The present invention relates to single-crystal spherical carbon nanoparticles that are single-crystals, are spherical, and have an average particle diameter of 1 nm to 30 nm. The single-crystal spherical carbon nanoparticles of the present invention can generate fluorescence with a high fluorescence quantum efficiency when excited by a light in wide wavelength range from ultraviolet light to visible light, and have fluorescence quantum efficiency of 10% or more compared to conventionally known carbon nanoparticles. The single-crystal spherical carbon nanoparticles can be used for drug delivery, because they do not have toxicities to living organisms that compound semiconductors made of cadmium, selenium, tellurium, and the like have. Furthermore, since the single-crystal spherical carbon nanoparticles are spherical, they can be densely packed as electrode materials for solar cells and secondary ion batteries, and can be used for negative electrode for lithium ion batteries or electrode material for solar cells.
B82Y 40/00 - Fabrication ou traitement des nanostructures
C30B 7/14 - Croissance des monocristaux à partir de solutions en utilisant des solvants liquides à la température ordinaire, p. ex. à partir de solutions aqueuses le matériau à cristalliser étant produit dans la solution par des réactions chimiques
2.
A METHOD OF PRODUCING SINGLE-CRYSTAL SPHERICAL CARBON NANOPARTICLES
The present application is related to a method of producing single-crystal spherical carbon nanoparticles that are single-crystals and spherical. The single-crystal spherical carbon nanoparticles produced by the production method of the present invention can generate fluorescence with high fluorescence quantum efficiency when excited by a light in a wide wavelength range from ultraviolet light to visible light, and have a fluorescence quantum efficiency of 10% or more compared to conventionally known carbon nanoparticles. In addition, The single-crystal spherical carbon nanoparticles produced by the production method of the present invention can be used for drug delivery, because they do not have toxicities to living organisms that compound semiconductors made of cadmium, selenium, tellurium, etc. have. Furthermore, since the single-crystal spherical carbon nanoparticles produced by the production method of the present invention are spherical, they can be densely packed as electrode materials for solar cells and secondary ion batteries, and can be used for a negative electrode for lithium batteries or an electrode material for solar cells.
B82Y 40/00 - Fabrication ou traitement des nanostructures
C09K 11/65 - Substances luminescentes, p. ex. électroluminescentes, chimiluminescentes contenant des substances inorganiques luminescentes contenant du carbone
C30B 7/00 - Croissance des monocristaux à partir de solutions en utilisant des solvants liquides à la température ordinaire, p. ex. à partir de solutions aqueuses
The present disclosure relates to single-crystal spherical silicon nanoparticles which are monocrystalline are spherical and have an average particle diameter of 1 nm to 20 nm as well as a method of producing the same. The single-crystal spherical silicon nanoparticles of the present invention can produce fluorescence at a high fluorescence quantum efficiency upon excitation by light in a wide range of wavelengths from deep ultraviolet light having a wavelength of 200 nm to 300 nm to visible light, and can increase the conventionally known fluorescence quantum efficiency of silicon nanoparticles from around 1% to 10% or more.
C09K 11/59 - Substances luminescentes, p. ex. électroluminescentes, chimiluminescentes contenant des substances inorganiques luminescentes contenant du silicium
C30B 29/60 - Monocristaux ou matériaux polycristallins homogènes de structure déterminée caractérisés par leurs matériaux ou par leur forme caractérisés par la forme
4.
METHOD OF PRODUCING SINGLE-CRYSTAL SPHERICAL SILICON NANOPARTICLES
The present disclosure relates to a method of producing single-crystal spherical silicon nanoparticles which are monocrystalline and spherical and has an average particle diameter of 1 nm to 20 nm. The method includes a step of mixing and reacting a raw material liquid containing silicon halide with a reduction liquid containing an anion of a condensed aromatic compound produced from lithium, sodium or potassium and the condensed aromatic compound. The anion of the condensed aromatic compound is prepared by mixing the lithium, sodium or potassium and the condensed aromatic compound at a temperature of less than 0° C. The single-crystal spherical silicon nanoparticles produced by the method of the present invention can produce fluorescence from blue to red upon excitation by light in a wide range of wavelengths from deep ultraviolet light having a wavelength of 200 nm to 300 nm to visible light, and can increase the conventionally known fluorescence quantum efficiency of silicon nanoparticles from around 1% to 10% or more.
C30B 7/14 - Croissance des monocristaux à partir de solutions en utilisant des solvants liquides à la température ordinaire, p. ex. à partir de solutions aqueuses le matériau à cristalliser étant produit dans la solution par des réactions chimiques
C09K 11/59 - Substances luminescentes, p. ex. électroluminescentes, chimiluminescentes contenant des substances inorganiques luminescentes contenant du silicium
C30B 29/60 - Monocristaux ou matériaux polycristallins homogènes de structure déterminée caractérisés par leurs matériaux ou par leur forme caractérisés par la forme
5.
METHOD FOR CONTINUOUSLY PRODUCING EUTECTIC ALLOY FINE PARTICLES
The present invention addresses the problem of providing a method for continuously producing eutectic alloy fine particles, the method enabling the production of eutectic alloy particles, the particle diameters of which are easily controlled. The present invention provides a method for producing eutectic alloy fine particles that have a particle diameter of 0.1 μm to 50 μm, wherein: a fluid to be processed containing at least a melt of a eutectic alloy, the melt that serves as a dispersoid, and a solvent that serves as a dispersion medium is used; the fluid to be processed is continuously introduced an atomizer which atomizes the fluid to be processed between at least two processing surfaces that are arranged to face each other; the fluid to be processed goes through a dispersion state in which the melt of a eutectic alloy and the solvent are both in a liquid state within the atomizer; and solid eutectic alloy fine particles are obtained by cooling the fluid discharged from the atomizer. With respect to this method for producing eutectic alloy fine particles, the melt of a eutectic alloy is dispersed in the solvent in the form of droplets between the at least two processing surfaces; and the particle diameters of the melt of a eutectic alloy in the form of droplets are controlled by changing the viscosity of the solvent to be introduced between the at least two processing surfaces.
B22F 9/08 - Fabrication des poudres métalliques ou de leurs suspensionsAppareils ou dispositifs spécialement adaptés à cet effet par des procédés physiques à partir d'un matériau liquide par coulée, p. ex. à travers de petits orifices ou dans l'eau, par atomisation ou pulvérisation
A spray dryer with which a fluid that has been subjected to a fluid processing in a spray device can be directly sprayed from the spray device into a drying chamber so that the fluid can be dried, without the need for a dispersion machine for adjusting the dispersion state of a dispersion solution to be sprayed into the drying chamber. The spray dryer includes a spray device. The spray device includes processing surfaces disposed opposing each other, and a rotation mechanism that rotates at least one of the processing surfaces relative to the other. The processing surfaces define a circular flow path through which is passed a fluid to be processed containing a first fluid and a second fluid. The circular flow path includes introduction ports. A first introduction port introduces, at an opening which connects to the circular flow path, the first fluid from the inside of the circular flow path. A second introduction port opens in the middle of the circular flow path, and combines the second fluid with the first fluid which has been constrained into a thin-film fluid by the processing surfaces. The fluid to be processed is subjected to fluid processing between the processing surfaces, and the fluid-treated fluid is sprayed to the outside from between the processing surfaces.
F26B 3/12 - Procédés de séchage d'un matériau solide ou d'objets impliquant l'utilisation de chaleur par convection, c.-à-d. la chaleur étant transférée d'une source de chaleur au matériau ou aux objets à sécher par un gaz ou par une vapeur, p. ex. l'air le gaz ou la vapeur entraînant le matériau ou les objets à sécher sous forme d'une pulvérisation
B01J 2/06 - Procédés ou dispositifs pour la granulation de substances, en généralTraitement de matériaux particulaires leur permettant de s'écouler librement, en général, p. ex. en les rendant hydrophobes par division du produit liquide en gouttelettes, p. ex. par pulvérisation, et solidification des gouttelettes en milieu liquide
F26B 17/28 - Machines ou appareils à mouvement progressif pour le séchage d'un matériau en vrac, à l'état plastique ou sous forme fluidisée, p. ex. granulés, fibres brutes le mouvement étant réalisé par des rouleaux ou des disques avec le matériau passant sur ou entre eux, p. ex. tambour de succion, tamis
A microreactor includes an outer member with a tapered inner peripheral surface, an inner member with a tapered outer peripheral surface, a clearance adjusting unit which enables adjustment of clearance distance L between the tapered inner peripheral surface and the tapered outer peripheral surface by relatively moving the outer member and the inner member in vertical direction. A relative rotation between the outer member and the inner member is restricted, a flow path is compartmentalized between the inner peripheral surface of the outer member and the outer peripheral surface of the inner member, through which an object to be processed is circulating from below to above, a region compartmentalized in the flow path by the tapered inner peripheral surface and the tapered outer peripheral surface functions as the processing region processing the object to be processed, and an apex angles of the taper of the tapered inner peripheral surface and the tapered outer peripheral surface are set to the same angles each other, the apex angles are degrees or more and 120 degrees or less.
A disperser includes an outer member and an inner member located radially inside the outer member. A flow path is formed between the outer member and the inner member, through which fluid flows from one side to the other side in the axial direction. The flow path includes a first region that extends spirally from the one side to the other side and a second region that extends continuously from the first region to the other side. The second region is defined by the tapered inner circumferential surface of the outer member and the tapered outer circumferential surface of the inner member. The tapered inner circumferential surface and the tapered outer circumferential surface are formed such that the angle of one with respect to the other in the axial cross section changes in the middle of the second region, and the second region of the flow path has portions each having a different clearance distance.
B01F 25/442 - Mélangeurs dans lesquels les composants du mélange sont pressés à travers des fentes caractérisés par la position relative des surfaces pendant le fonctionnement
B01F 35/512 - Récipients de mélange caractérisés par des propriétés de surface, p. ex. revêtus ou rugueux
B01F 35/92 - Systèmes de chauffage ou de refroidissement pour chauffer l'extérieur du récipient, p. ex. vestes chauffantes ou brûleurs
A disperser includes an outer member having a tapered inner circumferential surface, an inner member having a tapered outer circumferential surface that faces the tapered inner circumferential surface, and a clearance adjustment part that allows a clearance distance between the tapered inner circumferential surface and the tapered outer circumferential surface to be adjusted by moving the outer member and the inner member relative to each other. A flow path is formed between the inner circumferential surface of the outer member and the outer circumferential surface of the inner member, through which fluid flows from one side to the other side. The flow path includes a dispersion region defined by the tapered inner circumferential surface and the tapered outer circumferential surface. The tapered inner circumferential surface and the tapered outer circumferential surface are formed such that the angle of one with respect to the other in the axial cross section changes in the middle of the dispersion region.
B05B 3/02 - Appareillages de pulvérisation ou d'arrosage avec des éléments de sortie mobiles ou des éléments déflecteurs mobiles avec des éléments rotatifs
10.
METHOD FOR PRODUCING SINGLE-CRYSTAL SPHERICAL SODIUM METAL NANOPARTICLES
The present invention relates to a method for producing sodium metal nanoparticles that are single crystals, are spherical, and have an average particle diameter of 1-300 nm. Single-crystal spherical sodium metal nanoparticles yielded by the production method according to the present invention can generate fluorescence by excitation by ultraviolet light. The single-crystal spherical sodium metal nanoparticles can be used as a reducing agent for various organic substances due to the absence of the toxicity that is exhibited by compound semiconductors formed from cadmium, selenium, tellurium, and so forth. In addition, because they are spherical, the single-crystal spherical sodium metal nanoparticles can be used as a negative electrode for sodium batteries.
B22F 9/24 - Fabrication des poudres métalliques ou de leurs suspensionsAppareils ou dispositifs spécialement adaptés à cet effet par un procédé chimique avec réduction de mélanges métalliques à partir de mélanges métalliques liquides, p. ex. de solutions
The present application provides a method for producing copper particles having an average particle diameter within the range of 1 nm to 1,000 nm, the method being characterized by comprising a step of mixing at least a first fluid and a second fluid to precipitate copper particles, wherein one of the first fluid and the second fluid is a copper raw material solution containing a raw material of the copper particles, the other of the first fluid and the second fluid is a reducing agent solution containing at least one kind of reducing agent, the copper raw material solution contains monovalent copper ions and/or divalent copper ions, and the oxidation-reduction potential of the copper raw material solution is set so that the average particle diameter is achieved. According to this production method, copper particles having a controlled average particle diameter can be supplied easily and stably by using a method suitable for large-scale production without requiring a complex chemical reaction or a heat treatment.
B22F 9/24 - Fabrication des poudres métalliques ou de leurs suspensionsAppareils ou dispositifs spécialement adaptés à cet effet par un procédé chimique avec réduction de mélanges métalliques à partir de mélanges métalliques liquides, p. ex. de solutions
The present application provides a method for producing cerium oxide particles having an average particle diameter within the range of 1-100 nm, the method involving a step for mixing at least a first fluid and a second fluid to precipitate cerium oxide particles, wherein the method is characterized in that one of the first fluid and the second fluid is a cerium oxide raw material liquid at least including trivalent metal ions and/or tetravalent metal ions, the trivalent metal ions and/or tetravalent metal ions include trivalent cerium ions and/or tetravalent cerium ions, the other one of the first fluid and the second fluid is a cerium oxide precipitation solution at least including a basic substance, and the molar ratio between the trivalent metal ions and the tetravalent metal ions is set so as to achieve said average particle diameter. According to this production method, cerium oxide particles with a controlled average particle diameter can be stably supplied in a simple manner using a method suitable for large-scale production without requiring complex chemical reaction or heat treatment.
The present invention relates to a method for producing platinum-supporting single crystal spherical carbon nanoparticles in which platinum particles are supported on the surface of single crystal spherical carbon nanoparticles, wherein the production method comprises: mixing a single crystal spherical carbon nanoparticle raw material solution that contains a halocarbon and a platinum-supporting single crystal spherical carbon nanoparticle reducing solution that contains an anion of the aromatic compound generated from lithium, sodium or potassium and an aromatic compound to produce single crystal spherical carbon nanoparticles; then adding a platinum raw material solution that contains halogenated platinum to the resulting mixture to produce platinum-supporting single crystal spherical carbon nanoparticles. The platinum-supporting single crystal spherical carbon nanoparticles produced by this production method: are not toxic to living bodies; can be densely packed in, inter alia, the electrode materials of solar cells and secondary ion batteries; and can be used as a negative electrode for lithium ion batteries having improved low electrical conductivity, a fuel cell catalyst, and an electrode material for solar cells.
Provided in the present disclosure are: a heat exchanger which can be easily assembled and with which the occurrence of dry out can be prevented and a reduction in an overall heat transfer coefficient can be suppressed; and a method for using a heat exchanger. A heat exchanger 10 of the present disclosure comprises: an outer member 20 having an internal flow passage 24 that permits the flow of a heat medium, and a diameter-expanded inner circumferential surface 21cb that expands in diameter from the bottom toward the top; and an inner member 30 having an internal flow passage 32 that permits the flow of the heat medium, and a diameter-expanded outer circumferential surface 31a that expands in diameter from the bottom toward the top, the inner member being disposed on the inside of the outer member 20. A to-be-treated fluid passage 60 through which a fluid to be treated flows from the bottom to the top is demarcated between the diameter-expanded inner circumferential surface 21cb and the diameter-expanded outer circumferential surface 31a. The to-be-treated fluid passage 60 is formed, by at least one of the diameter-expanded inner circumferential surface 21cb and the diameter-expanded outer circumferential surface 31a, in a shape which circulates around in a spiral manner. Over the diameter-expanded inner circumferential surface 21cb and the diameter-expanded outer circumferential surface 31a, the fluid to be treated is subjected to heat exchange with the heat medium that flows through the internal flow passages 24, 32.
F28D 9/00 - Appareils échangeurs de chaleur comportant des ensembles de canalisations fixes en forme de plaques ou de laminés pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation
F28G 9/00 - Nettoyage par lessivage ou par lavage, p. ex. avec des solvants chimiques
F28G 13/00 - Accessoires ou procédés non couverts par les groupes Combinaisons d'accessoires ou de procédés couverts par les groupes
F28F 19/04 - Prévention de la formation de dépôts ou de la corrosion, p. ex. en utilisant des filtres en utilisant des revêtements, p. ex. des revêtements vitreux ou émaillés de caoutchoucPrévention de la formation de dépôts ou de la corrosion, p. ex. en utilisant des filtres en utilisant des revêtements, p. ex. des revêtements vitreux ou émaillés de matériaux plastiquesPrévention de la formation de dépôts ou de la corrosion, p. ex. en utilisant des filtres en utilisant des revêtements, p. ex. des revêtements vitreux ou émaillés de vernis
F28D 7/02 - Appareils échangeurs de chaleur comportant des ensembles de canalisations tubulaires fixes pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation les canalisations étant enroulées en hélice
The present invention relates to silicon compound coated metal magnesium particles in which at least a part of a surface of the metal magnesium particles is coated with the silicon compound, wherein an average particle diameter of the silicon compound coated metal magnesium particles is 5 nm or more and 500 nm or less, and a thickness of the silicon compound coating is 1 nm or more and 50 nm or less. The silicon compound coated metal magnesium particles of the present invention are easy to handle in the atmosphere, and have excellent oxidation resistance, and further the properties expected of the nano-size metal magnesium particles are improved at a maximum, or the properties are controlled by supplementing the properties.
The present invention relates to single-crystal spherical carbon nanoparticles, each characterized by being a single crystal, being spherical, and having an average particle diameter of 1 nm to 30 nm. Single-crystal spherical carbon nanoparticles according to the present invention can generate fluorescence at a high fluorescence quantum efficiency by means of excitation via light of a wide wavelength range stretching from ultraviolet light to visible light, and can increase the fluorescence quantum efficiency of conventionally known carbon nanoparticles to 10% or higher. Single-crystal spherical carbon nanoparticles according to the present invention are non-toxic to living organisms held by compound semiconductors formed from cadmium, selenium, tellurium, or the like, and can therefore be used in drug delivery. Furthermore, single-crystal spherical carbon nanoparticles according to the present invention are spherical, and therefore can be packed with an electrode material, etc. for solar cells or secondary ion batteries at a high density and can be used as an electrode material for solar cells as well as negative electrodes of lithium-ion batteries.
A microreactor 10 according to the present disclosure comprises: an outer member 11 having a tapered inner peripheral surface 16b; an inner member 12 having a tapered outer peripheral surface 17c; and a clearance adjusting unit 13 that can adjust a clearance distance L between the tapered inner peripheral surface 16b and the tapered outer peripheral surface 17c by moving the outer member 11 and the inner member 12 relative to each other in the vertical direction, wherein: relative rotation between the outer member 11 and the inner member 12 is restricted; a flow path 40 through which an object to be processed flows from down to up is defined between an inner peripheral surface 16 of the outer member 11 and an outer peripheral surface 17 of the inner member 12; in the flow path 40, a region defined by the tapered inner peripheral surface 16b and the tapered outer peripheral surface 17c functions as a processing region 40a for processing the object to be processed; and the apex angles θ1, θ2 of the tapers of the tapered inner peripheral surface 16b and the tapered outer peripheral surface 17c are set to be 5-120 degrees and to be the same angle as each other.
The present invention relates to a method for producing single-crystal spherical carbon nanoparticles that are single-crystal and spherical. The single-crystal spherical carbon nanoparticles produced by the production method according to the present invention can generate fluorescence at a high fluorescence quantum yield through excitation by light in a wide wavelength range from ultraviolet light to visible light and can increase the fluorescence quantum yield of carbon nanoparticles known heretofore to 10% or more. The single-crystal spherical carbon nanoparticles produced by the production method according to the present invention do not have a poisonous character to a living body which a compound semiconductor formed from cadmium, selenium, tellurium, and the like has and hence can be used for drug delivery. Moreover, the single-crystal spherical carbon nanoparticles produced by the production method according to the present invention are spherical, hence enable dense filling of an electrode material of a solar cell and a secondary ion battery and the like, and can be used as a negative electrode of a lithium ion battery and an electrode material for the solar cell.
A disperser 10 according to the present disclosure comprises a cylindrical outside member 11 that has a tapered inner peripheral surface 15b and that extends in the axial direction, an inside member 13 that has a tapered outer peripheral surface 16a facing the tapered inner peripheral surface 15b of the outside member 11 and that is disposed inwardly of the outside member 11 in the radial direction, and a fixation member 12 and a differential screw 14 that can adjust the clearance distance between the tapered inner peripheral surface 15b and the tapered outer peripheral surface 16a by moving the outside member 11 and the inside member 13 relative to each other in the axial direction, wherein: a circulation passage 40 through which a fluid circulates from one side in the axial direction to the other is provided between an inner peripheral surface 15 of the outside member 11 and an outer peripheral surface 16 of the inside member 13; the circulation passage 40 includes a dispersion area 40b which is compartmented by the tapered inner peripheral surface 15b and the tapered outer peripheral surface 16a; and the angle of one of the tapered inner peripheral surface 15b and the tapered outer peripheral surface 16a relative to the other in a cross section in the axial direction changes midway through the dispersion area 40b.
B01F 27/053 - Agitateurs caractérisés par leurs éléments, leurs matériaux ou leurs propriétés mécaniques caractérisés par leurs matériaux
B01F 27/272 - Mélangeurs à système stator-rotor, p. ex. avec des dents ou des cylindres s’engrenant les uns dans les autres ou ayant des orifices avec des moyens pour déplacer les matières à mélanger axialement entre les surfaces du rotor et du stator, p. ex. le système stator-rotor formé par des surfaces coniques ou cylindriques
B01F 27/94 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des cylindres ou des cônes rotatifs
B01F 35/512 - Récipients de mélange caractérisés par des propriétés de surface, p. ex. revêtus ou rugueux
B01F 35/92 - Systèmes de chauffage ou de refroidissement pour chauffer l'extérieur du récipient, p. ex. vestes chauffantes ou brûleurs
B01F 35/95 - Systèmes de chauffage ou de refroidissement utilisant des agitateurs chauffés ou refroidis
Provided are a disperser and a method for using the same with which it is possible to produce microparticles, in particular nanoparticles, by efficiently giving shear force to an object to be processed with low power. A disperser 10 according to the present disclosure comprises an outer member 11 and an inner member 12 disposed radially inside the outer member 11. Between the outer member 11 and the inner member 12, a flow path 30 is provided through which fluid flows from one side to the other side in an axial direction. The flow path 30 includes a first region that circles spirally from the one side to the other side, and a second region continuous from the first region to the other side. The second region is defined by a tapered inner circumferential surface 13c of the outer member 11 and a tapered outer circumferential surface 21c of the inner member 12. With respect to one of the tapered inner circumferential surface 13c and the tapered outer circumferential surface 21c, the angle of the other in a cross section in the axial direction is set to a different angle in the middle of the second region 30c, whereby a region with a different clearance distance is provided in the second region of the flow path 30.
B01F 27/053 - Agitateurs caractérisés par leurs éléments, leurs matériaux ou leurs propriétés mécaniques caractérisés par leurs matériaux
B01F 27/272 - Mélangeurs à système stator-rotor, p. ex. avec des dents ou des cylindres s’engrenant les uns dans les autres ou ayant des orifices avec des moyens pour déplacer les matières à mélanger axialement entre les surfaces du rotor et du stator, p. ex. le système stator-rotor formé par des surfaces coniques ou cylindriques
B01F 27/94 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des cylindres ou des cônes rotatifs
The present invention relates to single-crystal spherical silicon nanoparticles, characterized by being a single crystal, being spherical, and having an average particle diameter of 1-20 nm, and to a method for producing the same. The single-crystal spherical silicon nanoparticles according to the present invention can generate fluorescence at high fluorescence quantum efficiency by excitation by light of a wide wavelength range from deep ultraviolet light of 200-300 nm to visible light and make it possible to increase the fluorescence quantum efficiency of silicon nanoparticles known to date from about 1% to 10% or more.
C01B 33/18 - Préparation de silice finement divisée ni sous forme de sol ni sous forme de gelPost-traitement de cette silice
B82B 1/00 - Nanostructures formées par manipulation d’atomes ou de molécules, ou d’ensembles limités d’atomes ou de molécules un à un comme des unités individuelles
B82Y 20/00 - Nano-optique, p. ex. optique quantique ou cristaux photoniques
C09K 11/59 - Substances luminescentes, p. ex. électroluminescentes, chimiluminescentes contenant des substances inorganiques luminescentes contenant du silicium
H01L 33/06 - DISPOSITIFS À SEMI-CONDUCTEURS NON COUVERTS PAR LA CLASSE - Détails caractérisés par les corps semi-conducteurs ayant une structure à effet quantique ou un superréseau, p.ex. jonction tunnel au sein de la région électroluminescente, p.ex. structure de confinement quantique ou barrière tunnel
H01L 33/34 - Matériaux de la région électroluminescente contenant uniquement des éléments du groupe IV de la classification périodique
22.
MANUFACTURING METHOD FOR SINGLE CRYSTAL SPHERICAL SILICON NANOPARTICLES
The present invention is a manufacturing method for single crystal spherical silicon nanoparticles that are single crystals, are spherical, and have an average particle diameter of 1 nm to 20 nm. The manufacturing method includes a step for mixing and reacting the following: a raw material solution containing halogenated silicon; and a reducing solution containing anions of a condensed aromatic compound generated from the condensed aromatic compound and lithium, sodium, or potassium. The anions of the condensed aromatic compound are prepared by mixing the lithium, sodium, or potassium with the condensed aromatic compound at a temperature below 0°C. The single crystal spherical silicon nanoparticles manufactured by using the manufacturing method of the present invention make it possible to generate red fluorescence from blue fluorescence due to excitation by using wide wavelength light that ranges from deep ultraviolet light of 200 nm to 300 nm to visible light, and make it possible to increase the fluorescence quantum efficiency of previously known silicon nanoparticles from around 1% to at least 10%.
B82B 3/00 - Fabrication ou traitement des nanostructures par manipulation d’atomes ou de molécules, ou d’ensembles limités d’atomes ou de molécules un à un comme des unités individuelles
C01B 33/023 - Préparation par réduction de silice ou d'un matériau contenant de la silice
C09K 11/59 - Substances luminescentes, p. ex. électroluminescentes, chimiluminescentes contenant des substances inorganiques luminescentes contenant du silicium
B82Y 20/00 - Nano-optique, p. ex. optique quantique ou cristaux photoniques
H01L 31/0352 - Dispositifs à semi-conducteurs sensibles aux rayons infrarouges, à la lumière, au rayonnement électromagnétique d'ondes plus courtes, ou au rayonnement corpusculaire, et spécialement adaptés, soit comme convertisseurs de l'énergie dudit rayonnement e; Procédés ou appareils spécialement adaptés à la fabrication ou au traitement de ces dispositifs ou de leurs parties constitutives; Leurs détails caractérisés par leurs corps semi-conducteurs caractérisés par leur forme ou par les formes, les dimensions relatives ou la disposition des régions semi-conductrices
H01L 33/06 - DISPOSITIFS À SEMI-CONDUCTEURS NON COUVERTS PAR LA CLASSE - Détails caractérisés par les corps semi-conducteurs ayant une structure à effet quantique ou un superréseau, p.ex. jonction tunnel au sein de la région électroluminescente, p.ex. structure de confinement quantique ou barrière tunnel
H01L 33/34 - Matériaux de la région électroluminescente contenant uniquement des éléments du groupe IV de la classification périodique
In a coloring ultraviolet protective agent, the average molar absorption coefficient in the wavelength range from 200 nm to 380 nm is increased, and the color characteristics in the visible region are controlled. The coloring ultraviolet protective agent is useful for shielding ultraviolet rays and coloring. The coloring ultraviolet protective agent comprises M2 doped oxide particles in which oxide particles (M1Ox) including at least M1 being a metal element or metalloid element, are doped with at least one M2 selected from metal elements or metalloid elements other than M1, wherein x is an arbitrary positive number, wherein an average molar absorption coefficient in the wavelength range of 200 nm to 380 nm of a dispersion in which the M2 doped oxide particles are dispersed in a dispersion medium, is improved as compared with one of a dispersion in which the oxide particles (M1Ox) are dispersed in a dispersion medium, and wherein a hue or chroma of color characteristics in the visible region of the M2 doped oxide particles is controlled.
The present application provides a microsphere comprising a lactic acid-glycolic acid copolymer (PLGA) as a main component, in which a biologically active substance is uniformly dispersed, wherein an average volume-based particle diameter of the microsphere is 1 μm or more and 150 μm or less, and a mass of the biologically active substance or an empty hole of 1.5 μm or more is not present in the microsphere. The microsphere of the present invention can appropriately control the initial release amount of the biologically active substance and its release rate during a subsequent release period, and can continuously release the biologically active substance in vivo for a predetermined period of time.
A heat exchanger includes three flow paths, a first flow path, a second flow path, and a third flow path, which turn spirally in the space formed between an inner cylinder and an outer cylinder are provided. These flow paths are defined by an inner heat transfer body and an outer heat transfer body, and heat exchange is performed through the heat transfer bodies. The heat transfer bodies turn spirally, have a screw shape in an axial cross-sectional view, and are assembled into a screw shape. The flow path area of the first flow path is varied by changing the shapes of a male thread and a female thread, and the second flow path and the third flow path are formed in a spiral shape, allowing for exchange of heat through the heat transfer bodies.
F28D 7/02 - Appareils échangeurs de chaleur comportant des ensembles de canalisations tubulaires fixes pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation les canalisations étant enroulées en hélice
F28D 7/10 - Appareils échangeurs de chaleur comportant des ensembles de canalisations tubulaires fixes pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation les canalisations étant disposées l'une dans l'autre, p. ex. concentriquement
F28F 19/02 - Prévention de la formation de dépôts ou de la corrosion, p. ex. en utilisant des filtres en utilisant des revêtements, p. ex. des revêtements vitreux ou émaillés
26.
METHOD FOR CONTINUOUSLY PRODUCING EUTECTIC ALLOY FINE PARTICLES
The present invention addresses the problem of providing a method for continuously producing eutectic alloy fine particles, the method enabling the production of eutectic alloy particles, the particle diameters of which are easily controlled. The present invention provides a method for producing eutectic alloy fine particles that have a particle diameter of 0.1 µm to 50 µm, wherein: a fluid to be processed containing at least a melt of an eutectic alloy, the melt serving as a dispersoid, and a solvent that serves as a dispersion medium is used; the fluid to be processed is continuously introduced into an atomizer which atomizes the fluid to be processed between at least two processing surfaces that are arranged to face each other; the fluid to be processed goes through a dispersion state in which the melt of an eutectic alloy and the solvent are both in a liquid state within the atomizer; and solid eutectic alloy fine particles are obtained by cooling the fluid discharged from the atomizer. With respect to this method for producing eutectic alloy fine particles, the melt of an eutectic alloy is dispersed in the solvent in the form of droplets between the at least two processing surfaces; and the particle diameters of the melt of an eutectic alloy in the form of droplets are controlled by changing the viscosity of the solvent to be introduced between the at least two processing surfaces.
B22F 9/08 - Fabrication des poudres métalliques ou de leurs suspensionsAppareils ou dispositifs spécialement adaptés à cet effet par des procédés physiques à partir d'un matériau liquide par coulée, p. ex. à travers de petits orifices ou dans l'eau, par atomisation ou pulvérisation
Provided is a spray dryer with which a fluid that has been subjected to a fluid treatment in a spray device can be directly sprayed from the spray device into a drying chamber so that the fluid can be dried, without the need for a dispersion machine for adjusting the dispersion state of a dispersion liquid to be sprayed into the drying chamber. The spray dryer comprises a spray device F. The spray device F comprises processing surfaces 1, 2 disposed opposing each other, and a rotation mechanism M that rotates at least one of the processing surfaces 1, 2 relative to the other. The processing surfaces 1, 2 define an annular flow passage 3 through which is passed a fluid to be treated containing a first fluid and a second fluid. The annular flow passage 3 comprises introduction ports d1, d2. The introduction port d1 introduces, at an opening which connects to the annular flow passage 3, the first fluid from the inside of the annular flow passage 3. The introduction port d2 opens in the middle of the annular flow passage 3, and combines the second fluid with the first fluid which has been constrained into a thin-film fluid by the processing surfaces 1, 2. The fluid to be treated is subjected to fluid processing between the processing surfaces 1, 2, and the fluid-treated fluid is sprayed to the outside from between the processing surfaces 1, 2.
F26B 3/24 - Procédés de séchage d'un matériau solide ou d'objets impliquant l'utilisation de chaleur par conduction, c.-à-d. la chaleur étant transférée de la source de chaleur, p. ex. une flamme de gaz, au matériau ou aux objets à sécher par contact direct la source de chaleur, le matériau ou les objets à sécher étant animés d'un mouvement relatif, p. ex. de vibration le mouvement étant une rotation
F26B 17/28 - Machines ou appareils à mouvement progressif pour le séchage d'un matériau en vrac, à l'état plastique ou sous forme fluidisée, p. ex. granulés, fibres brutes le mouvement étant réalisé par des rouleaux ou des disques avec le matériau passant sur ou entre eux, p. ex. tambour de succion, tamis
B01J 2/02 - Procédés ou dispositifs pour la granulation de substances, en généralTraitement de matériaux particulaires leur permettant de s'écouler librement, en général, p. ex. en les rendant hydrophobes par division du produit liquide en gouttelettes, p. ex. par pulvérisation, et solidification des gouttelettes
28.
METHOD FOR PRODUCING ORGANIC MATERIAL MICROPARTICLES, AND METHOD FOR MODIFYING ORGANIC MATERIAL MICROPARTICLES
Provided are a method for producing organic material microparticles and a method for modifying organic material microparticles, whereby it becomes possible to improve the crystallinity of organic material microparticles or achieve the crystal transformation of the organic material microparticles while preventing the growth of the organic material microparticles in a solvent. A surfactant is added to a solvent that is capable of partially dissolving organic material microparticles, and then the organic material microparticles are reacted with the solvent. In this manner, it becomes possible to improve the degree of crystallization of the organic material microparticles or achieve the crystal transformation of the organic material microparticles without substantially altering the particle diameters of the organic material microparticles.
A61K 31/405 - Acides indole-alkanecarboxyliquesLeurs dérivés, p. ex. tryptophane, indométhacine
A61K 31/5383 - 1,4-Oxazines, p. ex. morpholine condensées en ortho ou en péri avec des systèmes hétérocycliques
B01J 19/00 - Procédés chimiques, physiques ou physico-chimiques en généralAppareils appropriés
C09B 67/00 - Traitements, sans réaction chimique, influençant les propriétés physiques, p. ex. de teintures ou d'impression, des matières colorantes, p. ex. traitement par des solvantsCaractéristiques du procédé de fabrication des préparations tinctorialesPréparations tinctoriales ayant un aspect physique particulier, p. ex. tablettes, feuilles
29.
MAIN AGENT UNIFORMLY DISPERSED MICROSPHERE AND A SUSTAINED RELEASE FORMULATION COMPRISING THE SAME
The present application provides a microsphere in which a main agent is uniformly dispersed in a polymer matrix, wherein an average volume-based particle diameter of the microsphere is 1 μm or more and 150 μm or less, and a variation coefficient of area ratios in four regions is 0.35 or less, wherein the area ratios in four regions are calculated by (s/A)×100 (%) wherein the four regions are prepared by preparing a cross section observation sample obtained by cutting the microsphere; observing the cross section observation sample with an electron microscope at a magnification capable of confirming the main agent in the microsphere or a higher magnification; and dividing the electron microscope observation image into four regions; and A is an area of a respective divided region, and s is a sum of cross section areas of the main agent included in the respective divided region. The microsphere of the present invention can appropriately control the initial release amount of the main agent and its release rate during a subsequent release period, and can continuously release the main agent for a predetermined period of time.
A61K 31/7048 - Composés ayant des radicaux saccharide et des hétérocycles ayant l'oxygène comme hétéro-atome d'un cycle, p. ex. leucoglucosane, hespéridine, érythromycine, nystatine
A61K 31/496 - Pipérazines non condensées contenant d'autres hétérocycles, p. ex. rifampine, thiothixène ou sparfloxacine
A61K 31/57 - Composés contenant des systèmes cycliques du cyclopenta[a]hydrophénanthrèneLeurs dérivés, p. ex. stéroïdes substitués en position 17 bêta par une chaîne à deux atomes de carbone, p. ex. prégnane ou progestérone
The flow reactor includes three flow passages including a first flow passage, a second flow passage, and a third flow passage which spirally circulate within a space formed between an inner tube and an outer tube. The flow passages are compartmented by an inner heat transfer body and an outer heat transfer body. The heat transfer bodies spirally circulate, have a screw-like cross-sectional shape in an axial cross-sectional view, and are assembled in a screw-like configuration. By changing the shapes of a male-thread portion and a female-thread portion, the flow passage area of the first flow passage is changed, the second flow passage and the third flow passage are spirally formed, and heat exchange and reaction take place through the heat transfer bodies.
F28D 7/00 - Appareils échangeurs de chaleur comportant des ensembles de canalisations tubulaires fixes pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation
F28D 7/16 - Appareils échangeurs de chaleur comportant des ensembles de canalisations tubulaires fixes pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation les canalisations étant espacées parallèlement
F28D 21/00 - Appareils échangeurs de chaleur non couverts par l'un des groupes
F28F 19/04 - Prévention de la formation de dépôts ou de la corrosion, p. ex. en utilisant des filtres en utilisant des revêtements, p. ex. des revêtements vitreux ou émaillés de caoutchoucPrévention de la formation de dépôts ou de la corrosion, p. ex. en utilisant des filtres en utilisant des revêtements, p. ex. des revêtements vitreux ou émaillés de matériaux plastiquesPrévention de la formation de dépôts ou de la corrosion, p. ex. en utilisant des filtres en utilisant des revêtements, p. ex. des revêtements vitreux ou émaillés de vernis
A heat exchanger with which a fluid to be treated or a generated gas can be prevented from stagnating in a heat transfer part, which can be disassembled for good washability, and which can be coated or lined. The heat exchanger is provided with tow flow passages, i.e. a first flow passage and a second flow passage, within a space formed between an inner tube and an outer tube which are concentric to each other. A spiral heat transfer body is disposed between the inner tube and the outer tube, and the spiral heat transfer body has a cross-sectional shape that is substantially triangular in the axial-direction cross section. The space is partitioned into the first flow passage and the second flow passage by the spiral heat transfer body, and heat is exchanged via the spiral heat transfer body between a first fluid flowing within the first flow passage and a fluid flowing within the second flow passage.
F28D 7/02 - Appareils échangeurs de chaleur comportant des ensembles de canalisations tubulaires fixes pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation les canalisations étant enroulées en hélice
F28F 9/00 - CartersBoîtes de distributionSupports auxiliaires pour les élémentsÉléments auxiliaires dans les carters
F28F 19/02 - Prévention de la formation de dépôts ou de la corrosion, p. ex. en utilisant des filtres en utilisant des revêtements, p. ex. des revêtements vitreux ou émaillés
A flow reactor can promote a reaction under appropriate temperature management, can precent reaction fluid or generated gas from being trapped in a heat transmission part, can be disassembled for easy cleaning, and to which a coating or lining can be applied. This flow reactor is provided with two flow paths, a reaction flow path and a second flow path, in a space formed between an inner cylinder and an outer cylinder that are concentric. A spiral heat transmission body is disposed between the inner cylinder and the outer cylinder, and the spiral heat transmission body has a substantially triangular cross-sectional shape in an axial cross-sectional view. The spiral heat transmission body partitions the space into the reaction flow path and the second flow path, and heat is exchanged via the spiral heat transmission body between a reaction fluid F1 flowing through the reaction flow path and a heat medium F2 flowing through the second flow path.
B01J 19/24 - Réacteurs fixes sans élément interne mobile
B01J 19/00 - Procédés chimiques, physiques ou physico-chimiques en généralAppareils appropriés
F28D 7/10 - Appareils échangeurs de chaleur comportant des ensembles de canalisations tubulaires fixes pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation les canalisations étant disposées l'une dans l'autre, p. ex. concentriquement
A method of producing silver fine particles includes continuously reducing silver ions contained in a silver compound to precipitate silver fine particles by introducing at least two fluids from separate flow paths and mixing the fluids, wherein one fluid of the at least two fluids contains the silver compound, and another fluid contains a reducing agent, and at least one fluid of the at least two fluids contains an amino acid. With this method, silver fine particles can be produced with sufficient continuous productivity and quality uniformity, without problems of deterioration of working environment and generation of explosive fulminating silver due to the use of a large amount of ammonia.
B22F 9/24 - Fabrication des poudres métalliques ou de leurs suspensionsAppareils ou dispositifs spécialement adaptés à cet effet par un procédé chimique avec réduction de mélanges métalliques à partir de mélanges métalliques liquides, p. ex. de solutions
B22F 1/107 - Poudres métalliques contenant des agents lubrifiants ou liantsPoudres métalliques contenant des matières organiques contenant des matériaux organiques comportant des solvants, p. ex. pour la coulée en moule poreux ou absorbant
The present invention relates to silicon-compound-coated metal magnesium particles in which the surfaces of nano-size metal magnesium particles are at least partially coated with a silicon compound, the silicon-compound-coated metal magnesium particles being characterized in that the average particle diameter thereof is 5-500 nm, and the thickness of the silicon compound coating is 1-50 nm. These silicon-compound-coated metal magnesium particles are easily handled in air and have excellent oxidation resistance, and the characteristics expected of nano-size metal magnesium particles are maximally improved, or the characteristics are supplemented and controlled.
B22F 1/02 - Traitement particulier des poudres métalliques, p.ex. en vue de faciliter leur mise en œuvre, d'améliorer leurs propriétés; Poudres métalliques en soi, p.ex. mélanges de particules de compositions différentes comportant un enrobage des particules
B22F 1/00 - Poudres métalliquesTraitement des poudres métalliques, p. ex. en vue de faciliter leur mise en œuvre ou d'améliorer leurs propriétés
B22F 9/00 - Fabrication des poudres métalliques ou de leurs suspensionsAppareils ou dispositifs spécialement adaptés à cet effet
In an agitator in which cavitation arising during treatment of a fluid being treated is suppressed, a stator part S is provided with a plurality of penetration parts in the circumferential direction of the stator part S, and a stator main part positioned between adjacent penetration parts. When a fluid is discharged from the inside of the stator part S to the outside through the penetration part by the rotation of a rotor, in the stator part S for the agitator treating the fluid, the side facing a blade of the rotor is an inner wall surface, the side facing a blade of the rotor is an inner wall surface, the side facing the side opposite to the blade of the rotor is an outer wall surface, an opening of the plurality of penetration parts that is provided in the inner wall surface is an inflow opening, and an opening of the plurality of penetration parts that is provided in the outer wall surface is an outflow opening, the opening area of the inflow opening being larger than the opening are of the outflow opening.
B01F 27/00 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins
B01F 27/271 - Mélangeurs à système stator-rotor, p. ex. avec des dents ou des cylindres s’engrenant les uns dans les autres ou ayant des orifices avec des moyens pour déplacer les matières à mélanger radialement entre les surfaces du rotor et du stator
36.
Black perylene pigment microparticles, method of producing the same, black pigment composition comprising the same, and method of producing black perylene pigment microparticles having controlled hue and/or chroma
The present application provides black perylene pigment microparticles having an average circularity of 0.8 or more which are amorphous; and a method of producing the black perylene pigment microparticles, which comprises a step of mixing a pigment solution in which a black perylene pigment is dissolved and a precipitation solvent for precipitating black perylene pigment microparticles from the pigment solution to form black perylene pigment microparticles, wherein at least one of the pigment solution and the precipitation solvent independently includes a salt of an alkaline earth metal and/or a particle growth inhibitor. The present invention can provide black perylene pigment microparticles having good dispersibility, high concealability and light-shielding property and controlled hue and chroma, and a method of easily producing the same, and the like.
A vacuum deaerator is provided with a refining device with which it is possible to suppress the occurrence of situations involving interrupted discharging and continuously discharge a material being treated that is highly viscous, etc. The vacuum deaerator introduces a liquid material being treated into a vessel having a vacuum therein to perform deaeration and then discharged the material being treated out of the vessel. A rotating rotor with refining device arranged in the vessel and a rotating discharge vane provided separately from the rotating rotor for the purpose of discharging the material being treated in the vessel out of the vessel are installed.
An agitator is capable of more efficiently applying a shear force to a treatment target fluid through the action of an intermittent jet flow. The agitator includes a rotor which includes blade, and a screen concentric therewith, the rotation of at least the rotor causing a treatment target fluid to pass through slits in the screen to become an intermittent get stream, which is discharged from inside the screen to the outside thereof, wherein the agitator is characterized in that: the screen has a cylindrical shape with a circular cross section; openings of the slits provided in an inner surface of the screen constitute flow intake openings; openings of the slits provided in an outer surface of the screen constitute flow discharge openings; spaces between the flow intake openings and the flow discharge openings constitute slit space; and the circumferential-directional width (So) of the flow discharge openings and the circumferential-directional width (Si) of the flow intake openings are greater than the circumferential-directional width (Sm) of the slit spaces.
B01F 27/921 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des hélices ou des vis avec des hélices montées centralement dans le récipient
B01F 27/84 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec plusieurs agitateurs tournant à des vitesses différentes ou dans des directions opposées autour du même axe
B01F 27/91 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des hélices
39.
Method of producing a microsphere comprising PLGA or PLA in which a biologically active substance is uniformly dispersed
The present application provides a microsphere comprising a lactic acid-glycolic acid copolymer (PLGA) or polylactide (PLA) as a main component, in which a biologically active substance is uniformly dispersed, wherein an average volume-based particle diameter of the microsphere is 1 μm or more and 150 μm or less, and a variation coefficient of area ratios in six regions is 0.35 or less, wherein the area ratios in six regions are calculated by (s/A)×100 (%) wherein the six regions are prepared by preparing a cross section observation sample obtained by cutting the microsphere; observing the cross section observation sample with an electron microscope at a magnification capable of confirming the biologically active substance in the microsphere or a higher magnification; and dividing the electron microscope observation image into six regions; and A is an area of a respective divided region, and s is a sum of cross section areas of the biologically active substance included in the respective divided region. The microsphere of the present invention can appropriately control the initial release amount of the biologically active substance and its release rate during a subsequent release period, and can continuously release the biologically active substance in vivo for a predetermined period of time.
A vacuum deaerator degasses material to be processed by placing a rotating rotor with a screen in a vacuum vessel, introducing a liquid material to be processed into the rotor from the interior thereof and causing the liquid to pass through the screen to refine the same. The vacuum deaerator is characterized in that: the screen is a cylinder with a circular cross-section and is in the form of a porous plate in which a plurality of through holes are opened in the radial direction of the cylindrical screen; and the screen is provided such that the area of inflow openings is greater than the area of outflow openings, where the inflow openings are openings of a plurality of penetration portions provided on the inner wall face of the screen and the outflow openings are openings of the plurality of penetration portions provided on the outer wall dace of the screen. Thus, the processing capacity of the vacuum deaerator is improved without increasing the size of the device.
B01F 25/45 - Mélangeurs dans lesquels les composants du mélange sont pressés ensemble au travers d’orifices ou d’espaces interstitiels, p. ex. entre des perles
B01F 25/452 - Mélangeurs dans lesquels les composants du mélange sont pressés ensemble au travers d’orifices ou d’espaces interstitiels, p. ex. entre des perles caractérisés par des éléments pourvus d'orifices ou d'espaces interstitiels
B01F 27/81 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical les agitateurs ayant des entrées de flux axiales centrales et des sorties de flux sensiblement radiales
B01F 27/91 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des hélices
B01F 27/92 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des hélices ou des vis
B01F 27/921 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des hélices ou des vis avec des hélices montées centralement dans le récipient
41.
PLGA microparticles, a sustained release formulation thereof and a production method thereof
Approximately spherical lactic acid-glycolic acid copolymer (PLGA) microparticles include a biologically active substance. An average volume-based particle diameter of the PLGA microparticles is 1 μm or more and 150 μm or less. A Reactive Span Factor (R.S.F.) of the PLGA microparticles is satisfied with formula (1): 0.1<(R.S.F.)≤1.7 formula (1), wherein an R.S.F. means (D90−D10)/D50; D90 is a particle diameter (μm) corresponding to the cumulative 90% by volume of the cumulative particle diameter distribution from the small particle side; D50 is a particle diameter (μm) corresponding to the cumulative 50% by volume of the cumulative particle diameter distribution from the small particle side; and D10 is a particle diameter (μm) corresponding to the cumulative 10% by volume of the cumulative particle diameter distribution from the small particle side.
A61K 47/34 - Composés macromoléculaires obtenus par des réactions autres que celles faisant intervenir uniquement des liaisons non saturées carbone-carbone, p. ex. polyesters, acides polyaminés, polysiloxanes, polyphosphazines, copolymères de polyalkylène glycol ou de poloxamères
The present invention relates to silicon coated metal microparticles in which at least a part of a surface of a metal microparticle composed of at least one of metal elements or metalloid elements is coated with silicon, wherein the silicon coated metal microparticles are a product obtained by a reduction treatment of silicon compound coated precursor microparticles in which at least a part of a surface of a precursor microparticle containing a precursor of the metal microparticles is coated with a silicon compound, or silicon doped precursor microparticles containing a precursor of the metal microparticles. Because it is possible particularly to strictly control a particle diameter of the silicon compound coated metal microparticle by controlling conditions of the reduction treatment, design of a more appropriate composition can become facilitated, compared with a conventional composition, in terms of diversified usages and desired properties of silicon compound coated metal microparticles.
A fluid treatment device with a new configuration is provided. The fluid treatment device is provided with an upstream treatment unit defined by treatment surfaces that rotate relative to each other, and a downstream treatment unit arranged downstream of the upstream treatment unit. The upstream treatment unit is configured such that, by passing the fluid to be treated into an upstream treatment space defined by the treatment surfaces, the fluid to be treated is subjected to upstream treatment. The downstream treatment unit is provided with a downstream treatment space which performs the function of retaining and mixing the fluid to be treated by means of a labyrinth seal. An upstream outlet of the fluid to be treated from the upstream treatment unit opens into the downstream treatment space, and the downstream treatment space is configured to use the labyrinth seal to perform the function of controlling retention time. The downstream treatment space is provided with narrow seal spaces, and retention spaces arranged upstream of the seal spaces and wider than the seal spaces, and the upstream outlet opens to a retention space.
B01F 35/92 - Systèmes de chauffage ou de refroidissement pour chauffer l'extérieur du récipient, p. ex. vestes chauffantes ou brûleurs
B01F 27/271 - Mélangeurs à système stator-rotor, p. ex. avec des dents ou des cylindres s’engrenant les uns dans les autres ou ayant des orifices avec des moyens pour déplacer les matières à mélanger radialement entre les surfaces du rotor et du stator
B01F 27/272 - Mélangeurs à système stator-rotor, p. ex. avec des dents ou des cylindres s’engrenant les uns dans les autres ou ayant des orifices avec des moyens pour déplacer les matières à mélanger axialement entre les surfaces du rotor et du stator, p. ex. le système stator-rotor formé par des surfaces coniques ou cylindriques
B01F 27/93 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des disques rotatifs
B01J 19/00 - Procédés chimiques, physiques ou physico-chimiques en généralAppareils appropriés
B01J 19/12 - Procédés utilisant l'application directe de l'énergie ondulatoire ou électrique, ou un rayonnement particulaireAppareils à cet usage utilisant des radiations électromagnétiques
B01J 19/18 - Réacteurs fixes avec éléments internes mobiles
B01J 19/20 - Réacteurs fixes avec éléments internes mobiles en forme d'hélice, p. ex. réacteurs à vis
B01F 101/00 - Mélange caractérisé par la nature des matières mélangées ou par le domaine d'application
Provided is a method for producing an organic compound, the method making it possible to ensure an adequate reaction time and obtain a targeted substance at a high yield even in an organic reaction that requires a relatively long time to complete the reaction. A method for producing an organic compound, wherein the method is characterized in that: a fluid processing apparatus F used in the production method is equipped with an upstream processing unit that processes a fluid to be processed between at least two processing surfaces 1 and 2 that relatively rotate, and a downstream processing unit disposed downstream of the upstream processing unit, the downstream processing unit being provided with a plurality of labyrinth seals that function to retain and stir the fluid to be processed that has been processed by the upstream processing unit; due to the fluid to be processed, which contains at least one type of organic compound, being passed through the upstream processing unit, the fluid to be processed is subjected to upstream processing; due to the fluid to be processed that has been subjected to upstream processing being passed through the downstream processing unit, the fluid to be processed that has been subjected to upstream processing is subjected to downstream processing; and the upstream processing and the downstream processing are performed continuously.
C07D 317/00 - Composés hétérocycliques contenant des cycles à cinq chaînons comportant deux atomes d'oxygène comme uniques hétéro-atomes du cycle
B01J 19/00 - Procédés chimiques, physiques ou physico-chimiques en généralAppareils appropriés
B01J 19/18 - Réacteurs fixes avec éléments internes mobiles
C07C 51/377 - Préparation d'acides carboxyliques, de leurs sels, halogénures ou anhydrides par des réactions ne créant pas de groupes carboxyle par élimination d'hydrogène ou de groupes fonctionnelsPréparation d'acides carboxyliques, de leurs sels, halogénures ou anhydrides par des réactions ne créant pas de groupes carboxyle par hydrogénolyse de groupes fonctionnels
C07C 67/08 - Préparation d'esters d'acides carboxyliques par réaction d'acides carboxyliques ou d'anhydrides symétriques avec le groupe hydroxyle ou O-métal de composés organiques
C07C 67/343 - Préparation d'esters d'acides carboxyliques par modification de la partie acide de l'ester sans introduction d'un groupe ester par isomérisationPréparation d'esters d'acides carboxyliques par modification de la partie acide de l'ester sans introduction d'un groupe ester par modification de la taille du squelette carboné par augmentation du nombre d'atomes de carbone
C07D 317/12 - Composés hétérocycliques contenant des cycles à cinq chaînons comportant deux atomes d'oxygène comme uniques hétéro-atomes du cycle comportant les hétéro-atomes en positions 1, 3 non condensés avec d'autres cycles avec uniquement des atomes d'hydrogène ou des radicaux ne contenant que des atomes de carbone et d'hydrogène, liés directement aux atomes de carbone du cycle
The objective of the present invention is to provide a fuel supply device and a fuel supply method with which it is possible, using simple equipment, to achieve stable operation of electricity generation by means of a diesel engine employing liquid biomass fuel including various types of palm oil. This device, which employs liquid biomass fuel including palm oil as liquid fuel stock, and supplies the same to a diesel engine, includes a liquid fuel stock tank 1 in which the liquid fuel stock is stored, and a circulating pipeline 3 which is laid in such a way as to supply the liquid fuel stock from the liquid fuel stock tank 1 to the diesel engine 4 and to return to the liquid fuel stock tank 1. A pressure regulating valve 6 is disposed on a return pipeline 33 side of the circulating pipeline 3, to maintain the pressure in the circulating pipeline 3 at or above atmospheric pressure and to maintain the flow velocity in the circulating pipeline 3 at or above 0.3 m/sec, and the liquid fuel stock is constantly circulated.
F02M 37/00 - Appareils ou systèmes pour transférer le combustible liquide des réservoirs de stockage aux carburateurs ou aux injecteursDispositions d'épuration du combustible liquide spécialement conçues pour les moteurs à combustion interne ou aménagées sur ceux-ci
46.
Main agent uniformly dispersed microsphere and a sustained release formulation comprising the same
The present application provides a microsphere in which a main agent is uniformly dispersed in a polymer matrix, wherein an average volume-based particle diameter of the microsphere is 1 μm or more and 150 μm or less, and a variation coefficient of area ratios in four regions is 0.35 or less, wherein the area ratios in four regions are calculated by (s/A)×100(%) wherein the four regions are prepared by preparing a cross section observation sample obtained by cutting the microsphere; observing the cross section observation sample with an electron microscope at a magnification capable of confirming the main agent in the microsphere or a higher magnification; and dividing the electron microscope observation image into four regions; and A is an area of a respective divided region, and s is a sum of cross section areas of the main agent included in the respective divided region. The microsphere of the present invention can appropriately control the initial release amount of the main agent and its release rate during a subsequent release period, and can continuously release the main agent for a predetermined period of time.
A61K 31/095 - Composés du soufre, du sélénium ou du tellure, p. ex. thiols
A61K 31/57 - Composés contenant des systèmes cycliques du cyclopenta[a]hydrophénanthrèneLeurs dérivés, p. ex. stéroïdes substitués en position 17 bêta par une chaîne à deux atomes de carbone, p. ex. prégnane ou progestérone
A61K 31/496 - Pipérazines non condensées contenant d'autres hétérocycles, p. ex. rifampine, thiothixène ou sparfloxacine
A61K 31/7048 - Composés ayant des radicaux saccharide et des hétérocycles ayant l'oxygène comme hétéro-atome d'un cycle, p. ex. leucoglucosane, hespéridine, érythromycine, nystatine
47.
MICROSPHERES IN WHICH BIOACTIVE SUBSTANCE IS UNIFORMLY DISPERSED, AND SUSTAINED-RELEASE PREPARATION CONTAINING SAME
The present application provides microspheres in which a bioactive substance is uniformly dispersed, the microspheres having a lactic acid-glycolic acid copolymer (PLGA) as the main component, wherein the microspheres are characterized in that the average volume-based particle size of the microspheres is 1-150 μm (inclusive), and there are no lumps of bioactive substance or voids measuring 1.5 μm or larger in the microspheres. In the microspheres of the present invention, the initial release level of the bioactive substance and the release rate during the subsequent release period are appropriately controlled, making it possible for the bioactive substance to be released continuously in the body over a certain period of time.
A61K 47/34 - Composés macromoléculaires obtenus par des réactions autres que celles faisant intervenir uniquement des liaisons non saturées carbone-carbone, p. ex. polyesters, acides polyaminés, polysiloxanes, polyphosphazines, copolymères de polyalkylène glycol ou de poloxamères
48.
Microsphere comprising PLGA or PLA in which a biologically active substance is uniformly dispersed and a sustained release formulation comprising the same
The present application provides a microsphere comprising a lactic acid-glycolic acid copolymer (PLGA) or polylactide (PLA) as a main component, in which a biologically active substance is uniformly dispersed, wherein an average volume-based particle diameter of the microsphere is 1 μm or more and 150 μm or less, and a variation coefficient of area ratios in six regions is 0.35 or less, wherein the area ratios in six regions are calculated by (s/A)×100 (%) wherein the six regions are prepared by preparing a cross section observation sample obtained by cutting the microsphere; observing the cross section observation sample with an electron microscope at a magnification capable of confirming the biologically active substance in the microsphere or a higher magnification; and dividing the electron microscope observation image into six regions; and A is an area of a respective divided region, and s is a sum of cross section areas of the biologically active substance included in the respective divided region. The microsphere of the present invention can appropriately control the initial release amount of the biologically active substance and its release rate during a subsequent release period, and can continuously release the biologically active substance in vivo for a predetermined period of time.
In the present application, a microsphere is provided, which contains, as a main component, a poly(lactic-co-glycolic) acid (PLGA) or a polylactic acid (PLA) in which a physiologically active substance is dispersed uniformly, the microsphere being characterized in that the volume average particle diameter is 1 to 150 μm, inclusive, and also characterized in that, when the microsphere is cut to prepare a cross-sectional observation specimen, then the cross-sectional observation specimen is observed with an electron microscope at a magnification equal to or higher than a magnification at which the physiologically active substance in the microsphere can be confirmed, then an image obtained by the observation of the cross section with the electron microscope is divided into six regions, and then a ratio of the total (s) of the cross-sectional areas of the physiologically active substance contained in each of the divided regions to the area (A) of the corresponding region, i.e., (s/A)×100(%), is calculated, the coefficient of variation of the calculated ratios in the six regions is 0.35 or less. The microsphere according to the present invention is regulated appropriately with respect to the initial release amount of the physiologically active substance and the release rate of the physiologically active substance during the subsequent releasing period, and can release the physiologically active substance in vivo continuously for a certain period.
A61K 47/34 - Composés macromoléculaires obtenus par des réactions autres que celles faisant intervenir uniquement des liaisons non saturées carbone-carbone, p. ex. polyesters, acides polyaminés, polysiloxanes, polyphosphazines, copolymères de polyalkylène glycol ou de poloxamères
Microspheres in which a principal agent is uniformly dispersed in a polymer matrix, the microspheres being characterized in that the average volume-based particle size of the microspheres is 1–150 μm and in that, when the microspheres are sliced to produce a cross-sectional observation sample, the cross-sectional observation sample is observed by electron microscope at at least the magnification at which the principal agent in the microspheres can be identified, the cross-sectional image observed by electron microscope is quadrisected, and the ratio (s/A)×100 (%) of the sectional area (A) of each of the sections and the total cross-sectional area (s) of the primary agent included in the section is calculated, the coefficient of variation of the ratios calculated for the four sections is no more than 0.35. The microspheres make it possible for the amount of principal agent initially released and the release speed of the principal agent during the release period following initial release to be appropriately controlled, making it possible for the principal agent to be continuously released over a fixed period of time.
A61K 47/34 - Composés macromoléculaires obtenus par des réactions autres que celles faisant intervenir uniquement des liaisons non saturées carbone-carbone, p. ex. polyesters, acides polyaminés, polysiloxanes, polyphosphazines, copolymères de polyalkylène glycol ou de poloxamères
A stirrer is provided that can more efficiently achieve shearing applied, by an action of an intermittent jet flow, to a fluid to be processed. The stirrer concentrically includes a rotor including a blade, a partition wall, and a screen, wherein: the screen includes a plurality of slits in a circumferential direction thereof and screen members located between the adjacent slit; by rotating at least the rotor of the two components, the fluid to be processed is discharged from the inside to the outside of the screen as the intermittent jet flow through the slit of the screen; the screen has a cylindrical shape having a circular cross section; an opening of the slit provided on the inner wall surface of the screen is used as an inflow opening; openings of the plurality of slits provided on the outer wall surface of the screen are used as outflow openings; and the width of the outflow openings in the circumferential direction is set to be smaller than the width of the inflow opening in the circumferential direction.
B22C 5/00 - Machines ou dispositifs spécialement conçus pour la préparation ou la manutention des matériaux à mouler, dans la mesure où ils sont spécialement adaptés à cette fin
B01F 25/45 - Mélangeurs dans lesquels les composants du mélange sont pressés ensemble au travers d’orifices ou d’espaces interstitiels, p. ex. entre des perles
B01F 25/452 - Mélangeurs dans lesquels les composants du mélange sont pressés ensemble au travers d’orifices ou d’espaces interstitiels, p. ex. entre des perles caractérisés par des éléments pourvus d'orifices ou d'espaces interstitiels
B01F 27/91 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des hélices
B01F 27/92 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des hélices ou des vis
B01F 27/81 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical les agitateurs ayant des entrées de flux axiales centrales et des sorties de flux sensiblement radiales
B01F 27/921 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des hélices ou des vis avec des hélices montées centralement dans le récipient
A stirrer is provided such that a fluid being processed can be more efficiently shown by way of the action of an intermittent jet flow and processing capacity can be improved. The stirrer concentrically includes a rotor that includes a plurality of flat vanes and that rotates, and a screen that is place around the rotor. The screen includes a plurality of slits in the circumferential direction thereof, and screen members that are positioned between adjacent slits. The fluid being processed is discharged by rotation of the rotor from the inside of the screen to the outside as an intermittent jet flow through the slits. The width of the distal working face on the distal end of the vane in the rotational direction is smaller than the width of the basal end of the vane in the rotational direction.
Provided is a heat exchanger comprising a structure that is advantageous in increasing the overall heat transfer coefficient which represents the efficiency of heat exchange. Three flow paths, a first flow path 11, a second flow path 21, and a third flow path 31, which turn spirally in the space formed between an inner cylinder 61 and an outer cylinder 52 are provided. These flow paths are defined by an inner heat transfer body 41 and an outer heat transfer body 51, and heat exchange is performed through the heat transfer bodies. The heat transfer bodies turn spirally, have a screw shape in an axial cross-sectional view, and are assembled into a screw shape. The flow path area of the first flow path 11 is varied by changing the shapes of a male thread and a female thread, and the second flow path 21 and the third flow path 31 are formed in a spiral shape, allowing for exchange of heat through the heat transfer bodies.
F28D 9/00 - Appareils échangeurs de chaleur comportant des ensembles de canalisations fixes en forme de plaques ou de laminés pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation
F28D 9/02 - Appareils échangeurs de chaleur comportant des ensembles de canalisations fixes en forme de plaques ou de laminés pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation les sources de potentiel calorifique se déplaçant l'une par rapport à l'autre suivant un angle
F28F 3/08 - Éléments construits pour être empilés, p. ex. pouvant être séparés pour leur nettoyage
The present invention addresses the problem of providing a flow reactor that is advantageously structured to increase the overall heat transfer coefficient, which represents the efficiency of heat exchange with respect to a reactive fluid to be treated. This flow reactor is provided with three flow passages, which are a first flow passage (11), a second flow passage (21), and a third flow passage (31) which spirally circulate within a space formed between an inner tube (61) and an outer tube (52). The flow passages are compartmented by an inner heat transfer body (41) and an outer heat transfer body (51), and heat exchange occurs through these heat transfer bodies. The heat transfer bodies spirally circulate, have a screw-like cross-sectional shape in an axial cross-sectional view, and are assembled in a screw-like configuration. By changing the shapes of a male-thread portion and a female-thread portion, the flow passage area of the first flow passage (11) is changed, the second flow passage (21) and the third flow passage (31) are spirally formed, and heat exchange and reaction take place through the heat transfer bodies.
F28D 9/00 - Appareils échangeurs de chaleur comportant des ensembles de canalisations fixes en forme de plaques ou de laminés pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation
F28F 3/08 - Éléments construits pour être empilés, p. ex. pouvant être séparés pour leur nettoyage
B01J 19/24 - Réacteurs fixes sans élément interne mobile
Provided is a flow reactor which can promote a reaction under appropriate temperature management, can prevent reaction fluid or generated gas from being trapped in a heat transmission part, can be disassembled for easy cleaning, and to which coating or lining can be applied. This flow reactor is provided with two flow paths, a reaction flow path 11 and a second flow path 21, in a space formed between an inner cylinder 10 and an outer cylinder 20 that are concentric. A spiral heat transmission body 41 is disposed between the inner cylinder 10 and the outer cylinder 20, and the spiral heat transmission body 41 has a substantially triangular cross-sectional shape in an axial cross-sectional view. The spiral heat transmission body 41 partitions the space into the reaction flow path 11 and the second flow path 21, and heat is exchanged via the spiral heat transmission body 41 between a reaction fluid F1 flowing through the reaction flow path 11 and a heat medium F2 flowing through the second flow path 21.
Provided is a heat exchanger with which a fluid to be treated or a generated gas can be prevented from stagnating in a heat transfer part, which can be disassembled for good washability, and which can be coated or lined. The heat exchanger is provided with two flow passages, i.e. a first flow passage 11 and a second flow passage 21, within a space formed between an inner cylinder 10 and an outer cylinder 20 which are concentric to each other. A spiral heat transfer body 41 is disposed between the inner cylinder 10 and the outer cylinder 20, and the spiral heat transfer body 41 has a cross-section shape that is substantially triangular in the axial-direction cross section. The space is partitioned into the first flow passage 11 and the second flow passage 21 by the spiral heat transfer body 41, and heat is exchanged via the spiral heat transfer body 41 between a first fluid F1 flowing within the first flow passage 11 and a fluid F2 flowing within the second flow passage 21.
F28D 7/02 - Appareils échangeurs de chaleur comportant des ensembles de canalisations tubulaires fixes pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation les canalisations étant enroulées en hélice
F28D 9/00 - Appareils échangeurs de chaleur comportant des ensembles de canalisations fixes en forme de plaques ou de laminés pour les deux sources de potentiel calorifique, ces sources étant en contact chacune avec un côté de la paroi d'une canalisation
57.
Forced thin film-type flow reactor and method for operating same
A forced thin film-type flow reactor is provided with a clearance adjustment mechanism that allows the clearance to be set and adjusted by an alternative means. The flow reactor processes a fluid to be processed by passing the fluid to be processed between a first processing surface and a second processing surface capable of moving towards and away from each other, and the flow reactor comprises a pressure balancing mechanism and a mechanical clearance mechanism. The pressure balancing mechanism forms a minute first clearance by providing pressure balance between the pressure applied by the fluid to be processed, which acts in the direction in which the first processing surface and the second processing surface move away from each other, and a force produced by a back pressure mechanism, which acts in the direction in which the first processing surface and the second processing surface move towards each other.
B01J 19/18 - Réacteurs fixes avec éléments internes mobiles
A61L 2/07 - Procédés ou appareils de désinfection ou de stérilisation de matériaux ou d'objets autres que les denrées alimentaires ou les lentilles de contactAccessoires à cet effet utilisant des phénomènes physiques de la chaleur des gaz chauds de la vapeur
The present invention pertains to a production method for fine particles of silver, whereby silver ions contained in a silver compound are continuously reduced and fine particles of silver are precipitated, by introducing at least two fluids from different flow paths and mixing the fluids. The production method for fine particles of silver is characterized by one fluid out of the at least two fluids containing the silver compound, the other fluid containing a reducing agent, and at least one fluid out of the at least two fluids containing amino acid. As a result of the present invention, fine particles of silver can be produced with sufficient continuous productivity and quality uniformity and without the issues of deterioration of the work environment due to the use of large amounts of ammonia or the generation of explosive fulminating silver.
B22F 9/24 - Fabrication des poudres métalliques ou de leurs suspensionsAppareils ou dispositifs spécialement adaptés à cet effet par un procédé chimique avec réduction de mélanges métalliques à partir de mélanges métalliques liquides, p. ex. de solutions
The present invention relates to silicon-compound-coated fine metal particles, with which surfaces of fine metal particles, composed of at least one type of metal element or metalloid element, are at least partially coated with a silicon compound and a ratio of Si—OH bonds contained in the silicon-compound-coated fine metal particles is controlled to be 0.1% or more and 70% or less. By the present invention, silicon-compound-coated fine metal particles that are controlled in dispersibility and other properties can be provided by controlling the ratio of Si—OH bonds or the ratio of Si—OH bonds/Si—O bonds contained in the silicon-compound-coated fine metal particles. By controlling the ratio of Si—OH bonds or the ratio of Si—OH bonds/Si—O bonds, a composition that is more appropriate for diversifying applications and targeted properties of silicon-compound-coated fine metal particles than was conventionally possible can be designed easily.
C09C 3/12 - Traitement par des composés organiques du silicium
60.
PERYLENE-BASED BLACK PIGMENT FINE PARTICLES, METHOD FOR PRODUCING SAME, BLACK PIGMENT COMPOSITION CONTAINING SAME, AND METHOD FOR PRODUCING PERYLENE-BASED BLACK PIGMENT FINE PARTICLES HAVING CONTROLLED HUE AND/OR SATURATION
The present invention is a method for producing perylene-based black pigment fine particles, which comprises a step for producing perylene-based black pigment fine particles by mixing a pigment solution, in which amorphous perylene-based black pigment fine particles having an average circularity of 0.8 or more and a perylene-based black pigment are dissolved, with a precipitation solvent for having the perylene-based black pigment fine particles precipitate from the pigment solution, wherein at least one of the pigment solution and the precipitation solvent independently contains an alkaline earth metal salt and/or a particle growth inhibitor. The present invention is able to provide: perylene-based black pigment fine particles which have good dispersibility, high concealability and high light blocking properties, while having controlled hue and saturation; a method by which the perylene-based black pigment fine particles are easily produced; and the like.
Provided is a stirrer that can more efficiently achieve shearing applied, by an action of an intermittent jet flow, to a fluid to be processed. The stirrer is characterized by concentrically comprising a rotor 2 including a blade 12, a partition wall 10, and a screen 9, wherein: the screen 9 includes a plurality of slits 18 in a circumferential direction thereof and screen members 19 located between the adjacent slits 18; by rotating at least the rotor 2 of the two components, the fluid to be processed is discharged from the inside to the outside of the screen 9 as the intermittent jet flow through the slits 18 of the screen 9; the screen 9 has a cylindrical shape having a circular cross section; an opening of the slit 18 provided on the inner wall surface of the screen 9 is used as an inflow opening 28; openings of the plurality of slits 18 provided on the outer wall surface of the screen 9 are used as outflow openings 29; and the width (So) of the outflow openings 29 in the circumferential direction is set to be smaller than the width (Si) of the inflow opening 28 in the circumferential direction.
Provided is an agitator that is capable of more efficiently applying a shear force to a treatment target fluid through the action of an intermittent jet stream. The agitator comprises a rotor 2 which includes blades 12, and a screen 9 concentric therewith, the rotation of at least the rotor 2 causing a treatment target fluid to pass through slits 18 in the screen 9 to become an intermittent jet stream, which is discharged from inside the screen 9 to the outside thereof, wherein the agitator is characterized in that: the screen 9 has a cylindrical shape with a circular cross section; openings of the slits 18 provided in an inner surface of the screen 9 constitute flow intake openings 33; openings of the slits 18 provided in an outer surface of the screen 9 constitute flow discharge openings 34; spaces between the flow intake openings 33 and the flow discharge openings 34 constitute slit spaces 35; and the circumferential-directional width (So) of the flow discharge openings and the circumferential-directional width (Si) of the flow intake openings 33 are greater than the circumferential-directional width (Sm) of the slit spaces 35.
The present invention seeks to provide an agitator in which cavitation arising during treatment of a fluid being treated is suppressed. In this agitator, a stator part S is provided with a plurality of penetration parts 13a in the circumferential direction of the stator part S, and a stator main part positioned between adjacent penetration parts 13a. When a fluid is discharged from the inside of the stator part S to the outside through the penetration part 13a by the rotation of a rotor, in the stator part S for the agitator treating the fluid, the side facing a blade of the rotor is an inner wall surface, the side facing the side opposite to the blade is an outer wall surface, an opening of the plurality of penetration parts 13a that is provided in the inner wall surface is an inflow opening 13b, and an opening of the plurality of penetration parts 13a that is provided in the outer wall surface is an outflow opening 13c, the opening area of the inflow opening 13b being larger than the opening area of the outflow opening 13c.
B01F 7/10 - Mélangeurs à agitateurs tournant dans des récipients fixes; Pétrins avec agitateurs tournant autour d'un axe horizontal ou incliné à disques tournants
B01F 7/02 - Mélangeurs à agitateurs tournant dans des récipients fixes; Pétrins avec agitateurs tournant autour d'un axe horizontal ou incliné
B01F 7/08 - Mélangeurs à agitateurs tournant dans des récipients fixes; Pétrins avec agitateurs tournant autour d'un axe horizontal ou incliné à vis sans fin
Provided is a stirrer such that a fluid being processed can be more efficiently shorn by way of the action of an intermittent jet flow and processing capacity can be improved. The stirrer concentrically comprises a rotor 2 that comprises a plurality of flat vanes 12 and that rotates, and a screen 9 that is placed around the rotor 2. The screen 9 comprises a plurality of slits 18 in the circumferential direction thereof, and screen members 19 that are positioned between adjacent slits 18. The fluid being processed is discharged by rotation of the rotor 2 from the inside of the screen 9 to the outside as an intermittent jet flow through the slits 18. The width (b) of the distal working face 30 on the distal end 21 of the vane 12 in the rotational direction is smaller than the width (B) of the basal end 32 of the vane 12 in the rotational direction.
The present invention seeks to provide a vacuum deaerator with refining device with which it is possible to suppress the occurrence of situations involving interrupted discharging and continuously discharge a material being treated from under a high vacuum even in deaeration treatment of a material being treated that is highly viscous, etc. The vacuum deaerator introduces a liquid material being treated into a vessel 10 having a vacuum therein to perform deaeration and then discharges the material being treated out of the vessel 10. A rotating rotor 32 with refining device 31 arranged in the vessel 10 and a rotating discharge vane 42 provided separately from the rotating rotor 32 for the purpose of discharging the material being treated in the vessel 10 out of the vessel 10 are installed.
A vacuum degassing machine that degasses material to be processed by placing a rotating rotor 30 with a screen in a vacuum vessel, introducing a liquid material to be processed into the rotor 30 from the interior thereof and causing the liquid to pass through the screen 3 to refine the same, wherein the vacuum degassing machine is characterized in that: the screen 3 is a cylinder with a circular cross-section and is in the form of a porous plate in which a plurality of through holes are opened in the radial direction of the cylindrical screen 3; and the screen 3 is provided such that the area of inflow openings is greater than the area of outflow openings, where the inflow openings are openings of a plurality of penetration portions provided on the inner wall face of the screen 3 and the outflow openings are openings of the plurality of penetration portions provided on the outer wall face of the screen. Thus, the processing capacity of the vacuum degassing machine is improved without increasing the size of the device.
The present invention provides: roughly spherical poly(lactic-co-glycolic acid) (PLGA) microparticles which have a volume-based average particle diameter of 1-150 μm inclusive, the relative span factor (R.S.F.) of which satisfies requirement (1): 0.1<(R.S.F.)≤1.7 [wherein: R.S.F. means (D90-D10)/D50; D90 represents a particle diameter corresponding to 90 vol% accumulated from the smaller particle side in the cumulative particle size distribution; D50 represents a particle diameter corresponding to 50 vol% accumulated from the smaller particle side in the cumulative particle size distribution; and D10 represents a particle diameter corresponding to 10 vol% accumulated from the smaller particle side in the cumulative particle size distribution] and which contain a physiologically active substance; and a method for efficiently manufacturing the same. According to the present invention, provided are roughly spherical PLGA microparticles which include few coarse or fine particles, show a sharp particle diameter distribution centering on a desired particle diameter, and have a volume-based average particle diameter of 1-150 μm inclusive, without performing a classification step.
A61K 9/52 - Préparations en capsules, p. ex. de gélatine, de chocolat du type à libération prolongée ou discontinue
A61J 3/06 - Dispositifs ou procédés spécialement conçus pour donner à des produits pharmaceutiques une forme physique déterminée ou une forme propre à leur administration la forme de pilules, tablettes ou pastilles
A61K 47/34 - Composés macromoléculaires obtenus par des réactions autres que celles faisant intervenir uniquement des liaisons non saturées carbone-carbone, p. ex. polyesters, acides polyaminés, polysiloxanes, polyphosphazines, copolymères de polyalkylène glycol ou de poloxamères
68.
Ultraviolet and/or near-infrared blocking agent composition for transparent material
An object of the present invention is to provide an ultraviolet and/or near-infrared shielding agent composition for transparent material using silicon compound-coated silicon-doped zinc oxide particles that are controlled in properties in an ultraviolet region and/or a near-infrared region. The present invention provides an ultraviolet and/or near-infrared shielding agent composition for transparent material used for a purpose of shielding ultraviolet rays and/or near-infrared rays, the ultraviolet and/or near-infrared shielding agent composition for transparent material featuring that the ultraviolet and/or near-infrared shielding agent contains silicon compound-coated silicon-doped zinc oxide particles, with which surfaces of silicon-doped zinc oxide particles that are zinc oxide particles doped with at least silicon are at least partially coated with a silicon compound.
Provided is a fluid treatment device having a novel configuration. This fluid treatment device F is provided with: an upstream-side treatment part defined by treatment surfaces 1, 2, which can be moved towards and away from each other and which rotate relative to each other; and a downstream-side treatment part disposed on the downstream side of the upstream-side treatment part. The upstream-side treatment part is configured so that a fluid being treated is passed through an upstream-side treatment space 3 defined by the treatment surfaces 1, 2, whereby an upstream-side treatment is performed on the fluid being treated. The downstream-side treatment part is provided with a downstream-side treatment space 81 connecting to the upstream-side treatment space 3. A part of a rotary member 10, 91, which rotates integrally with the rotating treatment surface 1, forms a part of a wall surface defining the downstream-side treatment space 81. The downstream-side treatment part is configured so as to be able to utilize the rotation of the rotary member 10, 91 to perform a downstream-side treatment on the fluid being treated in succession from the upstream-side treatment.
B01J 19/00 - Procédés chimiques, physiques ou physico-chimiques en généralAppareils appropriés
B01F 7/26 - Mélangeurs à agitateurs tournant dans des récipients fixes; Pétrins avec agitateurs tournant autour d'un axe vertical à disques rotatifs
B01F 7/28 - Mélangeurs à agitateurs tournant dans des récipients fixes; Pétrins avec agitateurs tournant autour d'un axe vertical à cylindres
B01F 13/00 - Autres mélangeurs; Installations pour effectuer des mélanges comportant des combinaisons de mélangeurs de types différents
B01F 15/06 - Systèmes de chauffage ou de refroidissement
B01J 19/12 - Procédés utilisant l'application directe de l'énergie ondulatoire ou électrique, ou un rayonnement particulaireAppareils à cet usage utilisant des radiations électromagnétiques
B01J 19/18 - Réacteurs fixes avec éléments internes mobiles
Provided is a method for producing an organic compound, the method making it possible to ensure an adequate reaction time and obtain a target substance at a high yield even in an organic reaction that requires a relatively long time to complete the reaction. A method for producing an organic compound, wherein the method is characterized in that: a fluid processing apparatus F used in the production method is equipped with an upstream processing unit that processes a fluid to be processed between at least two processing surfaces 1 and 2 that relatively rotate, and a downstream processing unit disposed downstream of the upstream processing unit, the downstream processing unit being provided with a plurality of labyrinth seals that function to retain and stir the fluid to be processed that has been processed by the upstream processing unit; due to the fluid to be processed, which contains at least one type of organic compound, being passed through the upstream processing unit, the fluid to be processed is subjected to upstream processing; due to the fluid to be processed that has been subjected to upstream processing being passed through the downstream processing unit, the fluid to be processed that has been subjected to upstream processing is subjected to downstream processing; and the upstream processing and the downstream processing are performed continuously.
C07C 29/12 - Préparation de composés comportant des groupes hydroxyle ou O-métal liés à un atome de carbone ne faisant pas partie d'un cycle aromatique à six chaînons par hydrolyse d'esters d'acides minéraux
C07C 31/10 - Alcools monohydroxyliques acycliques contenant trois atomes de carbone
C07C 31/12 - Alcools monohydroxyliques acycliques contenant quatre atomes de carbone
C07C 31/125 - Alcools monohydroxyliques acycliques contenant de cinq à vingt-deux atomes de carbone
C07C 45/74 - Préparation de composés comportant des groupes C=O liés uniquement à des atomes de carbone ou d'hydrogènePréparation des chélates de ces composés par des réactions ne créant pas de groupe C=O par isomérisationPréparation de composés comportant des groupes C=O liés uniquement à des atomes de carbone ou d'hydrogènePréparation des chélates de ces composés par des réactions ne créant pas de groupe C=O par modification de la taille du squelette carboné par augmentation du nombre d'atomes de carbone par réaction de composés comportant des groupes C=O sur eux-mêmes ou avec d'autres composés comportant des groupes C=O combinée avec une déshydratation
C07C 69/18 - Esters d'acide acétique de composés trihydroxylés
C07C 69/602 - Esters d'acides dicarboxyliques avec plusieurs liaisons doubles carbone-carbone
C07D 317/72 - Composés hétérocycliques contenant des cycles à cinq chaînons comportant deux atomes d'oxygène comme uniques hétéro-atomes du cycle comportant les hétéro-atomes en positions 1, 3 condensés en spiro avec des carbocycles
C07C 49/217 - Composés non saturés comportant des groupes cétone liés à des atomes de carbone acycliques contenant des cycles aromatiques à six chaînons avec insaturation autre que celle des cycles aromatiques
C07C 49/255 - Composés non saturés comportant des groupes cétone liés à des atomes de carbone acycliques contenant des groupes éther, des groupes , des groupes ou des groupes
B01J 19/18 - Réacteurs fixes avec éléments internes mobiles
C07C 67/08 - Préparation d'esters d'acides carboxyliques par réaction d'acides carboxyliques ou d'anhydrides symétriques avec le groupe hydroxyle ou O-métal de composés organiques
C07C 67/343 - Préparation d'esters d'acides carboxyliques par modification de la partie acide de l'ester sans introduction d'un groupe ester par isomérisationPréparation d'esters d'acides carboxyliques par modification de la partie acide de l'ester sans introduction d'un groupe ester par modification de la taille du squelette carboné par augmentation du nombre d'atomes de carbone
A fluid treatment device with a new configuration is provided. The fluid treatment device F is provided with an upstream treatment unit defined by treatment surfaces 1, 2 that rotate relative to each other, and a downstream treatment unit arranged downstream of the upstream treatment unit. The upstream treatment unit is configured such that, by passing the fluid to be treated into an upstream treatment space 3 defined by the treatment surfaces 1, 2, the fluid to be treated is subjected to upstream treatment. The downstream treatment unit is provided with a downstream treatment space 81 which performs the function of retaining and mixing the fluid to be treated by means of a labyrinth seal. An upstream outlet 4 of the fluid to be treated from the upstream treatment unit opens into the downstream treatment space 81, and the downstream treatment space 81 is configured to use the labyrinth seal to perform the function of controlling retention time. The downstream treatment space 81 is provided with narrow seal spaces 84, and retention spaces 83 arranged upstream of the seal spaces 84 and wider than the seal spaces 84, and the upstream outlet 4 opens to a retention space 83.
B01J 19/18 - Réacteurs fixes avec éléments internes mobiles
B01F 7/26 - Mélangeurs à agitateurs tournant dans des récipients fixes; Pétrins avec agitateurs tournant autour d'un axe vertical à disques rotatifs
B01F 7/28 - Mélangeurs à agitateurs tournant dans des récipients fixes; Pétrins avec agitateurs tournant autour d'un axe vertical à cylindres
B01F 13/00 - Autres mélangeurs; Installations pour effectuer des mélanges comportant des combinaisons de mélangeurs de types différents
B01F 15/06 - Systèmes de chauffage ou de refroidissement
B01J 19/00 - Procédés chimiques, physiques ou physico-chimiques en généralAppareils appropriés
B01J 19/12 - Procédés utilisant l'application directe de l'énergie ondulatoire ou électrique, ou un rayonnement particulaireAppareils à cet usage utilisant des radiations électromagnétiques
Provided is a continuous stirring device with a novel configuration. The continuous stirring device F has an outer wall 61 and an inner wall 10 disposed inside the outer wall 61 that are concentric, and mixes an object to be processed in a processing space 81 formed between the outer wall 61 and the inner wall 10 with the object to be processed passing through the processing space while at least one of the outer wall 61 and the inner wall 10 rotates with respect to the other. The configuration is such that a plurality of labyrinth seals are placed in the processing space 81, and retention of the object to be processed on the upstream side of the labyrinth seals and subsequent passage of the object to be processed through the labyrinth seals are repeated to mix the object to be processed, or to mix the object to be processed while controlling the retention time for the object to be processed. When a narrow seal space 84 and a retention space 83 that is disposed on the upstream side of the seal space 84 and that is wider than the seal space 84 are treated as a group, the processing space 81 comprises a plurality of consecutive groups of seal spaces 84 and retention spaces 83 from the upstream side to the downstream side of the flow of the object to be processed.
B01F 7/28 - Mélangeurs à agitateurs tournant dans des récipients fixes; Pétrins avec agitateurs tournant autour d'un axe vertical à cylindres
B01F 13/00 - Autres mélangeurs; Installations pour effectuer des mélanges comportant des combinaisons de mélangeurs de types différents
B01F 15/06 - Systèmes de chauffage ou de refroidissement
B01J 19/00 - Procédés chimiques, physiques ou physico-chimiques en généralAppareils appropriés
B01J 19/12 - Procédés utilisant l'application directe de l'énergie ondulatoire ou électrique, ou un rayonnement particulaireAppareils à cet usage utilisant des radiations électromagnétiques
B01J 19/18 - Réacteurs fixes avec éléments internes mobiles
73.
Filtration membrane module and filtration processing method
The purpose of this invention is to provide a filtration membrane module with which is possible to improve the centrifugal separation effect of the primary-side flowpath during filtration, and the centrifugal separation effect of the area following the outer peripheral surface of the flowpath membrane element of the outer ring-shaped flowpath during backwash, and improve filtration efficiency and cleaning efficiency while curbing the accumulation of deposits on the membrane surface during filtration and during backwash. This filtration membrane module comprises: a membrane element equipped with a primary-side flowpath on the outside of a hollow cylindrical filtration surface; and a cylindrical housing positioned on the outside thereof. A flow adjuster is positioned inside the primary-side flowpath. A flow adjuster for backwash is positioned inside the secondary-side flowpath, which is an outer ring-shaped flowpath between the membrane element and the housing. The flow adjuster and the flow adjuster for backwash comprise spiral-shaped fins or the like in order to exhibit a centrifugal separation function in an area that follows the outer peripheral surface of the membrane element or the filtration surface.
Provided are an immediately-before-stirring-type fluid processing device and an immediately-before-stirring-type fluid processing method that can adjust or improve the final properties of a fluid to be processed that is introduced as a raw material into an annular flow channel of a microreactor employing the annular flow channel, which is formed between relatively rotating processing surfaces, as a flow channel in which fluid processing is performed. A fluid to be processed, which has been prepared in a fluid preparing system so as to be in an ideal state for reaction, is charged into a fluid processing device. The fluid processing device subjects the fluid to be processed to reaction processing in an annular flow channel, which is formed between two processing surfaces. A cylindrical stirring space is provided in the radially inner side of the annular flow channel, and a rotor and a screen are disposed inside the stirring space. Stirring energy is applied by the rotor and a shearing force is applied between the rotor and the screen to the fluid to be processed immediately before the fluid to be processed is introduced into the annular flow channel.
B01J 19/18 - Réacteurs fixes avec éléments internes mobiles
B01F 27/93 - Mélangeurs à agitateurs tournant dans des récipients fixesPétrins avec des agitateurs tournant autour d'un axe sensiblement vertical avec des disques rotatifs
B01F 23/231 - Mélange de gaz avec des liquides en introduisant des gaz dans des milieux liquides, p. ex. pour produire des liquides aérés par barbotage
B01F 23/233 - Mélange de gaz avec des liquides en introduisant des gaz dans des milieux liquides, p. ex. pour produire des liquides aérés en utilisant des agitateurs entraînés munis d’éléments d'agitation complètement immergés
The object of the present invention is to provide silicon doped metal oxide particles for UV absorption, which average molar absorption coefficient in the wavelength range of 200 nm to 380 nm, is enhanced. Provided is silicon doped metal oxide particles in which the metal oxide particles are doped with silicon, wherein an average molar absorption coefficient in the wavelength range of 200 nm to 380 nm, of a dispersion in which the silicon doped metal oxide particles are dispersed in a dispersion medium, is improved as compared with similar metal oxide particles not doped with silicon.
The present invention is a method of producing highly crystalline silver microparticles by a reduction reaction, which comprises precipitating the silver microparticles by reacting a silver solution containing at least silver ions and a reducing agent solution containing at least a reducing agent by a continuous wet reduction method, wherein a reduction rate from the silver solution to the silver microparticles is 99% or more; an average primary particle diameter of the silver microparticles is 100 nm or more and 1,000 nm or less; and an average crystallite diameter relative to the average primary particle diameter of the silver microparticles is 80% or more. Even highly crystalline silver microparticles having 95% or more of the ratio (d/D) of the average crystallite diameter (d) relative to the average primary particle diameter (D), that is, silver microparticles in which almost all silver microparticles are single crystals, can be continuously produced by a liquid phase method, by the present invention.
B22F 9/24 - Fabrication des poudres métalliques ou de leurs suspensionsAppareils ou dispositifs spécialement adaptés à cet effet par un procédé chimique avec réduction de mélanges métalliques à partir de mélanges métalliques liquides, p. ex. de solutions
B22F 1/05 - Poudres métalliques caractérisées par la dimension ou la surface spécifique des particules
B22F 1/0545 - Dispersions ou suspensions de particules de taille nanométrique
77.
Method for producing oxide particles with controlled color characteristics, oxide particles, and coating or film-like composition comprising the same
A method for producing oxide particles with controlled color characteristics and to provide oxide particles with controlled color characteristics includes controlling color characteristics of the oxide particles by controlling the ratio of M-OH bonds, the binding of one or more different elements (M) other than oxygen or hydrogen with hydroxyl group (OH), in oxide particles selected from metal oxide particles and metalloid oxide particles. Oxide particles having controlled color characteristics of any one of reflectance, transmittance, molar absorption coefficient, hue, or color saturation can be provided by controlling the percentage of the M-OH bonds contained in metal oxide particles or metalloid oxide particles.
A method of producing an organic pigment composition including at least organic pigment microparticles, wherein a diffuse reflectance of the organic pigment microparticles is controlled for the purpose of improving a luminance of a color filter. The luminance of the color filter is controlled to be high, by controlling a ratio of an area of the diffuse reflectance in a target wavelength range to a total area of the diffuse reflectance in the entire measurement wavelength range in a diffuse reflection spectrum of the organic pigment microparticles in the wavelength range of 380 to 780 nm, to be high. The luminance of the color filter is controlled to be high, by coating at least a part of the surface of the organic pigment microparticles with an oxide.
C09K 11/06 - Substances luminescentes, p. ex. électroluminescentes, chimiluminescentes contenant des substances organiques luminescentes
G02B 1/04 - Éléments optiques caractérisés par la substance dont ils sont faitsRevêtements optiques pour éléments optiques faits de substances organiques, p. ex. plastiques
G01N 21/27 - CouleurPropriétés spectrales, c.-à-d. comparaison de l'effet du matériau sur la lumière pour plusieurs longueurs d'ondes ou plusieurs bandes de longueurs d'ondes différentes en utilisant la détection photo-électrique
C09B 67/20 - Préparations à base de pigments organiques
C09B 67/02 - Préparations tinctoriales caractérisées par un aspect physique particulier, p. ex. tablettes, feuilles
79.
Pigment composition for green filter and production method thereof
A pigment composition for a green filter includes a green pigment consisting of a halogenated zinc phthalocyanine, wherein as spectral transmission characteristics of a dispersion containing only the green pigment as a pigment, the transmittance at 400 nm is 1% or less; the transmittance at 450 nm is 25% or less; the transmittance at 600 nm is 30% or less; the transmittance at 650 nm is 0.3% or less; the transmittance at the peak wavelength is 80% or more; the half value width of the peak wavelength is 120 nm or less; the transmittance at 750 nm is 1% or less; and the transmittance at 800 nm is 20% or less. The pigment composition for a green filter has low transmittance in the blue range, low transmittance in the near infrared range, and high transmittance in the green range by only a green pigment.
With an aim to provide a method for producing an oxide particle with controlled color characteristics and also provide an oxide particle with controlled color characteristics, the present invention provides a method for producing an oxide particle, wherein the color characteristics of the oxide particle are controlled by controlling a ratio of an M-OH bond between an element (M) and a hydroxide group (OH) or an M-OH bond/M-O bond ratio, where the element (M) is one element or plural different elements other than oxygen or hydrogen included in the oxide particle selected from metal oxide particles and semi-metal oxide particles. According to the present invention, by controlling the M-OH bond or the M-OH bond/M-O bond ratio of the metal oxide particle or the semi-metal oxide particle, the oxide particle with controlled color characteristics of any of reflectance, transmittance, molar absorption coefficient, hue, and saturation can be provided.
The present invention addresses the problem of providing a method for efficiently producing uniform microparticles of curcumin and/or γ-oryzanol at a higher yield. The target microparticles are produced by dissolving a starting material in a solvent to give a starting material solution and then subjecting the starting material solution to crystallization by a poor solvent method to thereby deposit the starting material. To prepare the starting material solution, curcumin and/or γ-oryzanol are used as the starting material(s) and ethanol is used as the solvent. The starting material(s) and the solvent are stirred in a pressurized state at a temperature of 78.3-130° C. inclusive to give the starting material solution. Then, the starting material solution thus obtained is subjected to crystallization by the poor solvent method and thus the target microparticles are produced.
C07C 45/81 - SéparationPurificationStabilisationEmploi d'additifs par modification de l'état physique, p. ex. par cristallisation
C07J 53/00 - Stéroïdes ayant le squelette du cyclopenta[a]hydrophénanthrène modifié par condensation avec des cycles carbocycliques ou par formation d'un cycle additionnel par une liaison directe entre deux atomes de carbone cycliques
C09B 61/00 - Colorants naturels préparés à partir de sources naturelles
A silicon oxide-coated oxide composition for coating is disclosed in which color characteristics, particularly reflectivity are controlled, and a method of producing a composition for coating is disclosed which is used by blending the composition for coating to a paint constituting a coated body in which weather resistance is required. The silicon oxide-coated oxide composition for coating in which weather resistance is required includes silicon oxide-coated oxide particles wherein at least a part of the surface of the oxide particles is coated with silicon oxide, wherein the silicon oxide is amorphous for the purpose of controlling color characteristics of the silicon oxide-coated oxide composition for coating. The method of producing the composition for coating, wherein color characteristics of the oxide particles are controlled, includes producing the oxide particles by selecting presence or absence of amorphous silicon oxide covering at least a part of the surface of the oxide particles, and presence or absence of an acetyl group as a functional group contained in the silicon oxide-coated oxide particles.
A61K 8/49 - Cosmétiques ou préparations similaires pour la toilette caractérisés par la composition contenant des composés organiques contenant des composés hétérocycliques
A61Q 1/02 - Préparations contenant des colorants cutanés, p. ex. pigments
A61Q 17/04 - Préparations topiques pour faire écran au soleil ou aux radiationsPréparations topiques pour bronzer
The present invention is a method of producing silicon compound coated oxide particles in which at least a part of a surface of a metal oxide particle is coated with a silicon compound, wherein wettability and color characteristics are controlled by controlling a ratio of Si—OH bonds contained in the silicon compound coated oxide particles. By the present invention, silicon compound coated oxide particles having controlled wettability such as hydrophilicity, water repellency or oil repellency, and controlled color characteristics of either reflectivity, molar absorption coefficient or transmittance can be provided.
With an aim to provide an oxide particle with controlled color characteristics, the present invention provides a method for producing an oxide particle, wherein the color characteristics of the oxide particle are controlled by controlling a M-OH bond/M-O bond ratio, which is a ratio of a M-OH bond between an element (M) and a hydroxide group (OH) to a ratio of an M-O bond between the element (M) and oxygen (O), where the element (M) is one or plural different elements other than oxygen or hydrogen included in the oxide particle selected from metal oxide particles and semi-metal oxide particles. According to the present invention, by controlling the M-OH bond/M-O bond ratio of the metal oxide particle or the semi-metal oxide particle, the oxide particle with controlled color characteristics of any of reflectance, transmittance, molar absorption coefficient, hue, and saturation can be provided.
A method for modifying a fine particle dispersion liquid has excellent dispersibility and dispersion stability. In this method for modifying a fine particle dispersion liquid having improved fine particle dispersibility, impurities included in an agglomeration of fine particles contained in the fine particle dispersion liquid are released into the dispersion liquid by applying physical energy to the agglomeration and performing dispersion processing for dispersion into particles that are smaller than the agglomeration of fine particles. The impurities are removed from the dispersion liquid by means of a removal unit provided with a filtration membrane before reagglomeration is caused by the impurities.
A method for modifying a fine particle dispersion liquid with which dispersibility and dispersion stability can be improved includes performing filtration to remove impurities in a dispersion liquid using a dispersion liquid modifying device provided with a removal unit that uses a filtration membrane. The quantity of impurities is reduced from a first region until said quantity reaches a second pH-dependent region. In the second pH-dependent region, the dispersibility of the fine particles in the dispersion liquid is in a range in which the dispersibility depends more on a change in dispersion liquid pH than on a change in the quantity of impurities in the dispersion liquid. With the quantity of impurities reduced to the second pH-dependent region, the dispersibility of the fine particles is controlled by adjusting the pH of the fine particle dispersion liquid.
The purpose of this invention is to increase the membrane flowrate of a primary-side flowpath during filtration and the flowrate in an area that follows the outer peripheral surface of a membrane element of an outer ring-shaped flowpath during backwash, and to improve filtration efficiency and cleaning efficiency while curbing the build-up of deposits on the membrane surface during filtration and backwashing. This filtration membrane module comprises: a membrane element 13 equipped with a primary-side flowpath 14 which is defined by a hollow cylindrical filtration surface 15; and a tubular housing 12 positioned on the outside thereof. A flow adjuster is positioned on the inside of the primary-side flowpath 14. An outside flow adjuster is positioned inside the outer ring-shaped flowpath 16 between the membrane element 13 and the housing 12. The flow adjuster and the outside flow adjuster are comprised of spiral-shaped fins or a static mixer so as to exhibit a flow accelerating function which increases the flowrate in an area that follows the outer peripheral surface of the filtration surface 15 or the membrane element 13.
B01D 35/00 - Dispositifs filtrants ayant des particularités non couvertes spécifiquement par les groupes , applications non couvertes spécifiquement par les groupes Dispositifs auxiliaires pour la filtrationStructure du carter de filtre
B01D 65/00 - Accessoires ou opérations auxiliaires, en général, pour les procédés ou les appareils de séparation utilisant des membranes semi-perméables
B01D 65/08 - Prévention de l'encrassement de la membrane ou de la polarisation par concentration
The purpose of this invention is to provide a filtration membrane module with which it is possible to improve the centrifugal separation effect of the primary-side flowpath during filtration, and the centrifugal separation effect of the area following the outer peripheral surface of the flowpath membrane element of the outer ring-shaped flowpath during backwash, and improve filtration efficiency and cleaning efficiency while curbing the accumulation of deposits on the membrane surface during filtration and during backwash. This filtration membrane module comprises: a membrane element equipped with a primary-side flowpath on the outside of a hollow cylindrical filtration surface; and a cylindrical housing positioned on the outside thereof. A flow adjuster is positioned inside the primary-side flowpath. A flow adjuster for backwash is positioned inside the secondary-side flowpath, which is an outer ring-shaped flowpath between the membrane element and the housing. The flow adjuster and the flow adjuster for backwash comprise spiral-shaped fins or the like in order to exhibit a centrifugal separation function in an area that follows the outer peripheral surface of the membrane element or the filtration surface.
B01D 35/00 - Dispositifs filtrants ayant des particularités non couvertes spécifiquement par les groupes , applications non couvertes spécifiquement par les groupes Dispositifs auxiliaires pour la filtrationStructure du carter de filtre
B01D 65/00 - Accessoires ou opérations auxiliaires, en général, pour les procédés ou les appareils de séparation utilisant des membranes semi-perméables
89.
FORCED THIN FILM-TYPE FLOW REACTOR AND METHOD FOR OPERATING SAME
The present invention provides a forced thin film-type flow reactor that, in addition to a pressure balance mechanism with which it is possible to set and adjust the clearance between processing surfaces using pressure balancing, is provided with a clearance adjustment mechanism that allows the clearance to be set and adjusted by an alternative means. The flow reactor processes a fluid for processing by passing the fluid for processing between a first processing surface and a second processing surface disposed so as to be capable of moving towards and away from each other, and the flow reactor comprises a pressure balancing mechanism and a mechanical clearance mechanism. The pressure balancing mechanism forms a minuscule first clearance by providing pressure balance between the pressure applied by the fluid for processing, which acts in the direction in which the first processing surface and the second processing surface move away from each other, and a force produced by a back pressure mechanism, which acts in the direction in which the first processing surface and the second processing surface move towards each other. The mechanical clearance mechanism mechanically sets a second clearance, which is greater than the first clearance, and makes it possible to set the clearance irrespective of the pressure of the fluid for processing.
B01J 19/18 - Réacteurs fixes avec éléments internes mobiles
A61L 2/18 - Procédés ou appareils de désinfection ou de stérilisation de matériaux ou d'objets autres que les denrées alimentaires ou les lentilles de contactAccessoires à cet effet utilisant des substances chimiques des substances liquides
A61L 2/20 - Procédés ou appareils de désinfection ou de stérilisation de matériaux ou d'objets autres que les denrées alimentaires ou les lentilles de contactAccessoires à cet effet utilisant des substances chimiques des substances gazeuses, p. ex. des vapeurs
B01J 19/00 - Procédés chimiques, physiques ou physico-chimiques en généralAppareils appropriés
B08B 3/08 - Nettoyage impliquant le contact avec un liquide le liquide ayant un effet chimique ou dissolvant
The purpose of the present invention is to provide novel solid gold-nickel alloy nanoparticles and a production method thereof. Provided are solid gold-nickel alloy nanoparticles having a particle diameter of 500 nm or less. In particular, gold-nickel alloy nanoparticle are provided in which the concentration of nickel in the gold-nickel alloy is 2.0-92.7 wt %, and the main component is a gold-nickel alloy in which gold and nickel are in a nano-level fine mixed state. The gold-nickel alloy particles have as the main component a substitutional solid solution of gold and nickel. These gold-nickel alloy particles are optimally formed by mixing and discharging gold ions, and a substance having reducing characteristics in the thin film fluid occurring between processing surfaces which are arranged facing each other, which can move towards and away from each other, and at least one of which rotates relative to the other.
C22C 19/03 - Alliages à base de nickel ou de cobalt, seuls ou ensemble à base de nickel
B22F 1/00 - Poudres métalliquesTraitement des poudres métalliques, p. ex. en vue de faciliter leur mise en œuvre ou d'améliorer leurs propriétés
B82Y 30/00 - Nanotechnologie pour matériaux ou science des surfaces, p. ex. nanocomposites
B22F 9/24 - Fabrication des poudres métalliques ou de leurs suspensionsAppareils ou dispositifs spécialement adaptés à cet effet par un procédé chimique avec réduction de mélanges métalliques à partir de mélanges métalliques liquides, p. ex. de solutions
C22C 30/00 - Alliages contenant moins de 50% en poids de chaque constituant
91.
SILICON-DOPED METAL OXIDE PARTICLES, AND UV-ABSORBING COMPOSITION CONTAINING SILICON-DOPED METAL OXIDE PARTICLES
The present invention is intended to provide UV-absorbing silicon-doped metal oxide particles having an increased average molar attenuation coefficient in a wavelength range of 200 nm to 380 nm. The present invention provides silicon-doped metal oxide particles obtained by doping metal oxide particles with silicon, wherein the silicon-doped metal oxide particles are characterized in that a liquid dispersion obtained by dispersing the silicon-doped metal oxide particles in a dispersion medium has a better average molar attenuation coefficient in a wavelength range of 200 nm to 380 nm than when non-silicon-doped metal oxide particles of the same species are used.
A method of producing organic pigment microparticles includes: Step 1 of precipitating organic pigment microparticles by mixing an organic pigment raw material liquid in which an organic pigment raw material is mixed with a solvent, and a precipitation solvent for precipitating the organic pigment microparticles from the organic pigment raw material liquid in a thin film fluid formed by introducing the organic pigment raw material liquid and the precipitation solvent in a space between at least two processing surfaces which are disposed so as to face each other, being capable of approaching to and separating from each other, at least one of which rotates relatively to the other; and Step 2 of coating at least a part of the organic pigment microparticles with an oxide coating; wherein the oxide coating is optically colorless and transparent, and Step 1 and Step 2 are performed out continuously in the thin film fluid.
C09B 67/00 - Traitements, sans réaction chimique, influençant les propriétés physiques, p. ex. de teintures ou d'impression, des matières colorantes, p. ex. traitement par des solvantsCaractéristiques du procédé de fabrication des préparations tinctorialesPréparations tinctoriales ayant un aspect physique particulier, p. ex. tablettes, feuilles
B01F 7/00 - Mélangeurs à agitateurs tournant dans des récipients fixes; Pétrins
B01F 15/02 - Mécanismes d'alimentation ou d'évacuation
93.
METHOD FOR MANUFACTURING HIGHLY CRYSTALLINE SILVER PARTICLES
The present invention is a method for manufacturing fine silver particles by reduction reaction, wherein the method for manufacturing highly crystalline silver particles is characterized in that: a silver solution that includes at least silver ions and a reducing solution that includes at least a reducing agent are made to react by a continuous wet reduction method; fine silver particles are made to precipitate; the reduction rate from the silver solution to the fine silver particles is at least 99%; the average primary particle diameter of the fine silver particles is in the range 100–1000 nm; and the average crystal diameter is at least 80% of the average primary particle diameter of the fine silver particles. The present invention makes it possible to continuously obtain, by a liquid-phase method, fine silver particles with a ratio (d/D) of the average crystal diameter (d) to the average primary particle diameter (D) being at least 95%, i.e., all of the fine silver particles are close to being single crystals.
B22F 9/24 - Fabrication des poudres métalliques ou de leurs suspensionsAppareils ou dispositifs spécialement adaptés à cet effet par un procédé chimique avec réduction de mélanges métalliques à partir de mélanges métalliques liquides, p. ex. de solutions
B22F 1/00 - Poudres métalliquesTraitement des poudres métalliques, p. ex. en vue de faciliter leur mise en œuvre ou d'améliorer leurs propriétés
B22F 9/20 - Fabrication des poudres métalliques ou de leurs suspensionsAppareils ou dispositifs spécialement adaptés à cet effet par un procédé chimique avec réduction de mélanges métalliques à partir de mélanges métalliques solides
94.
Silicon oxide-coated iron oxide composition for coating comprising iron oxide particles coated with silicon oxide
The present invention provides a composition for coating having high ultraviolet ray protection ability for a coating material, and properties required for a coating material such as texture, appearance, designability and weather resistance. The composition is a silicon oxide-coated iron oxide composition for coating comprising iron oxide particles, a primary particle diameter of which is 1 nm or more and 50 nm or less, wherein at least a part of the surface of said iron oxide particles is coated with silicon oxide, and wherein said composition comprises an iron oxide particle dispersion having the average molar absorption coefficient of 1500 L/(mol·cm) or more for the light of the wavelengths from 190 nm to 380 nm in a state that said coated iron oxide particles are dispersed in a dispersion medium. It is preferable that the transmittance of said iron oxide particle containing dispersion for the light of the wavelengths from 200 nm to 420 nm is 2.0% or less, and the transmittance of said iron oxide particle containing dispersion for the light of the wavelengths from 620 nm to 780 nm is 80% or more.
A61K 8/49 - Cosmétiques ou préparations similaires pour la toilette caractérisés par la composition contenant des composés organiques contenant des composés hétérocycliques
A61Q 1/02 - Préparations contenant des colorants cutanés, p. ex. pigments
A61Q 17/04 - Préparations topiques pour faire écran au soleil ou aux radiationsPréparations topiques pour bronzer
The object of the present invention is to provide a method of producing oxide particles, which can improve crystallinity of the obtained oxide particles, more desirably can form single crystal oxide particles stably. The present invention provides a method of producing oxide particles, which comprises at least two fluids to be processed including the first fluid and the second fluid, wherein one of the first fluid and the second fluid is an oxide raw material liquid obtained by mixing at least an oxide particle raw material with a solvent, and the other of the first fluid and the second fluid is an oxide precipitation solvent obtained by mixing at least a basic substance with a solvent, and wherein the method comprises mixing the first fluid and the second fluid in the space between the processing surfaces which are disposed so as to face each other, being capable of approaching to and separating from each other, at least one of which rotates relatively to the other; and discharging the mixed fluid in which the oxide particles are precipitated from the space between the processing surfaces; and wherein the method controls crystallinity of the oxide particles discharged from the space between the processing surfaces, by changing at least one selected from the group consisting of the temperature of the first fluid to be introduced in the space between the processing surfaces, the temperature of the second fluid to be introduced in the space between the processing surfaces, and the temperature of the first fluid and the second fluid at the time of mixing.
C01B 13/00 - OxygèneOzoneOxydes ou hydroxydes en général
C01B 13/32 - Méthodes de préparation des oxydes ou hydroxydes en général par oxydation ou hydrolyse d'éléments ou de composés à l'état liquide ou solide
At least a first fluid and a second fluid are used and are not miscible with each other. At least the first fluid includes one or two items selected from an organic compound, a reactant, and a phase transfer catalyst. From among the fluids other than the first fluid, at least the second fluid includes at least one item from among the items not selected from the three items. The first fluid and second fluid contain all three items. Each of the fluids are merged in a thin-film fluid formed between processing faces that rotate relative to each other. A phase transfer catalyst reaction occurs in the thin-film fluid. Among the first fluid and the second fluid, at least the fluid containing the phase transfer catalyst is prepared so that the phase transfer catalyst is substantially homogeneously mixed before being introduced between the processing faces.
C07C 67/343 - Préparation d'esters d'acides carboxyliques par modification de la partie acide de l'ester sans introduction d'un groupe ester par isomérisationPréparation d'esters d'acides carboxyliques par modification de la partie acide de l'ester sans introduction d'un groupe ester par modification de la taille du squelette carboné par augmentation du nombre d'atomes de carbone
B01J 31/02 - Catalyseurs contenant des hydrures, des complexes de coordination ou des composés organiques contenant des composés organiques ou des hydrures métalliques
C07C 67/333 - Préparation d'esters d'acides carboxyliques par modification de la partie acide de l'ester sans introduction d'un groupe ester par isomérisationPréparation d'esters d'acides carboxyliques par modification de la partie acide de l'ester sans introduction d'un groupe ester par modification de la taille du squelette carboné
C07C 69/757 - Esters d'acides carboxyliques dont un groupe carboxyle est lié à un atome de carbone d'un cycle autre qu'un cycle aromatique à six chaînons dont l'un des groupes OH, O-métal, —CHO, céto, éther, acyloxy, des groupes , des groupes ou des groupes se trouve dans la partie acide
A method of producing efficiently and stably core-shell type oxide particles, wherein the entire surface of the core oxide particles is uniformly coated with the shell oxide, includes at least two steps of: Step 1 of precipitating the core oxide particles in a mixed fluid prepared by mixing an oxide raw material liquid for core and an oxide precipitation solvent and Step 2 of coating the entire surface of the core oxide particles uniformly with the shell oxide by mixing the mixed fluid and an oxide raw material liquid for shell. (A) At least Steps 1 and 2 are performed continuously between at least two processing surfaces 1 and 2 which are capable of approaching to and separating from each other, at least one of which rotates relatively to the other; (B) after Step 1, Step 2 is completed within a prescribed time during which the core oxide particles do not aggregate in the mixed fluid; or (C) Step 1 and Step 2 are controlled so that the primary particle diameter of the core-shell type oxide particles is 190% or less relative to the primary particle diameter of the core oxide particles.
A61K 8/49 - Cosmétiques ou préparations similaires pour la toilette caractérisés par la composition contenant des composés organiques contenant des composés hétérocycliques
A61Q 1/02 - Préparations contenant des colorants cutanés, p. ex. pigments
A61Q 17/04 - Préparations topiques pour faire écran au soleil ou aux radiationsPréparations topiques pour bronzer
C09D 1/00 - Compositions de revêtement, p. ex. peintures, vernis ou vernis-laques, à base de substances inorganiques
An object of the present invention is to provide a method for producing oxide particles with controlled color characteristics and to provide oxide particles with controlled color characteristics. The present invention provides a method for producing oxide particles, comprising controlling color characteristics of the oxide particles by controlling the ratio of M-OH bonds, the binding of one or more different elements (M) other than oxygen or hydrogen with hydroxyl group (OH), in oxide particles selected from metal oxide particles and metalloid oxide particles. According to the present invention, oxide particles having controlled color characteristics of any one of reflectance, transmittance, molar absorption coefficient, hue, or color saturation can be provided by controlling the percentage of the M-OH bonds contained in metal oxide particles or metalloid oxide particles.
The purpose of the present invention is to provide a method for producing a silicon compound-coated oxide particle with controlled color characteristics, and a silicon compound-coated oxide particle with controlled color characteristics. The present invention provides a method for producing a silicon compound-coated oxide particle in which at least part of the surface of the oxide particle is coated with a silicon compound, the method being characterized in that color characteristics are controlled by controlling the ratio of Si-OH bonds included in the silicon compound.
The present invention pertains to a pigment composition for a green filter that includes a green pigment comprising a zinc halide phthalocyanine, wherein the pigment composition for a green filter is characterized in that the spectral transmission characteristics of the green pigment are such that the transmittance at 400 nm is 5% or less, the transmittance at 450 nm is 30% or less, the transmittance at 600 nm is 30% or less, the transmittance at 650 nm is 30% or less, the transmittance at the peak wavelength is 80% or more, the half-value width of the peak wavelength is 130 nm or less, the transmittance at 750 nm is 5% or less, and the transmittance at 800 nm is 35% or less. This pigment composition for a green filter keeps the transmittance of the blue region low, keeps the transmittance in the near infrared region low, and has a high transmittance of the green region.
brevets
