A method of extending shelf-life of food is provided herein. The extended shelf-life is provided by treating the food with at least one shelf-life extender selected from a group consisting of an isothiocyanate, a non-aromatic cyclic ketone, a boronic acid and a ligand.
A food with an extended shelf-life and a method of extending shelf-life of food is provided herein. The extended shelf-life is provided by treating the food with at least one shelf-life extender selected from a group consisting of an isothiocyanate, a non-aromatic cyclic ketone, a boronic acid, a ligand and their precursors.
An ultrasound indicating (USI) device and method for monitoring ultrasonication is provided. The USI device comprises a container comprising a USI formulation. The USI formulation comprises an organic liquid, a pH dye and an activator.
G01N 31/22 - Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroupsApparatus specially adapted for such methods using chemical indicators
G01N 21/01 - Arrangements or apparatus for facilitating the optical investigation
G01N 21/77 - Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator
G01N 21/78 - Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator producing a change of colour
A device is provided for monitoring ultrasonic energy applied to an object. The device comprises a container comprising water and at least one composition selected from the group consisting of: a water insoluble organic liquid as an emulsion aid and an oil; and optionally a pH indicator and at least one of a nitro compound or a halo compound.
G01N 21/78 - Systems in which material is subjected to a chemical reaction, the progress or the result of the reaction being investigated by observing the effect on a chemical indicator producing a change of colour
B08B 3/12 - Cleaning involving contact with liquid with additional treatment of the liquid or of the object being cleaned, e.g. by heat, by electricity or by vibration by sonic or ultrasonic vibrations
C10G 33/06 - De-watering or demulsification of hydrocarbon oils with mechanical means, e.g. by filtration
G01N 21/15 - Preventing contamination of the components of the optical system or obstruction of the light path
Compositions, devices and processes related to etching of a very thin layer or fine particles of a metal are disclosed for monitoring a variety of parameters, such as time, temperature, time-temperature, thawing, freezing, microwave, humidity, ionizing radiation, sterilization and chemicals. These devices have capabilities of producing a long and sharp induction period of an irreversible visual change. The devices are composed of an indicator comprising a very thin layer of a metal (e.g., polyester film having an extremely thin, e.g., about one hundred Angstroms layer of aluminum) and an activator, e.g., a reactant, such as water, water vapor, an acid, a base, oxidizing agent or their precursors, which is capable of reacting with the said indicator. The indicator retains its opacity and metallic luster, e.g., silvery white, mirror like finish of aluminum layer for a long time. The activator destroys the indicator layer including the naturally formed oxide layer. The indicator layer does not have a matrix/binder. As the device becomes transparent from being highly opaque, any color, message or image printed under it become visible at a pre-determined time, thus making the device self reading. A sealing tape or large label made from an activator and an indicator can be used for sealing boxes and monitoring self-life of perishables inside it. Ink formulations composed of a metal powder and a proper activator can be used for monitoring several sterilization processes, such as sterilization with steam. When water is used as an activator, a thin layer of metals, such as that of aluminum can be used as steam sterilization or humidity indicator. The process can also be used for making patterns, printing plates, electronic circuits and RFIDs (radio frequency identification devices).
G01K 3/04 - Thermometers giving results other than momentary value of temperature giving mean valuesThermometers giving results other than momentary value of temperature giving integrated values in respect of time
G01N 31/22 - Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroupsApparatus specially adapted for such methods using chemical indicators
This application relates to a time-temperature indicator based on increased thermal reactivity of diacetylene upon melt recrystallization and a method of making it. A diacetylene is crystallized into a low thermal reactivity phase from a solvent system and converted into a higher thermal reactivity phase and low sensitivity to UV light by melt recrystallization.
G01N 31/22 - Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroupsApparatus specially adapted for such methods using chemical indicators
B41M 5/28 - Thermography using thermo-chromic compounds or layers containing liquid crystals, microcapsules, bleachable dyes or heat decomposable compounds, e.g. gas liberating
C07C 271/12 - Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms with the nitrogen atoms of the carbamate groups bound to hydrogen atoms or to acyclic carbon atoms to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
G01K 3/04 - Thermometers giving results other than momentary value of temperature giving mean valuesThermometers giving results other than momentary value of temperature giving integrated values in respect of time
G01K 11/16 - Measuring temperature based on physical or chemical changes not covered by group , , , or using changes in colour, translucency or reflectance of organic materials
7.
In-Situ Generation of Nucleating Agents for Indicating Devices
A nucleating agent composition, a method of forming the nucleating agent and a device comprising the nucleating agent composition are provided. The nucleating agent comprises a nucleating agent comprises silver halide salt with an average particle size of at least 10 nanometer to no more than 100 microns in a polymeric matrix wherein the polymeric matrix has a viscosity of at least 500 cP to no more than 50,000 cP.
A food with an extended shelf-life and a method of extending shelf-life of food is provided herein. The extended shelf-life is provided by treating the food with isothiocyanate, a non-aromatic cyclic ketone, a boronic acid, a ligand and their precursors.
A food with an extended shelf-life and a method of extending shelf-life of food is provided herein. The extended shelf-life is provided by treating the food with isothiocyanate, a non-aromatic cyclic ketone, a boronic acid, a ligand and their precursors.
A nucleating agent composition, a method of forming the nucleating agent and a device comprising the nucleating agent composition are provided. The nucleating agent comprises a nucleating agent comprises silver halide salt with an average particle size of at least 10 nanometer to no more than 100 microns in a polymeric matrix wherein the polymeric matrix has a viscosity of at least 500 cP to no more than 50,000 cP.
G01K 11/00 - Measuring temperature based on physical or chemical changes not covered by group , , , or
G01K 11/06 - Measuring temperature based on physical or chemical changes not covered by group , , , or using melting, freezing, or softening
G01K 11/12 - Measuring temperature based on physical or chemical changes not covered by group , , , or using changes in colour, translucency or reflectance
G01K 3/04 - Thermometers giving results other than momentary value of temperature giving mean valuesThermometers giving results other than momentary value of temperature giving integrated values in respect of time
11.
In-situ generation of nucleating agents for indicating devices
A nucleating agent composition, a method of forming the nucleating agent and a device comprising the nucleating agent composition are provided. The nucleating agent comprises a nucleating agent comprises silver halide salt with an average particle size of at least 10 nanometer to no more than 100 microns in a polymeric matrix wherein the polymeric matrix has a viscosity of at least 500 cP to no more than 50,000 cP.
A food with an extended shelf-life and a method of extending shelf-life of food is provided herein. The extended shelf-life is provided by treating the food with at least one shelf-life extender selected from a group consisting of an isothiocyanate, a non-aromatic cyclic ketone, a boronic acid, a ligand and their precursors.
A food with an extended shelf-life and a method of extending shelf-life of food is provided herein. The extended shelf-life is provided by treating the food with at least one shelf-life extender selected from a group consisting of an isothiocyanate, a non-aromatic cyclic ketone, a boronic acid, a ligand and their precursors.
G01N 31/22 - Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroupsApparatus specially adapted for such methods using chemical indicators
Compositions, devices and processes related to etching of a very thin layer or fine particles of a metal are disclosed for monitoring a variety of parameters, such as time, temperature, time-temperature, thawing, freezing, microwave, humidity, ionizing radiation, sterilization and chemicals. These devices have capabilities of producing a long and sharp induction period of an irreversible visual change. The devices are composed of an indicator comprising a very thin layer of a metal (e.g., polyester film having an extremely thin, e.g., about one hundred Angstroms layer of aluminum) and an activator, e.g., a reactant, such as water, water vapor, an acid, a base, oxidizing agent or their precursors, which is capable of reacting with the said indicator. The indicator retains its opacity and metallic luster, e.g., silvery white, mirror like finish of aluminum layer for a long time. The activator destroys the indicator layer including the naturally formed oxide layer. The indicator layer does not have a matrix/binder. As the device becomes transparent from being highly opaque, any color, message or image printed under it become visible at a pre-determined time, thus making the device self reading. A sealing tape or large label made from an activator and an indicator can be used for sealing boxes and monitoring self-life of perishables inside it. Ink formulations composed of a metal powder and a proper activator can be used for monitoring several sterilization processes, such as sterilization with steam. When water is used as an activator, a thin layer of metals, such as that of aluminum can be used as steam sterilization or humidity indicator. The process can also be used for making patterns, printing plates, electronic circuits and RFIDs (radio frequency identification devices).
G01N 31/22 - Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroupsApparatus specially adapted for such methods using chemical indicators
G01K 3/04 - Thermometers giving results other than momentary value of temperature giving mean valuesThermometers giving results other than momentary value of temperature giving integrated values in respect of time
Compositions, devices and processes related to etching of a very thin layer or fine particles of a metal are disclosed for monitoring a variety of parameters, such as time, temperature, time-temperature, thawing, freezing, microwave, humidity, ionizing radiation, sterilization and chemicals. These devices have capabilities of producing a long and sharp induction period of an irreversible visual change. The devices are composed of an indicator comprising a very thin layer of a metal and an activator, e.g., a reactant, such as water, water vapor, an acid, a base, oxidizing agent or their precursors, which is capable of reacting with the said indicator. Ink formulations composed of a metal powder and a proper activator can be used for monitoring several sterilization processes, such as sterilization with steam. When water is used as an activator, a thin layer of metals, such as that of aluminum can be used as steam sterilization or humidity indicator.
G01N 31/22 - Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroupsApparatus specially adapted for such methods using chemical indicators
G01K 3/04 - Thermometers giving results other than momentary value of temperature giving mean valuesThermometers giving results other than momentary value of temperature giving integrated values in respect of time
This application relates to a time-temperature indicator based on increased thermal reactivity of a diacetylene upon melt recrystallization and a method of making it. A diacetylene is crystallized into a low thermal reactivity phase from a solvent system and converted into a higher thermal reactivity phase and low sensitivity to UV light by melt recrystallization.
G01N 31/22 - Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroupsApparatus specially adapted for such methods using chemical indicators
B41M 5/28 - Thermography using thermo-chromic compounds or layers containing liquid crystals, microcapsules, bleachable dyes or heat decomposable compounds, e.g. gas liberating
G01K 3/04 - Thermometers giving results other than momentary value of temperature giving mean valuesThermometers giving results other than momentary value of temperature giving integrated values in respect of time
17.
INDICATING DEVICES BASED ON LATERAL DIFFUSION OF A MOBILE PHASE THROUGH A NON-POROUS STATIONARY PHASE
This invention relates to indicating devices, such as time-temperature indicators based on lateral diffusion of a vapor of a solid and/or liquid mobile phase (e.g., a sublimeable dye or an activator) through a non-porous stationary phase, such as a thin layer of a polymeric material. The lateral diffusion of the mobile phase creates a noticeable boundary in the stationary phase whose movement depends upon processes, such as time and temperature.
Indicating devices based on the counter balancing effect of one parameter with that of others are disclosed. Color changing and self -reading indicating devices, such as a time indicator having essentially no effect of temperature are developed by this method. In diffusion based time-temperature indicating devices, the effect of temperature is lowered by crosslinking the medium of the device. The devices have net activation energy near zero kcal/mole.
G04F 1/00 - Apparatus which can be set and started to measure-off predetermined or adjustably-fixed time intervals without driving mechanisms, e.g. egg timers
19.
Freeze, thaw and refreeze indicators based on rapid reactions in the solid state
A freeze indicator, which is preferably a self-activating freeze indicator. The freeze indicator has a substrate with a freeze indicator composition coated thereon wherein the freeze indicator has a liquid diacetylene; and a catalyst or catalyst precursor and a protective cover.
G01K 3/04 - Thermometers giving results other than momentary value of temperature giving mean valuesThermometers giving results other than momentary value of temperature giving integrated values in respect of time
20.
Personal and area self-indicating instant radiation alert dosimeter
Described is a self-indicating instant radiation dosimeter (1001) for monitoring high energy radiations, such as X-ray. The dosimeter contains a radiation sensitive, color changing, indicating composition (10), e.g., a diacetylene (R—C≡C—C≡C—R′, where R and R′ are substituents groups) or a radiochromic dye, a polymeric binder (20) and optionally a shelf life extender (50) or an activator (40). The radiation sensitive composition (10) changes color instantly when exposed to high energy radiation. The dose is estimated by comparing the color with a color reference chart or more accurately with a spectrophotometer or an optical densitometer. The radiation sensitive composition (10) is protected from low energy radiation such as UV light, by a layer of low energy absorbing materials, such as UV absorbers.
A large number of properties of nanostructures depend on their size, shape and many other parameters. As the size of a nanostructure decreases, there is a rapid change in many properties. When the nanostructure is completely destroyed, those properties essentially disappear. Systems based on changes in properties of nanostructures due to the destruction of nanostructures are proposed. The systems can be used for monitoring the total exposure to organic, inorganic, organometallic and biological compounds and agents using analytical methods.
Described is a multi-sensor radiation dosimeter system with (1) a self-indicating, instant radiation sensor and (2) a conventional radiation sensor for monitoring high energy radiations, such as X-ray, electrons and neutrons. Conventional radiation sensors, such as X-ray film, TLD (Thermoluminescence Dosimeters), RLG (Radioluminescence Glass) and OSL (Optically Simulated Luminescence), are highly sensitive but are not instant. In the event of a dirty bomb, nuclear detonation or a radiological accident, one needs to know the exposure instantly so proper precautions can be taken and medical treatment, if required, can be given to the victim. If a self-indicating instant sensor is one of the sensors, one would know the dose instantly, and dose can be determined with higher accuracy than by the traditional methods. This type of device offers the best of both technologies.
A general purpose high accuracy dosimeter reader, 80, for determination of a treatment condition, based on comparison of an image of treated dosimeter, 111, with a series of images of pre-treated dosimeter, 114, is disclosed. A dosimeter undergoes noticeable changes, such as a color change upon treatment with certain materials, such as toxic gases and processes, such as ionizing radiation and sterilization is pre-treated. The dosimeter is imaged with an imaging device, 115, such as charge-coupled device camera and images of the dosimeter or the changes, e.g., color change, are stored in an information storage device, 118. In order to determine the treatment condition, the treatment dosimeter is imaged and the image is compared with the series of pre-treated images of the dosimeter using software. The closest match of the treated dosimeter with the pre-treated and pre-imaged dosimeter would indicate the treatment conditions. The process and device can be used for almost any indicating device, process and treatment.
A tamper resistant and evident, self indicating instant radiation alert dosimeter (referred to as SIRAD) made by encapsulating a radiation sensing system in a polymeric material is disclosed. SIRAD is made from many layers of polymeric materials by multi-step processes. The radiation sensing system of SIRAD is encapsulated in a polymeric media made by a casting or reaction injection molding process.
