having a slightly off-axis non-polar oriented crystalline surface plane. In a specific embodiment, the slightly off-axis non-polar oriented crystalline surface plane is up to about −0.6 degrees in a c-plane direction, but can be others. In a specific embodiment, the present invention provides a gallium nitride containing epitaxial layer formed overlying the slightly off-axis non-polar oriented crystalline surface plane. In a specific embodiment, the device includes a surface region overlying the gallium nitride epitaxial layer that is substantially free of hillocks.

IPC Classes  ?

  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof

88.

Large area nonpolar or semipolar gallium and nitrogen containing substrate and resulting devices

      
Application Number 13548931
Grant Number 08492185
Status In Force
Filing Date 2012-07-13
First Publication Date 2013-07-23
Grant Date 2013-07-23
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Speck, James
  • Houck, William
  • Schmidt, Mathew
  • Chakraborty, Arpan

Abstract

A method for fabricating large-area nonpolar or semipolar GaN wafers with high quality, low stacking fault density, and relatively low dislocation density is described. The wafers are useful as seed crystals for subsequent bulk growth or as substrates for LEDs and laser diodes.

IPC Classes  ?

  • H01L 21/00 - Processes or apparatus specially adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof

89.

Photonic-crystal light emitting diode and method of manufacture

      
Application Number 12569844
Grant Number 08455894
Status In Force
Filing Date 2009-09-29
First Publication Date 2013-06-04
Grant Date 2013-06-04
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Sharma, Rajat
  • Hall, Eric M.

Abstract

−2. The backside of the stack, exposed by removal of the original substrate, has a photonic crystal pattern for improved light extraction.

IPC Classes  ?

  • H01L 33/02 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies

90.

Large area nitride crystal and method for making it

      
Application Number 13731453
Grant Number 09564320
Status In Force
Filing Date 2012-12-31
First Publication Date 2013-05-16
Grant Date 2017-02-07
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Speck, James S.
  • Kamber, Derrick S.
  • Pocius, Douglas W.

Abstract

Techniques for processing materials in supercritical fluids including processing in a capsule disposed within a high-pressure apparatus enclosure are disclosed. The disclosed techniques are useful for growing crystals of GaN, AlN, InN, and their alloys, including InGaN, AlGaN, and AlInGaN for the manufacture of bulk or patterned substrates, which in turn can be used to make optoelectronic devices, lasers, light emitting diodes, solar cells, photoelectrochemical water splitting and hydrogen generation devices, photodetectors, integrated circuits, and transistors.

IPC Classes  ?

  • H01L 21/02 - Manufacture or treatment of semiconductor devices or of parts thereof
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
  • C30B 25/02 - Epitaxial-layer growth
  • C30B 25/18 - Epitaxial-layer growth characterised by the substrate
  • C30B 29/40 - AIIIBV compounds
  • C30B 33/06 - Joining of crystals

91.

Surface morphology of non-polar gallium nitride containing substrates

      
Application Number 13621485
Grant Number 08749030
Status In Force
Filing Date 2012-09-17
First Publication Date 2013-01-17
Grant Date 2014-06-10
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Raring, James W.
  • Elsass, Christiane

Abstract

Optical devices such as LEDs and lasers are discloses. The devices include a non-polar gallium nitride substrate member having an off-axis non-polar oriented crystalline surface plane. The off-axis non-polar oriented crystalline surface plane can be up to about −0.6 degrees in a c-plane direction and up to about −20 degrees in a c-plane direction in certain embodiments. In certain embodiments, a gallium nitride containing epitaxial layer is formed overlying the off-axis non-polar oriented crystalline surface plane. In certain embodiments, devices include a surface region overlying the gallium nitride epitaxial layer that is substantially free of hillocks.

IPC Classes  ?

  • H01L 29/04 - Semiconductor bodies characterised by their crystalline structure, e.g. polycrystalline, cubic or particular orientation of crystalline planes
  • H01L 33/16 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies with a particular crystal structure or orientation, e.g. polycrystalline, amorphous or porous

92.

Microcavity light emitting diode method of manufacture

      
Application Number 12569337
Grant Number 08354679
Status In Force
Filing Date 2009-09-29
First Publication Date 2013-01-15
Grant Date 2013-01-15
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Sharma, Rajat

Abstract

−2.

IPC Classes  ?

  • H01L 27/15 - Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components with at least one potential-jump barrier or surface barrier, specially adapted for light emission
  • H01L 29/26 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, elements provided for in two or more of the groups , , , ,
  • H01L 31/12 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof structurally associated with, e.g. formed in or on a common substrate with, one or more electric light sources, e.g. electroluminescent light sources, and electrically or optically coupled thereto
  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof

93.

Multi color active regions for white light emitting diode

      
Application Number 12880803
Grant Number 08314429
Status In Force
Filing Date 2010-09-13
First Publication Date 2012-11-20
Grant Date 2012-11-20
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Raring, James
  • Sharma, Rajat
  • Poblenz, Christiane

Abstract

A light emitting diode device has a gallium and nitrogen containing substrate with a surface region with an epitaxial layer overlying the surface region. Preferably the device includes a first active region overlying the surface and configured to emit first electromagnetic radiation having a wavelength ranging from about 405 nm to 490 nm; a second active region overlying the surface and configured to emit second electromagnetic radiation having a wavelength ranging from about 491 nm to about 590 nm; and a third region overlying the surface region and configured to emit third electromagnetic radiation having a wavelength ranging from about 591 nm to about 700 nm. A p-type epitaxial layer covers the first, second, and third active regions.

IPC Classes  ?

  • H01L 31/0256 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by their semiconductor bodies characterised by the material

94.

Polarization direction of optical devices using selected spatial configurations

      
Application Number 13553691
Grant Number 09105806
Status In Force
Filing Date 2012-07-19
First Publication Date 2012-11-15
Grant Date 2015-08-11
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Sharma, Rajat
  • Hall, Eric M.

Abstract

A GaN based light emitting diode device which emits polarized light or light of various degrees of polarization for use in the creation of optical devices. The die are cut to different shapes, or contain some indicia that are used to represent the configuration of the weak dipole plane and the strong dipole plane. This allows for the more efficient manufacturing of such light emitting diode based optical devices.

IPC Classes  ?

  • H01L 33/20 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies with a particular shape, e.g. curved or truncated substrate
  • H01L 33/18 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies with a particular crystal structure or orientation, e.g. polycrystalline, amorphous or porous within the light emitting region
  • H01L 33/32 - Materials of the light emitting region containing only elements of group III and group V of the periodic system containing nitrogen

95.

High indium containing InGaN substrates for long wavelength optical devices

      
Application Number 12785404
Grant Number 08306081
Status In Force
Filing Date 2010-05-21
First Publication Date 2012-11-06
Grant Date 2012-11-06
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Schmidt, Mathew
  • D'Evelyn, Mark P.

Abstract

An improved optical device. The device has a gallium nitride substrate member comprising indium entities, gallium entities, and nitrogen entities. In one or more embodiments, the gallium nitride substrate member has an indium content ranging from about 1 to about 50% in weight. Preferably, the gallium nitride substrate member has a semipolar crystalline surface region or a non-polar crystalline surface region. The device has an epitaxially formed laser stripe region comprising an indium content ranging from about 1 to about 50% and formed overlying a portion of the semipolar crystalline orientation surface region or the non-polar crystalline surface region. The laser stripe region is characterized by a cavity orientation in a predefined direction according to a specific embodiment. The laser strip region has a first end and a second end including respective a first cleaved facet provided on the first end of the laser stripe region and a second cleaved facet provided on the second end of the laser stripe region.

IPC Classes  ?

96.

Polarized white light devices using non-polar or semipolar gallium containing materials and transparent phosphors

      
Application Number 12754886
Grant Number 08299473
Status In Force
Filing Date 2010-04-06
First Publication Date 2012-10-30
Grant Date 2012-10-30
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Sharma, Rajat
  • Hall, Eric M.
  • Feezell, Daniel F.

Abstract

A light emitting device includes a substrate having a surface region and a light emitting diode overlying the surface region. The light emitting diode is fabricated on a semipolar or nonpolar GaN containing substrate and emits electromagnetic radiation of a first wavelength. The diode includes a quantum well region characterized by an electron wave function and a hole wave function. The electron wave function and the hole wave function are substantially overlapped within a predetermined spatial region of the quantum well region. The device has a transparent phosphor overlying the light emitting diode. The phosphor is excited by the substantially polarized emission to emit electromagnetic radiation of a second wavelength.

IPC Classes  ?

  • H01L 27/15 - Devices consisting of a plurality of semiconductor or other solid-state components formed in or on a common substrate including semiconductor components with at least one potential-jump barrier or surface barrier, specially adapted for light emission
  • H01L 33/00 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof

97.

Method and structure for manufacture of light emitting diode devices using bulk GaN

      
Application Number 12749476
Grant Number 08252662
Status In Force
Filing Date 2010-03-29
First Publication Date 2012-08-28
Grant Date 2012-08-28
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Poblenz, Christiane
  • Schmidt, Mathew C.
  • Feezell, Daniel F.
  • Raring, James W.
  • Sharma, Rajat

Abstract

A method for manufacturing a plurality light emitting diodes includes providing a gallium nitride containing bulk crystalline substrate material configured in a non-polar or semi-polar crystallographic orientation, forming an etch stop layer, forming an n-type layer overlying the etch stop layer, forming an active region, a p-type layer, and forming a metallization. The method includes removing a thickness of material from the backside of the bulk gallium nitride containing substrate material. A plurality of individual LED devices are formed from at least a sandwich structure comprising portions of the metallization layer, the p-type layer, active layer, and the n-type layer. The LED devices are joined to a carrier structure. The method also includes subjecting the gallium nitride containing bulk crystalline substrate material to at least one etching process to selectively remove crystalline material underlying the etch stop layer, wherein the etch stop layer is exposed, and the etch stop layer remains substantially intact.

IPC Classes  ?

  • H01L 21/30 - Treatment of semiconductor bodies using processes or apparatus not provided for in groups

98.

Method and surface morphology of non-polar gallium nitride containing substrates

      
Application Number 12497289
Grant Number 08247887
Status In Force
Filing Date 2009-07-02
First Publication Date 2012-08-21
Grant Date 2012-08-21
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Raring, James
  • Poblenz, Christiane

Abstract

An optical device, e.g., LED, laser. The device includes a non-polar gallium nitride substrate member having a slightly off-axis non-polar oriented crystalline surface plane. In a specific embodiment, the slightly off-axis non-polar oriented crystalline surface plane is up to about −0.6 degrees in a c-plane direction, but can be others. In a specific embodiment, the present invention provides a gallium nitride containing epitaxial layer formed overlying the slightly off-axis non-polar oriented crystalline surface plane. In a specific embodiment, the device includes a surface region overlying the gallium nitride epitaxial layer that is substantially free of hillocks.

IPC Classes  ?

  • H01L 29/04 - Semiconductor bodies characterised by their crystalline structure, e.g. polycrystalline, cubic or particular orientation of crystalline planes

99.

Polarization direction of optical devices using selected spatial configurations

      
Application Number 12720593
Grant Number 08247886
Status In Force
Filing Date 2010-03-09
First Publication Date 2012-08-21
Grant Date 2012-08-21
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • Sharma, Rajat
  • Hall, Eric M.

Abstract

A GaN based light emitting diode device which emits polarized light or light of various degrees of polarization for use in the creation of optical devices. The die are cut to different shapes, or contain some indicia that are used to represent the configuration of the weak dipole plane and the strong dipole plane. This allows for the more efficient manufacturing of such light emitting diode based optical devices.

IPC Classes  ?

  • H01L 33/20 - SEMICONDUCTOR DEVICES NOT COVERED BY CLASS - Details thereof characterised by the semiconductor bodies with a particular shape, e.g. curved or truncated substrate
  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds

100.

Method for growth of indium-containing nitride films

      
Application Number 13346507
Grant Number 08482104
Status In Force
Filing Date 2012-01-09
First Publication Date 2012-08-09
Grant Date 2013-07-09
Owner SLT TECHNOLOGIES, INC. (USA)
Inventor
  • D'Evelyn, Mark P.
  • Poblenz, Christiane
  • Krames, Michael R.

Abstract

A method for growth of indium-containing nitride films is described, particularly a method for fabricating a gallium, indium, and nitrogen containing material. On a substrate having a surface region a material having a first indium-rich concentration is formed, followed by a second thickness of material having a first indium-poor concentration. Then a third thickness of material having a second indium-rich concentration is added to form a sandwiched structure which is thermally processed to cause formation of well-crystallized, relaxed material within a vicinity of a surface region of the sandwich structure.

IPC Classes  ?

  • H01L 29/20 - Semiconductor bodies characterised by the materials of which they are formed including, apart from doping materials or other impurities, only AIIIBV compounds
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