A method for determining the refractive index profile of a preform when the RIP is not substantially symmetrical. (i) The preform is scanned, starting with a first projection angle, and raw data are created representing the object through measured data. (ii) Optionally, the object is rotated and step (i) repeated iteratively until all projection angles have been scanned and all measured data have been created. (iii) The measured data are processed to form a sinogram and, if the optional step (ii) has been completed, the method proceeds to step (v). (iv) The object is rotated and steps (i) and (iii) are repeated iteratively until all projection angles have been scanned. (v) A 2D RIP is calculated. (vi) A line section of interest is selected within the 2D RIP. (vii) A fitting procedure is applied to the line section of interest. (viii) Finally, refractive index steps/gradients and dimensions are determined.
G01N 21/41 - RefractivityPhase-affecting properties, e.g. optical path length
G01N 21/39 - Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using tunable lasers
G01N 21/88 - Investigating the presence of flaws, defects or contamination
2.
ULTRA LOW-NA REFRACTIVE INDEX PROFILING SYSTEM AND METHOD FOR FILTERING OUT SEVERELY DISTURBING DIFFRACTION EFFECTS
A method for determining a refractive index profile of an optical object having a cylindrical surface includes: (a) scanning the surface at a first plurality of scanning locations with a pinhole aperture in a path of one or more optical beams; (b) measuring a first deflection function based detecting the optical beams after deflection by the optical object for each of the first plurality of scanning locations; (c) scanning the surface at a second plurality of scanning locations where the path of the optical beams is free of the pinhole aperture; (d) measuring a second deflection function based on detecting the optical beams after deflection by the optical object for each of the second plurality of scanning locations; (e) merging at least portions of the first and second deflection functions to obtain a composite deflection function; and (f) calculating the refractive index profile using the composite deflection function.
HERAEUS QUARZGLAS BITTERFELD GMBH & CO. KG (Germany)
Inventor
Ma, Qiulin
Chang, Kai Huei
Schuster, Kay
Lorenz, Michael
Abstract
A process for manufacturing an MCF preform having a center longitudinal axis, a plurality of core rods each positioned in a respective core hole and extending along the axis, and a common cladding covering each of the plurality of core rods. The process includes the following steps. A cylinder is provided which will form the cladding of the preform and may have a center core hole. Peripheral core holes are created in the cylinder extending along the longitudinal axis. Each of a plurality of core rods is inserted into a respective peripheral core hole. The cylinder with the core rods inserted in the respective core holes is heated by exposing the cylinder and core rods to a heating element, thereby integrating the core rods and the cylinder and forming the preform, wherein the position error of the core holes with respect to the diameter of the preform is ≤0.6%.
A process for manufacturing a MCF preform having core rods positioned in core holes and a common cladding covering each of the core rods. A cylinder is provided having an outside diameter of at least about 200 mm which will form the cladding and may have a center core hole. Peripheral core holes are created in the cylinder. Each of a plurality of core rods is inserted into a respective peripheral core hole. The cylinder with the core rods inserted is heated, thereby collapsing the cylinder onto the core rods and forming the preform. A gap between the peripheral core rods and the peripheral holes is maintained during the step of creating the plurality of peripheral core holes in the range of about 0.2 to 4 mm, an average radial temperature gradient is maintained during the step of heating the cylinder between about 0.5 to 4 °K/mm, or both.
A drawing furnace for drawing a glass element includes: a furnace body having an upper end and a lower end. The furnace body includes a top annular plate, an A/C induction coil capable of accepting electrical current and producing an oscillating electronic signal, a cylindrical susceptor capable of producing heat output, a cylindrical quartz beaker, an insulating material disposed between the susceptor and the beaker, and a bottom annular plate housing and supporting at least one of the susceptor, the beaker, and the insulating material. wherein the furnace body comprises a central longitudinal axis; A rotational drive system operably connected to the bottom annular plate by an annular rotation gear system rotates the bottom annular plate along with the susceptor, beaker, and/or insulating material at a frequency between 0.01 to 10 Hz. The electrical current and oscillation frequency determine the heat output of the susceptor.
A process for manufacturing an MCF preform having a center longitudinal axis, a plurality of core rods each positioned in a respective core hole and extending along the axis, and a common cladding covering each of the plurality of core rods. The process includes the following steps. A cylinder is provided which will form the cladding of the preform and may have a center core hole. Peripheral core holes are created in the cylinder extending along the longitudinal axis. Each of a plurality of core rods is inserted into a respective peripheral core hole. The cylinder with the core rods inserted in the respective core holes is heated by exposing the cylinder and core rods to a heating element, thereby integrating the core rods and the cylinder and forming the preform, wherein the position error of the core holes with respect to the diameter of the preform is ≤ 0.6%.
An apparatus for producing large glass preforms with minimal clad to-core waveguide distortion from a glass body having a weight, an outer surface, core rods, and a cladding surrounding and separated from the core rods by a gap. The apparatus includes collars affixed to the top and bottom of the cladding; a spacer upon which the core rods rest; a first unit holding and supporting both the bottom collar and the spacer; a second unit holding and supporting the top collar; and a frame defining a heating zone having a heating element to heat the glass body. The weight of the glass body above and below the molten glass in the heating zone is supported by the first and second units without contacting the outer surface of the glass body.
C03B 37/012 - Manufacture of preforms for drawing fibres or filaments
H04B 10/2507 - Arrangements specific to fibre transmission for the reduction or elimination of distortion or dispersion
G01B 11/08 - Measuring arrangements characterised by the use of optical techniques for measuring diameters
G01B 11/25 - Measuring arrangements characterised by the use of optical techniques for measuring contours or curvatures by projecting a pattern, e.g. moiré fringes, on the object
A method for determining the refractive index profile of a preform when the RIP is not substantially step-index like, (a) The preform deflection function is measured and transformed into a measured RIP. (b) A RI level and radius are assumed for the preform layer being evaluated and a compensation level RIP is calculated, (c) A theoretical deflection function is generated corresponding to the assumed RI level and radius and the generated data are transformed into a fitting RIP. (d) The fitting RIP is compared to the measured RIP and the comparison is evaluated against a predetermined accuracy level for the preform layer being evaluated, (e) Steps (b) and (c) are repeated iteratively until the predetermined accuracy level has been achieved. Steps (b) through (e) are repeated for each preform layer that needs to be compensated. Finally, a measurement artifact compensated refractive index profile is calculated for the preform.
A method for determining the refractive index profile of a preform when the RIP is not substantially step-index like. (a) The preform deflection function is measured and transformed into a measured RIP. (b) A RI level and radius are assumed for the preform layer being evaluated and a compensation level RIP is calculated. (c) A theoretical deflection function is generated corresponding to the assumed RI level and radius and the generated data are transformed into a fitting RIP. (d) The fitting RIP is compared to the measured RIP and the comparison is evaluated against a predetermined accuracy level for the preform layer being evaluated. (e) Steps (b) and (c) are repeated iteratively until the predetermined accuracy level has been achieved. Steps (b) through (e) are repeated for each preform layer that needs to be compensated. Finally, a measurement artifact compensated refractive index profile is calculated for the preform.
To achieve a high degree of precision and an exact positioning of anti-resonant elements in a sufficiently stable and reproducible manner in an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, formation of anti-resonant element precursors includes formation of elongated pressure chambers, each of which adjoins a wall deformable under pressure and heat in the region of target positions of the anti-resonant elements. A section of the deformable wall is caused to protrude in the direction of a cladding tube inner bore, thereby forming an anti-resonant element or a precursor for same, while carrying out a process of elongating a primary preform to form the hollow-core fiber or further processing the primary preform to a secondary preform from which the hollow-core fiber is drawn.
Method of producing glass components and preforms for use in the method. The preform includes a primary rod having a constant outside diameter and a flat bottom portion, wherein the primary rod comprises a core rod surrounded by at least one outer cladding layer; and a cylindrical sacrificial tip having a first end attached to the flat bottom portion of the primary rod, a second end opposite the first end, and a hollow interior region extending fully from the first end to the second end, wherein the sacrificial tip is circular in cross section and the first end of the sacrificial tip has a constant inside diameter and outside diameter along its entire length from the first end to the second end, and wherein the constant outside diameter is equal to the outside diameter of the primary rod. When the preform is heated in a furnace, the sacrificial tip melts and collapses into a drawing bulb which either draws the primary rod directly into the glass fiber or results in a tapered (i.e. tipped) preform for subsequent fiber draw. Material waste as well as the drip time is reduced and the cladding-to-core ratio, crucial for waveguide properties, is maintained for the whole preform compared to a square cut preform without the sacrificial tip.
Methods are known for producing an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, said jacket region comprising multiple anti-resonant elements. The known methods have the steps of: providing a cladding tube that has a cladding tube inner bore and a cladding tube longitudinal axis along which a cladding tube wall extends that is delimited by an interior and an exterior; forming a number of precursors for anti-resonant elements at target positions of the cladding tube wall; and elongating the primary preform in order to form the hollow-core fiber or further processing the primary preform in order to form a secondary preform from which the hollow-core fiber is drawn. The aim of the invention is to achieve a high degree of precision and an exact positioning of the anti-resonant elements in a sufficiently stable and reproducible manner on the basis of the aforementioned methods. This is achieved in that the formation of the anti-resonant element precursors includes the formation of elongated pressure chambers, each of which adjoins a wall that can be deformed under pressure and heat in the region of the target positions of the anti-resonant elements and which cause a section of the deformable wall to protrude in the direction of the cladding tube inner bore under the effect of pressure and heat, thereby forming an anti-resonant element or a precursor for same, while carrying out a process according to step (c).
A variable seal for shielding from contaminants both an object to be heated in, and the heating element of, a high-temperature furnace. The seal has a first support ring and a second support ring separated by a distance. One or more components control the distance between the two support rings. A high-temperature fabric cylinder is attached to the support rings, is located where the object enters or exits the furnace, and surrounds at least a portion of the object. A mechanism engages the approximate center of the fabric cylinder to close the fabric cylinder as the one or more components decrease the distance between the two support rings and to open the fabric cylinder as the one or more components increase the distance between the two support rings, whereby the fabric cylinder continuously contacts the circumference of the object regardless of the diameter of the object.
An apparatus and related process for producing a high-strength weld between two glass components. Chucks clamp and move respective first ends of the glass components toward each other inside an enclosure, where the second ends are heated, softened, and welded together in a weld zone. The enclosure has layers of stacked quartz glass bricks and allows the weld zone to cool slowly and avoid stress. A propane quartz melting torch directs a flame inside the enclosure and toward the second ends as the glass components move toward each other. The flame softens the second ends and creates substantially smooth polished surfaces in the weld zone having an increased hydroxide content. At least 80% of the weld zone has a hydroxide content greater than about 10 ppm average in a 10 μm depth from the surface and the tensile strength of the weld zone is above about 10 MPa.
An automated large outside diameter preform tipping process. A zone of the preform is heated inside a furnace and softened. The preform tip is shaped and the process is controlled by the movement of the glass above and below the heating zone and by sensing the weight of the lower part of the preform, which in effect is a measure of the viscosity of the softened material. Once the correct viscosity is reached, the bottom holder is moved away from the top holder with a non-linear, accelerated velocity profile (derived from the FEM simulation of glass flow) which is precisely programmed and controlled so that the preform tip is optimally shaped (usually short and sharp tipped) with minimum waste and waveguide distortion when drawn into a fiber. The same concept of the non-linear, accelerated velocity profile can also be applied to other tipping processes such as horizontal preform tipping processes.
A variable seal for shielding from contaminants both an object to be heated in, and the heating element of, a high-temperature furnace. The seal has a first support ring and a second support ring separated by a distance. One or more components control the distance between the two support rings. A high-temperature fabric cylinder is attached to the support rings, is located where the object enters or exits the furnace, and surrounds at least a portion of the object. A mechanism engages the approximate center of the fabric cylinder to close the fabric cylinder as the one or more components decrease the distance between the two support rings and to open the fabric cylinder as the one or more components increase the distance between the two support rings, whereby the fabric cylinder continuously contacts the circumference of the object regardless of the diameter of the object.
An apparatus and related process for producing large glass preforms with minimal clad to-core waveguide distortion from a glass body having a weight, an outer surface, core rods, and a cladding surrounding and separated from the core rods by a gap. The apparatus includes collars affixed to the top and bottom of the cladding; a spacer upon which the core rods rest; a first unit holding and supporting both the bottom collar and the spacer; a second unit holding and supporting the top collar; and a frame defining a heating zone having a heating element to heat the glass body. The weight of the glass body above and below the molten glass in the heating zone is supported by the first and second units without contacting the outer surface of the glass body.
C03B 37/012 - Manufacture of preforms for drawing fibres or filaments
H04B 10/2507 - Arrangements specific to fibre transmission for the reduction or elimination of distortion or dispersion
G01B 11/08 - Measuring arrangements characterised by the use of optical techniques for measuring diameters
G01B 11/25 - Measuring arrangements characterised by the use of optical techniques for measuring contours or curvatures by projecting a pattern, e.g. moiré fringes, on the object
Methods for producing glass components and obtainted glass component, e.g. optical fiber preform. A method includes providing a cladding tube (110) with a longitudinal axis including a first and a second bore separated by a chamfered region (114); inserting a spacer (120) into the first bore; inserting a rod (130) into the first bore (116); moving the spacer (120) into the chamfered section (114), causing the spacer (120) to rotate within the chamfered region (114); and rotating the cladding tube (110) into a vertical orientation, whereby the spacer (120) is prevented from entering the second bore (118) and supports the rod (130). Each portion of the chamfered region has a height perpendicular to the longitudinal axis greater than the height of the second bore. The spacer has a length parallel to the longitudinal axis greater than the height of the second bore but less the distance between the deepest point of the bottom of the chamfered region and an intersection of the top of the chamfered region and the first bore.
Apparatus and method for producing elongated glass components with low bow. The apparatus may include a heating element to heat a bulk glass component where a strand may be drawn from the bulk glass component in a downward direction and a gripper device including a clamping element to support the strand while pulling or drawing it from the bulk glass component in a linear motion, and a low-friction mounting element attached to the clamping element which allows translational movement of the clamping element in an x-y plane. The gripper device may further be used to reduce bow in the strand while it is being drawn by moving the clamping element on the mounting element in a direction opposite the direction of any measured transverse acceleration.
A method of forming a glass preform of predetermined length comprises providing a length of glass material to be separated to form a preform length and a remaining length; forming a notch in the glass material; inducing a tensile stress in excess of the tensile strength of the glass in an area adjacent to the notch; and separating the preform length from the remaining length at the notch.
C03B 33/06 - Cutting or splitting glass tubes, rods, or hollow products
C03B 37/012 - Manufacture of preforms for drawing fibres or filaments
C03B 37/014 - Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means
C03B 37/018 - Manufacture of preforms for drawing fibres or filaments made entirely or partially by chemical means by glass deposition on a glass substrate, e.g. by chemical vapour deposition
C03B 33/10 - Glass-cutting tools, e.g. scoring tools
21.
Elongation method and preform for producing an optical glass component
Method of producing glass components and preforms for use in the method. The preform includes a primary rod having a constant outside diameter and a square bottom and a sacrificial tip having a first end attached to the bottom of the primary rod, a second end opposite the first end, and a hollow interior region extending from the first end to the second end. The sacrificial tip is circular in cross section and the first end of the sacrificial tip has an outside diameter equal to the outside diameter of the primary rod. When the preform is heated in a furnace, the sacrificial tip melts and collapses into a drawing bulb which either draws the primary rod directly into the glass fiber or results in a tapered (i.e. tipped) preform for subsequent fiber draw. Material waste as well as the drip time is reduced and the cladding-to-core ratio, crucial for waveguide properties, is maintained for the whole preform compared to a square cut preform without the sacrificial tip.
Methods for preform and tube draw based on controlling forming zone viscosity determined by calculating a holding force exerted by the glass component in the forming zone on the strand being drawn below. The holding force may be calculated by determining a gravitational force applied to the strand and a pulling force applied to the strand by a pulling device, where the holding force is equal to the opposite of the algebraic sum of the gravitational and pulling forces. The holding force may also be calculated by measuring a stress-induced birefringence in the strand at a point between the forming zone and the pulling device, determining an amount of force applied to the strand at the point corresponding to the birefringence, and calculating the holding force by correcting the amount of force for a gravitational effect of the weight of the strand between the forming zone and the point.
G01N 11/06 - Investigating flow properties of materials, e.g. viscosity or plasticityAnalysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture by timing the outflow of a known quantity
G01N 11/02 - Investigating flow properties of materials, e.g. viscosity or plasticityAnalysing materials by determining flow properties by measuring flow of the material
C03B 37/012 - Manufacture of preforms for drawing fibres or filaments
G01N 11/00 - Investigating flow properties of materials, e.g. viscosity or plasticityAnalysing materials by determining flow properties
G01N 11/08 - Investigating flow properties of materials, e.g. viscosity or plasticityAnalysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture by measuring pressure required to produce a known flow
G01N 11/04 - Investigating flow properties of materials, e.g. viscosity or plasticityAnalysing materials by determining flow properties by measuring flow of the material through a restricted passage, e.g. tube, aperture
23.
Methods and apparatus for determining geometric properties of optical fiber preforms
Methods and apparatus for evaluating the geometric properties of optical fiber preforms, which methods include: providing an optical fiber preform having a longitudinal axis, an outer diameter and a circumference; providing a two-dimensional pattern having a length parallel to the longitudinal axis of the preform and a width greater than the outer diameter of the preform; providing an image capturing device disposed such that the preform is aligned between the pattern and the image capturing device; rotating the preform about its longitudinal axis and acquiring a first plurality of images of the pattern viewed through the preform at at least two different points along the circumference of the preform; and determining at least one geometric property of the preform from the first plurality of images.
G01N 21/41 - RefractivityPhase-affecting properties, e.g. optical path length
G01M 11/00 - Testing of optical apparatusTesting structures by optical methods not otherwise provided for
G01B 11/08 - Measuring arrangements characterised by the use of optical techniques for measuring diameters
G01B 11/24 - Measuring arrangements characterised by the use of optical techniques for measuring contours or curvatures
G01B 11/25 - Measuring arrangements characterised by the use of optical techniques for measuring contours or curvatures by projecting a pattern, e.g. moiré fringes, on the object
G01N 21/95 - Investigating the presence of flaws, defects or contamination characterised by the material or shape of the object to be examined
An apparatus and a method for measurement of transparent cylindrical articles during their manufacture in high temperature furnaces having openings for viewing the articles as they pass through the furnace. The cylindrical articles may, for example, be optical fiber preforms which have at least two layers of vitreous material and from which optical fibers are made. Measurement is accomplished using a digital camera with a sensing and digital recording device and a lens, and a processor programmed with an algorithm which analyzes the images recorded by the sensing and digital recording device by eliminating noise, identifying and locating the outer edges of the transparent cylindrical article and calculating measurements of the article including the diameter and the axial center of the article.
A method of manufacturing an optical fiber preform or an optical fiber is provided. The method includes the steps of: (a) providing a glass tube and a glass core rod; (b) inserting the glass core rod into the glass tube to form an assembled body; (c) heating the assembled body to cause the glass tube to collapse on and adhere to the glass core rod; and (d) treating an interface gap between the glass core rod and the glass tube during heating of at least a portion of the assembled body. Treating of the interface gap involves: (i) establishing a vacuum pressure in the interface gap, (ii) increasing a pressure of the interface gap by a treatment gas through the interface gap for a predetermined time, and (iii) re-establishing a vacuum pressure in the interface gap after the predetermined time has elapsed.
